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Scale inhibitor formula for intraformational multi-crack fracturing for oilfields and preparation method

A scale inhibitor and fracturing technology, which is applied in the field of oilfield fracturing, can solve the problems of decreased conductivity of proppant filled fractures, small effect of formation conductivity, and rock matrix damage, etc., to extend the effective period of scale prevention and expand The effect of anti-fouling radius and long release time

Active Publication Date: 2016-05-25
BC P INC CHINA NAT PETROLEUM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The main problem of antiscalants represented by the above-mentioned patent documents is that the methods currently used to remove or prevent scale have limitations:
The measures are relatively small, and the intensity of reconstruction of the original pore throats of the reservoir is low, so it is impossible to greatly improve the seepage of the reservoir
[0009] 2. Acidification, damage to the rock matrix, acid discharge after acidification operation will cause serious pollution, and secondary scaling will easily lead to acidification failure
[0010] 3. Fracturing can greatly increase the conductivity of the formation in the short term, but during the production process, formation scaling, clay swelling, iron ion precipitation and organic matter precipitation will greatly reduce the conductivity of the fractures filled with proppant and the measures will fail
[0011] 4. Composite measures, acidification and extrusion injection plugging removal are relatively single, and have a relatively small effect on improving the formation conductivity; the joint operation of extrusion anti-scaling agent and fracturing can greatly improve the formation conductivity and delay scaling Speed, but squeezing the antiscalant Relying on a single injection of antiscalant cannot solve the long-term antiscaling problem

Method used

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  • Scale inhibitor formula for intraformational multi-crack fracturing for oilfields and preparation method
  • Scale inhibitor formula for intraformational multi-crack fracturing for oilfields and preparation method
  • Scale inhibitor formula for intraformational multi-crack fracturing for oilfields and preparation method

Examples

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Effect test

Embodiment 1

[0029] This embodiment provides a formula of antiscalant for multi-fracture fracturing in an oil field, which consists of the following substances in percentage by weight: 30-50% of coating agent, 45-65% of antiscaling agent, 2- 5%.

[0030] Preparation process: After preparing the components, mix them in the reactor, raise the temperature of the reactor to 300-400°C while stirring, continue to stir for 20-30 minutes, and finally use granulation equipment to prepare irregular particles of 1-3mm , to produce antiscalant products for intralayer multi-fracture fracturing.

Embodiment 2

[0032] This example provides a formula of scale inhibitor for multi-fracture fracturing in an oil field, and its preparation process is as follows:

[0033] Step 1) According to the percentage by weight of the anti-fouling agent, first add 25% polyvinyl alcohol 2488 and 25% low molecular weight linear polyethylene, 15% polyamino polyether methylene phosphonic acid, 2% hexametaphosphate in the reactor , 5% zinc sulfate heptahydrate, 5% silicon phosphorus crystal, 18% sodium polyaspartate, G528 adhesive 5%;

[0034] Step 2) Melt, raise the temperature of the reactor to 350°C under stirring conditions, and continue stirring for 20 minutes;

[0035] Step 3) granulation, using granulation equipment to prepare irregular granules of 1-3 mm, and produce antiscalant products for multi-fracture fracturing in layers used in oil fields.

[0036] In this embodiment, the coating agent is a mixture of polyvinyl alcohol 2488 and low-molecular-weight linear polyethylene, accounting for 50% by...

Embodiment 3

[0038] This example provides a formula of scale inhibitor for multi-fracture fracturing in an oil field, and its preparation process is as follows:

[0039] Step 1) According to the percentage by weight of the anti-fouling agent, first add 22% polyvinyl alcohol 2488 and 18% low molecular weight linear polyethylene, 15% polyamino polyether methylene phosphonic acid, 5% hexametaphosphate in the reactor , 5% zinc sulfate heptahydrate, 13% silicon phosphorus crystal, 10% sodium polyaspartate, G528 adhesive 2%;

[0040] Step 2) Melt, raise the temperature of the reactor to 350°C under stirring conditions, and continue stirring for 20 minutes;

[0041] Step 3) granulation, using granulation equipment to prepare irregular granules of 1-3 mm, and produce antiscalant products for multi-fracture fracturing in layers used in oil fields.

[0042] In this embodiment, the coating agent is a mixture of polyvinyl alcohol 2488 and low-molecular-weight linear polyethylene, accounting for 40% b...

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Abstract

The invention provides a scale inhibitor formula for intraformational multi-crack fracturing for oilfields. The scale inhibitor formula comprises, by weight, 30-50% of coating agent, 45-65% of scale inhibitor and 2-5% of adhesive. The scale inhibitor is high in compatibility and applicable to formation water of formations at different temperatures and in different ranges of pH and mineralization degree; the acting range is large, the antiscale radius can be enlarged, the valid period of scale prevention is prolonged, and all-sided scale prevention for immediate vicinity of wellbores, production wellbores and surface pipelines is achieved; the release time is long, the dissolving time in oil and water is more than 400 days, the scale-inhibition effect is good, and the scale inhibition rate reaches over 92.2%.

Description

technical field [0001] The invention belongs to the technical field of oil field fracturing, and in particular relates to a formula and a preparation method of a scale inhibitor for multi-fracture fracturing in an oil field. Background technique [0002] In the process of oil field production, when the fluid flows into and out of the wellbore, scale is formed due to sudden changes in temperature, pressure and flow velocity, resulting in scaling in the perforation section of the wellbore of the production well, the inner wall of the downhole tubing, the screen pipe, the liner pipe, and the inner wall of the pump pipe. , the liquid production rate drops or no liquid is produced; due to the incompatibility of the injected water and the formation water, the water injection well scales near the wellbore, which increases the pressure of the water injection well, fails to meet the injection requirements, and seriously affects the oilfield production. [0003] For oil-water wells th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/528
CPCC09K8/528
Inventor 万向辉蒋文学吴增智李勇汪小宇金娜谢新秋王玉功马托周然武龙王所良唐冬珠徐伟星荆建春王坤樊庆缘杨发陈迎花柴巧玲安全成
Owner BC P INC CHINA NAT PETROLEUM CORP
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