Preparation method of ATO thermal insulation coating
A heat-insulating coating and ATO technology, applied in polyurea/polyurethane coatings, coatings, etc., can solve the problems of uneven particle size distribution of ATO, affecting heat insulation effect, etc., achieve good heat insulation effect, stable performance, and improve dispersion effect of effect
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[0021] The preparation method of ATO thermal insulation paint of the present invention, it adopts the following steps:
[0022] First, add deionized water to the nano ATO powder and stir evenly to prepare a slurry, and then spray the evenly stirred slurry vertically through the nozzle to the surface of the high-speed rotating roller; during the implementation process, the mass flow rate of the slurry injection should be ensured. 6-8g / s, the vertical distance between the nozzle and the roller is 0.01-0.1mm, the diameter of the roller used at the same time is 40-50mm, and the rotation speed of the roller is 300-350r / min; in the implementation process, the role of the nozzle and the roller makes The slurry is dispersed for the first time, and the slurry thrown to the atomization chamber is impacted by high-speed gas to achieve the second dispersion; this makes the ATO particle size smaller, laying a good foundation for the preparation of stable coatings.
[0023] In the atomizati...
Embodiment 1
[0026] Take ATO powder with a particle size of about 30nm, add it to deionized water to prepare a 20wt% slurry, and then spray the slurry vertically through the nozzle to the surface of the rotating roller; keep the mass flow rate of the slurry injection at 6g / s, the nozzle The vertical distance from the roller is 0.01mm, the diameter of the roller is 40mm, and the rotation speed of the roller is 300r / min; at the same time, in the atomization chamber, maintain an angle of 45° with the horizontal direction, and flow argon at a flow rate of 30m / s Gas impact slurry; then recover gas from the upper side of the atomization chamber, collect ATO slurry from the bottom of the atomization chamber; then, slowly add 40wt% water-based polyurethane emulsion to the collected ATO slurry, wherein ATO slurry and water-based polyurethane emulsion The volume ratio of the mixture was 1:3, and the magnetic stirring speed was 250r / min for 50min and then left to stand to obtain the nano-ATO coating. ...
Embodiment 2
[0028] Take ATO powder with a particle size of about 35nm, add it into deionized water to prepare a 25wt% slurry, and then spray the slurry vertically to the surface of the rotating roller through the nozzle; keep the mass flow rate of the slurry injection at 7g / s, and the nozzle The vertical distance from the roller is 0.05mm, the diameter of the roller is 45mm, and the rotation speed of the roller is 320r / min; at the same time, in the atomization chamber, maintain an angle of 60° with the horizontal direction, and flow argon at a flow rate of 30m / s Gas impact slurry; then recover gas from the upper side of the atomization chamber, collect ATO slurry from the bottom of the atomization chamber; then, slowly add 30wt% water-based polyurethane emulsion to the collected ATO slurry, wherein ATO slurry and water-based polyurethane emulsion The volume ratio of the mixture was 1:4, and the magnetic stirring was performed at a speed of 300r / min for 40min and then left to stand to obtai...
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