Hard magnetic compositions from iron oxide fines and methods for making same
一种铁氧化物、氧化物的技术,应用在铁化合物、化学仪器和方法、电感/变压器/磁铁制造等方向,能够解决安全处理昂贵、担忧等问题
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Embodiment 1
[0164] In one aspect, Tables 1 and 2 below show typical analyzes of iron ore materials or oxide fines that may be used to produce the disclosed hard magnetic materials. In other aspects, other ingredients can include various amounts of carbon, sulfur, sodium, potassium, and / or calcium.
[0165] Table 1. *
[0166]
[0167] * Amount provided as a percentage of the total composition (by weight)
[0168] Table 2. *
[0169]
[0170] * Amount provided as a percentage of the total composition (by weight)
Embodiment 2
[0172] In a general aspect, hard magnetic materials are prepared by mixing in a dry blend for a predetermined duration. The premix is then dry milled for a predetermined duration. The blended powder mixture is then calcined at about 1000° C. for 4 to 12 hours and then reground in a dry atmosphere. Then, the calcined and ground mixture is fired at about 1100° C. to 1300° C. for about 2 to 6 hours at a heating rate of 10° C. / min in an air atmosphere. After firing, the cooled mixture was characterized by X-ray diffraction analysis (XRD), X-ray fluorescence (XRF), scanning electron microscopy (SEM) and vibrating sample magnetometer (VSM).
[0173] In this example, strontium carbonate (SrCO 3 ) (99% chemical purity) and steelmaking by-product iron oxides to prepare the hard magnetic material (SrFe 12 o 19 ). The iron oxide samples were characterized using X-ray diffraction analysis (XRD), X-ray fluorescence (XRF) and scanning electron microscopy (SEM). The discovery of iron...
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