Preparation method of red light emitting fluorescent powder

A technology of red phosphor powder and red light, which is applied in the direction of luminescent materials, chemical instruments and methods, etc., can solve the problems of difficulty in film formation of phosphor powder in the LED light-emitting layer, short device life, poor anti-ultraviolet performance, etc., and achieve data Accurate and detailed, high precision, good purity effect

Active Publication Date: 2016-08-31
TAIYUAN UNIV OF TECH
View PDF3 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, the synthesis of red light phosphors is mainly based on the rare earth metal Eu as the central ion and the polymer material as the matrix to prepare red light materials. Although its luminous performance has been improved, there are still LED light-emitting layer phosphors made of it. Defects of difficult film formation, poor UV resistance, and short device life

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of red light emitting fluorescent powder
  • Preparation method of red light emitting fluorescent powder
  • Preparation method of red light emitting fluorescent powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0058] The present invention will be further described below in conjunction with accompanying drawing

[0059] figure 1 As shown, the state diagram for the preparation of the polymer, the position of each part must be correct, the proportion should be proportioned, and the operations should be performed in sequence.

[0060] Quantities of chemicals used in preparation are determined in pre-set ranges in grams, milliliters, centimeters 3 is the unit of measurement.

[0061] The preparation of the polymer is carried out in a three-necked flask, which is completed in a water bath, heating, magnetic stirring, nitrogen protection, and water circulation condensation;

[0062] The electric heater 1 is vertical, and the upper part of the electric heater 1 is a water bath 2, and the upper part of the water bath 2 is a three-necked flask 3, which is fixed by a fixed frame 21. The water bath 2 is a water bath 4, and the water bath 4 needs Submerge 4 / 5 of the volume of the three-necked...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
Login to view more

Abstract

The invention relates to a preparation method of red light emitting fluorescent powder. By aiming at the conditions of difficult film forming of red light fluorescent powder and poor ultraviolet light resistant performance, 2-thenoyltrifluoroacetone-phenanthroline-methacrylic acid-europium and (4-vinyl phenyl) trimethoxy silane is used as raw materials to prepare the red light emitting fluorescent powder through solution preparation, polymerization reaction, washing, suction filtration, vacuum freeze drying, grinding and screening. The preparation method has the advantages that the process is advanced; the data is precise, full and accurate; the prepared powder body material has high precision and good purity; the purity reaches 9.2 percent; the powder body particle diameter is less than or equal to 800nm; the chromaticity coordinate X is 0.625; Y is 0.308; red light is emitted out; the materials can be matched with blue and green luminous materials to be prepared into white light emitting light emitting diodes; the preparation method belongs to an advanced red light emitting fluorescent powder preparation method.

Description

technical field [0001] The invention relates to a method for preparing a phosphor powder emitting red light, and belongs to the technical field of preparation and application of luminescent materials. Background technique [0002] Silicone is the mainstream material of LED packaging materials, with Si-O-Si bond as the main chain and side chains containing organic groups, which have excellent heat resistance, UV resistance and processing performance. [0003] White light-emitting diodes (LEDs) are known as the fourth-generation green light sources because of their small size, low energy consumption, and long life, and have been widely used in industrial and civilian products. [0004] White light is a kind of composite light, which can be compounded by ultraviolet light to excite phosphors of red, green and blue three primary colors to obtain white light. Its color temperature and color rendering performance depend on the content of red light components. The role of color co...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C08F230/08C08F230/04C09K11/06
CPCC08F230/04C08F230/08C09K11/06C09K2211/182
Inventor 张爱琴贾虎生赵希瑾杨亚敏刘旭光许并社
Owner TAIYUAN UNIV OF TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products