Piezoresistive/piezoelectric interlayer material and preparation and application methods thereof, and interlayer type sensor and preparation and application methods thereof

A sandwich material, piezoelectric sensing technology, applied in chemical instruments and methods, the use of electric/magnetic devices to transmit sensing components, lamination and other directions, can solve the problems of insufficient toughness, deformation and dislocation of the package shell and the internal core sensor components, etc.

Active Publication Date: 2016-09-21
QINGDAO TECHNOLOGICAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the production of this sensor (energy harvester) still needs to adopt special pressing molding, high-temperature calcination, silver, high-voltage polarization and other complex processes, and the sensor made is relatively rigid, and the toughness is not high enough, and then the outer shell and the internal core sensor are packaged. Parts are prone to deformation and dislocation, resulting in some insurmountable defects in actual use, which urgently need further optimization and improvement

Method used

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  • Piezoresistive/piezoelectric interlayer material and preparation and application methods thereof, and interlayer type sensor and preparation and application methods thereof
  • Piezoresistive/piezoelectric interlayer material and preparation and application methods thereof, and interlayer type sensor and preparation and application methods thereof
  • Piezoresistive/piezoelectric interlayer material and preparation and application methods thereof, and interlayer type sensor and preparation and application methods thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Such as figure 1 As shown, the sandwich sensor using piezoresistive / piezoelectric interlayer materials of the present invention includes a tough substrate 1, a self-assembled film piezoresistive sensing functional layer 2 (including top / bottom electrodes), a piezoelectric sensing elastic sandwich functional layer 3. The encapsulation layer 5 and the electromagnetic shielding wire 6 connected to the top / bottom electrodes and penetrating the encapsulation layer. The electromagnetic shielding wire 6 is connected to the electrode static / dynamic signal acquisition system through the shielding connector.

[0044] The preparation steps of the piezoresistive / piezoelectric interlayer material are as follows:

[0045] (1) Preparation of CNT self-assembled film piezoresistive sensing functional layer (top / bottom electrode layer)

[0046] ①Introduction of negatively charged functional groups on the surface of CNT

[0047] Pretreatment and purification of CNT: Weigh a certain am...

Embodiment 2

[0070] Such as figure 2As shown, the tough substrate is disc-shaped, and the piezoelectric sensing elastic core functional layer 3 is attached to the outer surface of the spring 4 . Wherein the piezoelectric sensing elastic core functional layer of the CNT / ZnO sensor is the CNT self-assembled thin film piezoresistive film prepared by spinning the ZnO / PDMS slurry prepared in step (2) in Example 1. Sensing the inner layer of the top / bottom electrode of the functional layer and the surface of four stainless steel springs with equal length and stiffness; and while the ZnO / PDMS slurry is still in a semi-fluid state, the four corners of the interlayer stainless steel springs are symmetrically arranged on the top of the oppositely bonded CNTs. / Between the bottom electrode; finally transfer to a vacuum box, set the vacuum degree, temperature and reaction time to 0.05Pa, 40°C and 36 hours respectively, to obtain the CNT / ZnO piezoelectric sensing elastic sandwich functional layer.

...

Embodiment 3

[0075] The preparation process and structure of the piezoresistive / piezoelectric interlayer sensor are the same as in Example 1. The difference is: the nano conductive material used is GO (thickness 3-5 nanometer sheet, area average 2.7μm 2 , conductivity greater than 2S / cm); the piezoelectric sensing elastic core functional layer is a slurry made of polyvinylidene fluoride (PVDF) powder ultrasonically assisted in dissolving N-methylpyrrolidone, and then mixed with PDMS and PDMS curing agent made.

[0076] Using LCR digital bridge, quasi-static measuring instrument, and impedance analyzer to test the DC resistivity of 6 double-layer GO films in GO / PVDF piezoresistive / piezoelectric interlayer sensors, the DC resistivity is 398.4kΩ·cm, and the AC resistivity at 10kHz frequency 15.2kΩ cm; the piezoelectric gauge coefficient of the PVDF / PDMS layer is 21.5pC / N; combined with Wheatstone bridge technology and dynamic signal acquisition technology to study the sensitivity of the resi...

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Abstract

The invention relates to a piezoresistive / piezoelectric interlayer material and preparation and application methods thereof, and an interlayer type sensor and preparation and application methods thereof, used for engineering structure monitoring. The piezoresistive / piezoelectric interlayer material comprises a tenacious substrate, 5-50 self-assembly film piezoresistive perception function layer double-layers, i.e., top / bottom electrode layers, and a piezoelectric perception elastic core sandwich function layer which is prepared by a nanometer ZnO / PDMS or PVDF / PDMS and can comprise a stainless steel spring. After integral packaging, an interlayer type sensor pasted to the surface of an engineering structure or an embedded interlayer type sensor is obtained, the sensor has the advantages of good flexibility, high piezoresistive / piezoelectric perception sensitivity covering a full traffic frequency domain, good linearity, high stability and the like, and basic functions of such a structure itself are not affected.

Description

technical field [0001] The invention relates to a piezoresistive / piezoelectric interlayer material for engineering structure monitoring, an interlayer sensor, and a preparation and use method. Background technique [0002] With the rapid development of the national economy and the vigorous development of the construction industry, large-scale civil engineering structures and infrastructure, such as long-span bridges, tunnels, super high-rise buildings, etc. can be seen everywhere. Their service life spans decades, some even hundreds of years. However, these large structures (bridges, tunnels, stadiums and high-rise buildings, etc.) in the exposed environment will reduce the durability of the structure under the influence of material variation, load change, natural disasters, human factors, etc. , leading to failure before reaching the designed service life. Therefore, in order to improve the durability and earthquake resistance and disaster reduction capabilities of these ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01D5/12B32B33/00B32B37/14
CPCB32B33/00B32B37/144G01D5/12
Inventor 罗健林李秋义赵铁军王旭吴晓平
Owner QINGDAO TECHNOLOGICAL UNIVERSITY
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