Method for preparing master batches through direct PET melt mixing and equipment special for method

A special equipment and melt technology, which is applied in the field of direct mixing of PET melt to produce masterbatch, can solve the problems of insignificant viscosity reduction, melt viscosity reduction, and complicated process, so as to improve the quality of masterbatch, reduce viscosity drop, cost reduction effect

Active Publication Date: 2016-05-11
新凤鸣江苏新拓新材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the problems that the current process is easy to cause melt viscosity reduction, complicated process, waste of resources and high cost, the present invention proposes a process such as insignificant viscosity reduction, reduction of slicing and granulation, drying, solid-phase polycondensation, and powder grinding, which greatly Method and special equipment for preparing masterbatch by direct mixing of melts to reduce electricity, packaging and transportation costs

Method used

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  • Method for preparing master batches through direct PET melt mixing and equipment special for method
  • Method for preparing master batches through direct PET melt mixing and equipment special for method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Embodiment 1 A kind of PET melt of the present invention directly mixes and prepares the method for masterbatch, comprises the steps:

[0028] Step 1. Introduce a melt with a viscosity of 0.63dl / g from the PET main melt pipeline, and mix in matting agent (49%) and dispersant (1%) according to the mass ratio to obtain a compound; mix in matting agent and dispersant in proportion , to obtain the mixture, the mass ratio of the melt: matting agent: dispersant is 1:0.49:0.01; the melt is PET, the matting agent is titanium dioxide, and the dispersant is titanic acid Ester coupling agent;

[0029]Step 2. The mixture obtained in step 1 is entered into a twin-screw extruder under negative pressure for low-speed (120rpm) initial mixing to form an initial mixing melt;

[0030] Step 3. The primary mixed melt coming out of the twin-screw extruder is first blended by an ultrasonic dynamic mixer to obtain a miscible body;

[0031] Step 4. Water-cool the mixed melt from the ultrasoni...

Embodiment 2

[0033] Example 2 The special equipment constructed by the method described in Example 1, including extruder assembly 1, auxiliary material bin assembly 2, dispersant bin assembly 3, ultrasonic dynamic mixing assembly 4, pelletizing assembly 5 , dry packer 6 and control box, the main melt pipeline 7 is connected on the outlet of the discharge assembly 8, and the main melt pipeline 7 is connected with the extruder assembly 1 through the branch melt pipeline 71 The first feed port of the dispersant bin assembly 3 is connected to the first feed port, the discharge port of the auxiliary material bin assembly 2 is configured with the first feed material assembly 91, and the discharge port of the dispersant bin assembly 3 is configured with the second feed material assembly. 92, and the discharge port of the first feeding assembly 91 and the second feeding assembly 92 are all in communication with the second feeding port pipeline of the extruder assembly 1, the extruder assembly 1 Th...

Embodiment 3

[0049] Example 3 Contrast of conventional masterbatch preparation and melt preparation masterbatch

[0050] 1. Case of conventional masterbatch production: carrier PET, matting masterbatch, output 3 tons / day:

[0051] The carrier purchased by the masterbatch factory is PET high-viscosity chips (the chips are made through polymerization, pelletizing, drying, and solid-state polycondensation), with a viscosity of 0.82dl / g. The carrier is first ground into a diameter of about 500 mesh by a mill. Utilize powder metering to send 40% matting agent (TiO2), 59% carrier powder and 1% dispersant into twin-screw extruder (length-to-diameter ratio is 44), twin-screw rotating speed is 300rpm, comes out from screw extruder The melt is water-cooled, pelletized, dried and packaged, and the viscosity of the masterbatch is 0.40dl / g.

[0052] 2. Melt masterbatch production case: carrier PET, matting masterbatch, output 3 tons / day:

[0053]The melt with a viscosity of 0.62dl / g is introduced fr...

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Abstract

Provided are a method for preparing master batches through direct PET melt mixing and equipment special for the method. The method comprises the steps that melt is introduced from a main melt pipeline, a delustering agent and a dispersing agent are mixed in proportion, and the mixture enters a double-screw extruder in a negative-pressure state for low-speed preliminary mixing; and then blending is carried out through an ultrasonic dynamic mixer, dicing, drying and packaging are carried out after water cooling, and the corresponding master batches are prepared. The equipment comprises an extruder assembly, an auxiliary material bin assembly, a dispersing agent bin assembly, an ultrasonic dynamic mixing assembly, a dicing assembly, a drying and packaging machine and a control box. The main melt pipeline is connected to a discharging opening of a discharging assembly, and communicates with a first feeding opening pipeline of the extruder assembly through a branch melt pipeline, and a discharging opening of a corresponding feeding assembly communicates with a second feeding opening pipeline of the extruder assembly. The method and the equipment have the beneficial effects that viscosity is lowered, the quality is stable, and good spinnability is achieved; and the procedures of slicing and dicing, drying, solid phase condensation polymerization, grinding and the like are omitted, and cost is reduced.

Description

technical field [0001] The invention relates to a method for directly mixing PET melts to prepare master batches and special equipment thereof. Background technique [0002] At present, masterbatches are prepared by using carriers such as PET or PBT. These carriers are purchased by the masterbatch factory in the form of slices. These carriers are ground into powder and then mixed into functional powders. They are melted by twin-screw extrusion and subjected to high shear rate. , high-speed mixing and then sent to the granulator, granulated and dried to obtain the masterbatch. However, the twin-screw extrusion process involved in the traditional process requires high-speed rotation and mixing, which makes the viscosity of the melted raw materials drop significantly under the shearing effect of high-speed rotation, so it is necessary to choose high-viscosity slice compensation in the selection of raw materials. The loss of viscosity reduction during the tablet making process ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B29B9/06
CPCB29B9/06
Inventor 庄耀中赵春财孙建杰韩梅
Owner 新凤鸣江苏新拓新材有限公司
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