Angelica sinensis glycerol triacetate extract and application thereof to cigarettes

A technology of triacetin and extract, which is applied to the application field of angelica triacetin extract and angelica triacetin extract in cigarettes, which can solve the difficulty of filter sticks, increase production costs, limited solubility of additives, Complicated preparation process and other issues, to achieve the effect of covering cigarette miscellaneous gas, strong operability and standardization, and simple production process

Inactive Publication Date: 2016-07-06
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, this method of adding and applying has complicated preparation process and limited dissolving ability of triacetin for additives, and many extracts that have the effect of enhancing and invigorating the flavor of cigarettes are difficult to dissolve in triacetin, which limits this type of Application of Extract in Cigarette Filter Stick
On the other hand, if the filter rod is not flavored with triacetin as a carrier, but the additive is directly applied to the cigarette filter rod, it will bring greater difficulty to the production of the filter rod and significantly increase the production cost, which is not conducive to large-scale production. Scale promotion and application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Take the air-dried root of Angelica sinensis, cut into pieces, pulverize it with a pulverizer, and pass through a 40-mesh sieve to obtain angelica powder; weigh 300g of Angelica sinensis powder and place it in an extraction bottle, and add triacetin for tobacco at a ratio of 1:10. , stirred evenly and soaked for 2 hours, carried out ultrasonic extraction at 40°C, the extraction power was 400W, 40kHZ, the extraction time was 40 minutes, cooled to room temperature, and the resultant was placed in a microwave extractor for further extraction (200W, 40°C), Extract for 30 minutes, withdraw the microwave extractor, reflux the resultant at 70°C for 3 hours, cool to room temperature and filter off the residue to obtain a clear solution, which is the desired angelica triacetin extract.

[0023] Using glyceryl triacetate as a solvent, the extract of angelica triacetin is formulated into a solution with a concentration of 0.05%, and is evenly sprayed on the filter rod tow in a prop...

Embodiment 2

[0025] Take the root of Angelica sinensis dried in the air, cut it into pieces, pulverize it with a pulverizer, and pass through a 50-mesh sieve to obtain angelica powder; weigh 400g of Angelica sinensis powder and place it in an extraction bottle, and add glycerol triacetate for tobacco at a ratio of 1:15. , stirred evenly and soaked for 3 hours, carried out ultrasonic extraction at 45°C, the extraction power was 500W, 40kHZ, the extraction time was 60 minutes, cooled to room temperature, and the resultant was placed in a microwave extractor for further extraction (300W, 40°C), After extracting for 40 minutes, the microwave extractor was withdrawn, and the resultant was refluxed and extracted at 80°C for 4 hours. After cooling to room temperature, the residue was filtered off to obtain a clear solution, which was the desired angelica triacetin extract.

[0026] Using glyceryl triacetate as a solvent, the extract of angelica triacetin is prepared into a solution with a concentr...

Embodiment 3

[0028] Take the root of Angelica sinensis dried in the air, cut it into pieces, pulverize it with a pulverizer, and pass it through a 60-mesh sieve to obtain angelica powder; weigh 500g of Angelica sinensis powder and place it in an extraction bottle, and add triacetin for tobacco at a ratio of 1:10 , stirred evenly and soaked for 4 hours, ultrasonic extraction was carried out at 50°C, the extraction power was 600W, 40kHZ, the extraction time was 80 minutes, cooled to room temperature, and the resultant was placed in a microwave extractor for further extraction (400W, 50°C), After extraction for 60 minutes, the microwave extractor was withdrawn, and the resultant was extracted under reflux at 90°C for 6 hours. After cooling to room temperature, the residue was filtered off to obtain a clear solution, which was the desired angelica triacetin extract.

[0029] Using glyceryl triacetate as a solvent, the extract of angelica triacetin is prepared into a solution with a concentratio...

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PUM

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Abstract

The invention discloses angelica sinensis glycerol triacetate extract and application thereof to cigarettes.A preparation method of the angelica sinensis glycerol triacetate extract includes: using angelica sinensis powder obtained by sieving crushed dried angelica sinensis as the raw material and glycerol triacetate as extracting agent, and sequentially using ultrasonic extraction, microwave extraction and heating reflux extraction to obtain the angelica sinensis glycerol triacetate extract.A method for applying the angelica sinensis glycerol triacetate extract to the cigarettes includes: using glycerol triacetate as the solvent to prepare the angelica sinensis glycerol triacetate extract into a solution with the concentration being 0.05-0.10%, spraying the solution to filter stick tows according to a proportion that the weight of the solution accounts for 7-8% of the weight of cellulose acetate tows so as to obtain cigarette filter sticks, and using a conventional cigarette connecting procedure to produce the cigarettes with the filter sticks containing the effective components of angelica sinensis.The angelica sinensis glycerol triacetate extract can enrich the fragrance of the cigarettes, increase the sweetness of the cigarettes and evidently increase the smoking quality of the cigarettes.The preparation method is high in operability and normalization, easy in raw material obtaining, low in cost, simple in production process, convenient to achieve industrial production and promising in application prospect.

Description

technical field [0001] The invention belongs to the technical field of cigarette materials, and in particular relates to an angelica triacetin extract. At the same time, the invention also relates to the application of the angelica triacetin extract in cigarettes. Background technique [0002] Angelica, Radix Angelicae Sinensis, also known as Qingui, Yungui, West Angelica, and Rising Angelica. At present, the medicinal material Angelica sinensis refers to the root of the Umbelliferae plant Angelica sinensis. After processing, the medicinal material is nearly cylindrical, and there are many branched roots in the lower part, which are 15-35cm long. The surface is yellowish brown to brown exhausted, with longitudinal wrinkles and horizontal long lenticels. The diameter of the root head is 1.5-4.0 cm, with ring patterns, purple or yellow-green stem and leaf residues, and the surface of the main root is uneven; the diameter of the branch roots is 0.3-1.0 cm, thick at the top a...

Claims

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Application Information

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IPC IPC(8): C11B9/00A24D3/14
CPCC11B9/00A24D3/14
Inventor 韦克毅杜宇朱保昆凌军唐军林文强李超
Owner CHINA TOBACCO YUNNAN IND
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