Preparation method of super-hydrophobic or super-hydrophilic nanofiber membrane with antibacterial performance
A nanofiber membrane and nanofiber technology, applied in fiber processing, non-woven fabrics, filament/thread forming, etc., can solve problems such as large environmental pollution, complex processes, and fluorine-containing materials are not easy to degrade, and achieve cheap raw materials and synthetic Simple, improved selective wettability
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Embodiment 1
[0016] A method for preparing a superhydrophilic nanofiber membrane with antibacterial properties, comprising the following steps:
[0017] A. Step (1) Preparation of polyacrylonitrile solution: Dissolve 10g of polyacrylonitrile powder in 90g of N-N-dimethylformamide solution at room temperature and stir at 100rpm for 12h , until evenly stirred to obtain a polyacrylonitrile solution with a mass fraction of 10wt%;
[0018] B. Step (2) Electrospinning: At room temperature and humidity of 40-50%, the polyacrylonitrile solution prepared in step (1) with a mass fraction of 10wt% is subjected to electrostatic spinning at a rate of 2.5ml / h Spinning, the voltage of electrospinning is 20kV, the distance of electrospinning is 15cm, the receiving carrier of electrospinning is PET non-woven fabric, the drum speed of electrospinning is 50rpm, obtains polyacrylonitrile porous nanofiber film;
[0019] C. Step (3) Preparation of Chitosan Quaternary Ammonium Salt Solution: Dissolve 5g of Chit...
Embodiment 2
[0025] A method for preparing a superhydrophilic nanofiber membrane with antibacterial properties, comprising the following steps:
[0026] A. Step (1) Preparation of polyurethane solution: at room temperature, dissolve 2 g of polyurethane in 45 g of N-N-dimethylformamide and 45 g of tetrahydrofuran solution, and stir at a stirring speed of 100 rpm for 12 hours until Stir evenly, obtain the polyurethane solution that massfraction is 5wt%;
[0027] B. Step (2) Electrospinning: Under the condition of room temperature and humidity of 40-50%, the polyurethane solution with a mass fraction of 5wt% prepared in step (1) was electrospun at a speed of 5ml / h, The voltage of electrospinning is 25kV, the distance of electrospinning is 20cm, the receiving carrier of electrospinning is PET non-woven fabric, the drum speed of electrospinning is 50rpm, and polyurethane porous nanofiber film is obtained;
[0028] C. Step (3) Preparation of chitosan quaternary ammonium salt solution: Dissolve ...
Embodiment 3
[0034] A method for preparing a superhydrophilic nanofiber membrane with antibacterial properties, comprising the following steps:
[0035] A. Step (1) Preparation of polyimide solution: at room temperature, dissolve 20g of polyimide in 40g of N-N-dimethylformamide and 40g of N-methylpyrrolidone solution, and stir, stirring speed Be 100rpm, stirring time is 12h, until stirring evenly, obtaining the polyimide solution that mass fraction is 20wt%;
[0036] B. Step (2) Electrospinning: At room temperature and humidity of 40-50%, the polyimide solution with a mass fraction of 20wt% prepared in step (1) is subjected to electrostatic spinning at a rate of 1ml / h Spinning, the voltage of electrospinning is 25kV, the distance of electrospinning is 10cm, the receiving carrier of electrospinning is PET non-woven fabric, the drum speed of electrospinning is 50rpm, obtains polyimide porous nanofiber film;
[0037] C. Step (3) Preparation of chitosan quaternary ammonium salt solution: Diss...
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