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Efficient preparation method for flexible ultra-extension conductive thin film based on one-dimensional nano material

A technology of nano-materials and conductive films, which is applied in the field of nano-optical materials, can solve the problems of film damage, low efficiency, and the inability to pre-stretch the film, and achieve the effects of complete transfer, simple preparation process, and easy mass production

Active Publication Date: 2016-09-21
NANJING UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to address the deficiencies of the prior art and combine the advantages of pre-stretched PDMS and direct curing PDMS to prepare flexible and extensible conductive films. The high-efficiency preparation of conductive material films solves the problems of previous film transfers that cannot be pre-stretched, low efficiency, and film damage.

Method used

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  • Efficient preparation method for flexible ultra-extension conductive thin film based on one-dimensional nano material
  • Efficient preparation method for flexible ultra-extension conductive thin film based on one-dimensional nano material
  • Efficient preparation method for flexible ultra-extension conductive thin film based on one-dimensional nano material

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Effect test

Embodiment 1

[0034] A high-efficiency preparation method based on carbon nanotube flexible super-extended conductive film, comprising the following steps:

[0035] a. Fabrication of flexible and stretchable PDMS substrates

[0036] 1) Mix basic component A and curing agent B at a mass ratio of 10:1, stir for 30 minutes, mix evenly, and pump air bubbles;

[0037] 2) Mix components A and B without air bubbles, stir again for 10 minutes, and pump out air bubbles;

[0038] 3) Transfer it to a plastic petri dish and pump air bubbles;

[0039] 4) Place the culture dish at 70°C and cure for 7 hours;

[0040] 5) Finally, peel off the PDMS and the plastic Petri dish.

[0041] b. Preparation of one-dimensional nanomaterial solution

[0042] Take 0.01g of carbon nanotubes into a 15ml centrifuge tube, suck 10ml of ethanol with a straw, seal it with plastic sealing tape, put it into an ultrasonic machine with a power of 240w for 6 hours, centrifuge, and let it stand overnight.

[0043] c. Cleaning...

Embodiment 2

[0052] A high-efficiency preparation method based on silver nanowire flexible super-extended conductive film, comprising the following steps:

[0053] a. Fabrication of flexible and stretchable PDMS substrates

[0054] 1) Mix basic component A and curing agent B at a mass ratio of 10:1, stir for 30 minutes, mix evenly, and pump air bubbles;

[0055]2) Mix components A and B without air bubbles, stir again for 10 minutes, and pump out air bubbles;

[0056] 3) Transfer it to a plastic petri dish and pump air bubbles;

[0057] 4) Place the culture dish at 70°C and cure for 7 hours;

[0058] 5) Finally, peel off the PDMS and the plastic Petri dish.

[0059] b. Cleaning of glass sheets

[0060] Sonicate the cut 2.5*2.5cm glass slides in deionized water, isopropanol, ethanol, and deionized water for 10 minutes, and finally dry them with nitrogen.

[0061] c. Efficient preparation of ultra-extensible, highly stable, one-dimensional nanomaterial thin films:

[0062] 1) Take 5mg / ...

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Abstract

The invention discloses an efficient preparation method for a flexible ultra-extension conductive thin film based on a one-dimensional nano material, and belongs to the technical field of nano photoelectric materials. The preparation method comprises the steps of firstly, evenly spraying a one-dimensional nano conductive material solution on a hard substrate so as to prepare a conductive thin film; secondly, evenly spinning an uncured PDMS colloid at the surface of the conductive thin film, then placing a stretched cured PDMS film at the surface of an uncured PDMS film, and finally applying great pressure and placing the film in a vacuum drying oven so as to be cured. The preparation method provided by the invention for the flexible ultra-extension conductive thin film is simple in operation, low in cost and wide in application range. The preparation method has the characteristics of efficient transfer process and large-area preparation. The prepared conductive thin film shows prominent advantages of flexible ultra-extension and stable electrical performance.

Description

technical field [0001] The invention belongs to the technical field of nano-optoelectronic materials, relates to the technical field of nano-materials, conductive materials and conductive films, and in particular to a high-efficiency preparation method for flexible super-extended conductive films based on one-dimensional nano-materials. Background technique [0002] One-dimensional nanomaterials refer to materials that have two dimensions in the nanoscale range. One-dimensional nanomaterials include nanotubes, nanorods, nanowires, quantum wires, and nanobelts. Among them, one-dimensional nano-conductive materials with conductive functions have great potential in emerging strategic fields such as flexible transparent conductive films, flexible touch screens, flexible optoelectronic devices, and wearable electronics due to their unique thermal stability, mechanical flexibility, electronic transmission, and optical properties. Wide application prospects. It is of practical si...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B13/00B82Y30/00
CPCH01B13/0013B82Y30/00
Inventor 刘举庆曹立君黄维刘洋王展
Owner NANJING UNIV OF TECH
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