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Dyeing waste water treating agent and preparation method thereof

A technology for printing and dyeing wastewater and treatment agent, applied in the field of printing and dyeing, can solve the problems of high price, limitation, difficulty in regeneration, etc., and achieve the effects of good treatment effect and simple preparation method.

Inactive Publication Date: 2016-05-25
TAICANG JINDA PRINTING & DYEING CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most printing and dyeing factories still use activated carbon adsorption for decolorization, but activated carbon is selective to dyes, the price is high, and regeneration is difficult. The application in the adsorption and decolorization of printing and dyeing wastewater is limited. Generally, it is only used in the treatment or advanced treatment of printing and dyeing wastewater with low concentration.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] (1) Mix bentonite, cornstarch and wheatstarch evenly according to the mass ratio of 15:10:2, add water and extrude into granules with a diameter of 1-2mm;

[0027] (2) Calcining the particles obtained in step (1) at 500-600°C for 5-7 hours, and cooling to room temperature;

[0028] (3) Mix the calcined particles with a 40g / L acrylamide solution and stir;

[0029] (4) Add tert-butyl peroxybenzoate to the mixed system of step (3), react at 50°C for 4h, then add N-methylolacrylamide, react at 45°C for 4h;

[0030] (5) drying the mixture in step (4) to obtain the printing and dyeing wastewater treatment agent.

Embodiment 2

[0032] (1) Mix bentonite, cornstarch and wheatstarch evenly according to the mass ratio of 15:10:2, add water and extrude into granules with a diameter of 1-2mm;

[0033] (2) Calcining the particles obtained in step (1) at 520°C for 6 hours, and cooling to room temperature;

[0034] (3) Mix the calcined particles with 50g / L acrylamide solution in a mixing ratio of 1kg:8L;

[0035] (4) Add tert-butyl peroxybenzoate to the mixed system of step (3), react at 60°C for 6h, then add N-methylolacrylamide, react at 50°C for 2h;

[0036] (5) drying the mixture in step (4) to obtain the printing and dyeing wastewater treatment agent.

Embodiment 3

[0038] (1) Mix bentonite, cornstarch and wheatstarch evenly according to the mass ratio of 15:10:2, add water and extrude into granules with a diameter of 1-2mm;

[0039] (2) Calcining the particles obtained in step (1) at 550°C for 3 hours, and cooling to room temperature;

[0040] (3) Mix the calcined particles with 20g / L acrylamide solution, the mixing ratio is 1kg:8L and stir;

[0041] (4) Add tert-butyl peroxybenzoate to the mixed system of step (3), react at 50°C for 5h, then add N-methylolacrylamide, react at 45°C for 3h;

[0042] (5) drying the mixture in step (4) to obtain the printing and dyeing wastewater treatment agent.

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Abstract

The invention provides a preparation method of a dyeing waste water treating agent, comprising the following steps: (1) mixing bentonite, corn starch and wheat starch uniformly, adding water and extruding into particles 1-2mm in diameter; (2) calcining the particles obtained in step (1) for 5-7h, cooling to room temperature; (3) mixing the calcined particles with an acrylamide solution and stirring; (4) adding an initiator into the mixture system to initiate polyreaction, then adding a cross-linking agent to initiate cross linking reaction to obtain a mixture; and (5) baking the mixture in step (4) to obtain the dyeing waste water treating agent. The dyeing waste water treating agent provided by the invention fully utilizes the expandability and absorbability of the bentonite, has strong absorption on chroma, phosphorus, heavy metal ions, organic matters and the like, and can be used as a purifying agent in waste water treatment.

Description

technical field [0001] The invention belongs to the technical field of printing and dyeing, and in particular relates to a printing and dyeing wastewater treatment agent and a preparation method thereof. Background technique [0002] Although dyes do not have strong acute toxic effects like pesticides, people have found mutagenic and carcinogenic species in azo dyes, anthraquinone dyes, and triphenylmethane dyes, and the degradation products of dyes are mostly linked. Some carcinogenic aromatic compounds such as aniline. As a class of organic compounds with stable structure, dyes have the characteristics of anti-acid, anti-alkali, anti-light, anti-microbial, etc., and have a long residence period in the environment. Very low concentrations of dyes in water will also affect the quality of receiving water. In normal function, it is also toxic to aquatic microorganisms and fish, reducing the diversity of the entire aquatic ecosystem. Therefore, the negative effect of dyes on ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/00C02F1/28C02F1/42C02F101/20
CPCC02F1/00C02F1/281C02F1/42C02F2101/20
Inventor 张惠忠
Owner TAICANG JINDA PRINTING & DYEING CO LTD
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