Graphene heating film and preparation method thereof
A technology of graphene heating film and graphene film, applied in the field of graphene heating film and its preparation, can solve the problems of long transfer time and low transfer rate, and achieve the effects of short transfer time, high transfer rate and simple preparation steps
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[0066] Such as figure 2 As shown, a method for preparing a graphene heating film provided by the present invention includes the following process steps:
[0067] 1) The production of graphene film, the chemical vapor deposition method is used to prepare the graphene film on the surface of the metal substrate;
[0068] 2) Use spraying, brushing or rolling to cover the second insulating waterproof layer 4 with adhesive glue;
[0069] 3) Bonding the second insulating waterproof layer 4 covered with adhesive glue and the graphene film into a whole;
[0070] 4) Use mechanical peeling or electrochemical corrosion to remove the metal matrix on the graphene film to form a graphene film with an insulating and waterproof layer;
[0071] 5) Pasting the electrode layer 2 on the graphene film covered with the first insulating and waterproof layer 1;
[0072] 6) Paste the first insulating and waterproof layer 1 on the electrode layer 2;
[0073] 7) Connect the electrode layer 2 with the wire to prepa...
Example Embodiment
[0100] Example 1
[0101] 1) Choose to prepare a layer of graphene film on the surface of the metal substrate (such as aluminum foil, copper foil or nickel foil) by chemical vapor deposition at a temperature of 25°C, normal pressure, and inert gas (such as helium, neon, etc.) , Grow in a sterile environment for 15 hours, and prepare a layer of graphene film with a thickness of 30 μm;
[0102] 2). Choose one or more of polyurethane, polystyrene, epoxy resin and acrylate as the adhesive, and spray, brush or roll on the second insulating waterproof layer 4 (such as PVC film , PE film or PET film) prepare an adhesive layer with a thickness of about 150-280μm;
[0103] 3). Cover the surface of the graphene-grown substrate with PVC film, PE film or PET film with a bonding layer, and apply it for 5 hours under an environment with a temperature of 50°C and a pressure of 50 Pa. The second insulating and waterproof layer 4 of the layer is bonded to the graphene film as a whole;
[0104] 4). R...
Example Embodiment
[0108] Example 2
[0109] The difference between embodiment 2 and embodiment 1 is only in step 1), step 3) and step 4), and other steps are the same as in embodiment 1).
[0110] 1) Choose to prepare a layer of graphene film on the surface of the metal substrate (such as aluminum foil, copper foil or nickel foil) by chemical vapor deposition at a temperature of 25°C, normal pressure, and inert gas (such as helium, neon, etc.) , Grow in a sterile environment for 17 hours, prepare a layer of graphene film with a thickness of 38 μm;
[0111] 3). Cover the surface of the graphene-grown substrate with PVC film, PE film or PET film with an adhesive layer. Under an environment with a temperature of 90°C and a pressure of 50 Pa, it will be covered with adhesive for 3.2 hours. The second insulating and waterproof layer 4 of the junction layer is bonded to the graphene film as a whole;
[0112] 4). The metal matrix on the graphene film is removed by mechanical peeling or electrochemical corros...
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