Medium-density rigid polyurethane foam material and preparation method thereof
A polyurethane rigid foam, medium density technology, applied in the field of structural materials and their preparation, composite materials, can solve the problems of poor impact resistance, poor resilience, short storage period, etc., and achieve good compression resistance and waterproof performance. Good, long shelf life effect
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Embodiment 1
[0030] Embodiment 1: a kind of medium density polyurethane rigid foam material and preparation method thereof, its preparation process is:
[0031] Polyether polyol A (hydroxyl value 30mgKOH / g) 25kg
[0032] Polyether polyol B (hydroxyl value 295mgKOH / g) 25kg
[0033] Polyether polyol C (hydroxyl value 440mgKOH / g) 30kg
[0034] water 14kg
[0035] N,N-Dimethylcyclohexylamine 0.15kg
[0036] Pentamethyldiethylenetriamine 1kg
[0037] N-formylmorpholine 0.6kg
[0038] Glycerol 3kg
[0039] Silicone oil (viscosity (25°C) is 750mPa·s) 5kg
[0040] Polyisocyanate (NCO mass fraction is 31%) 100kg
[0041] (1) Weigh each raw material according to the formula quantity;
[0042] (2) Put polyether polyol A, polyether polyol B, polyether polyol C, glycerin and silicone oil in a mechanically stirred tank for 15 minutes, in 1×10 4 Remove air bubbles under Pa vacuum for 15 minutes to prepare the main mixture;
[0043] (3) Mix water, N,N-dimethylcyclohexylamine, pentamethyldiethyle...
Embodiment 2
[0046] Embodiment 2: a kind of medium density polyurethane rigid foam material and preparation method thereof, its preparation process is:
[0047] Polyether polyol A (hydroxyl value 20mgKOH / g) 20kg
[0048] Polyether polyol B (hydroxyl value 280mgKOH / g) 20kg
[0049] Polyether polyol C (hydroxyl value 420mgKOH / g) 20kg
[0050] water 10kg
[0051] N,N-Dimethylcyclohexylamine 0.1kg
[0052] Pentamethyldiethylenetriamine 0.8kg
[0053] N-formylmorpholine 0.4kg
[0054] Glycerol 2kg
[0055] Silicone oil (viscosity (25°C) is 650mPa·s) 4kg
[0056] Polyisocyanate (NCO mass fraction is 29%) 100kg
[0057] (1) Weigh each raw material according to the formula quantity;
[0058] (2) Put polyether polyol A, polyether polyol B, polyether polyol C, glycerin and silicone oil in a mechanical stirring tank and stir for 10 minutes, 5 Remove air bubbles under Pa vacuum for 10 minutes to prepare the main mixture;
[0059] (3) Mix water, N,N-dimethylcyclohexylamine, pentamethyldiethyl...
Embodiment 3
[0062]Embodiment 3: a kind of medium density polyurethane rigid foam material and preparation method thereof, its preparation process is:
[0063] Polyether polyol A (hydroxyl value 40mgKOH / g) 30kg
[0064] Polyether polyol B (hydroxyl value 310mgKOH / g) 30kg
[0065] Polyether polyol C (hydroxyl value 460mgKOH / g) 40kg
[0066] water 18kg
[0067] N,N-Dimethylcyclohexylamine 0.2kg
[0068] Pentamethyldiethylenetriamine 1.2kg
[0069] N-formylmorpholine 0.8kg
[0070] Glycerol 4kg
[0071] Silicone oil (viscosity (25°C) is 850mPa·s) 6kg
[0072] Polyisocyanate (NCO mass fraction is 33%) 100kg
[0073] (1) Weigh each raw material according to the formula quantity;
[0074] (2) Put polyether polyol A, polyether polyol B, polyether polyol C, glycerol and silicone oil in a mechanically stirred tank for 20 minutes, and stir in a 1×10 3 Remove air bubbles under Pa vacuum for 20 minutes to prepare the main mixture;
[0075] (3) Mix water, N,N-dimethylcyclohexylamine, pentamet...
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