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A kind of preparation method of large-scale titanium-aluminum alloy plate material

A titanium-aluminum alloy, large-size technology, which is applied in the field of preparation of large-size titanium-aluminum alloy plates, can solve the problems of difficult preparation of large-size plates, and achieve the effect of solving difficult deformation and low cost

Active Publication Date: 2017-08-11
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the problem that it is difficult to prepare large-size plates made of TiAl intermetallic compound materials, the present invention provides a method for preparing light-weight, high-temperature-resistant large-size titanium-aluminum alloy plates

Method used

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  • A kind of preparation method of large-scale titanium-aluminum alloy plate material
  • A kind of preparation method of large-scale titanium-aluminum alloy plate material
  • A kind of preparation method of large-scale titanium-aluminum alloy plate material

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Effect test

Embodiment 1

[0037] The preparation method of large-size titanium-aluminum alloy plate, the schematic diagram of its process flow is as follows figure 1 As shown, it specifically includes the following steps:

[0038] Step 1, according to the ratio of titanium-aluminum alloy, weigh zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy, and then weigh a high-purity Al block whose mass is 104wt% times the theoretical amount; first weigh Take zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy into the high-purity graphite crucible, and then add high-purity Al blocks into the high-purity graphite crucible;

[0039] Using intermediate frequency vacuum induction furnace, the vacuum degree is 0.8*10 -1 Pa, under the condition of temperature 1620°C, smelt to obtain titanium-aluminum alloy melt. Among them, the atomic percentage of the composition of titanium aluminum alloy is: Al: 46%, Cr: 1.8%, Nb: 1.8%, the balance is Ti and unavoidable impurities; the purity...

Embodiment 2

[0053] The preparation method of large-size titanium-aluminum alloy plate, the schematic diagram of its process flow is as follows figure 1 As shown, it specifically includes the following steps:

[0054] Step 1, according to the ratio of titanium-aluminum alloy, weigh zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy, and then weigh a high-purity Al block whose mass is 105wt% times the theoretical amount; Weigh the zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy into the high-purity graphite crucible, and then add the high-purity Al block into the high-purity graphite crucible;

[0055] Using intermediate frequency vacuum induction furnace, the vacuum degree is 1.0*10 -1 Pa, under the condition of temperature 1630°C, smelt to obtain titanium-aluminum alloy melt. Among them, the atomic percentage of the composition of titanium aluminum alloy is: Al: 47%, Cr: 2.0%, Nb: 2.0%, the balance is Ti and unavoidable impurities; the purity of ...

Embodiment 3

[0069] The preparation method of large-size titanium-aluminum alloy plate, the schematic diagram of its process flow is as follows figure 1 As shown, it specifically includes the following steps:

[0070] Step 1, according to the ratio of titanium-aluminum alloy, weigh zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy, and then weigh a high-purity Al block whose mass is 106wt% times the theoretical amount; Weigh the zero-grade sponge titanium, Al-Nb master alloy and Al-Cr master alloy into the high-purity graphite crucible, and then add the high-purity Al block into the high-purity graphite crucible;

[0071] Using intermediate frequency vacuum induction furnace, the vacuum degree is 1.1*10 -1 Pa, under the condition of temperature 1650°C, smelt to obtain titanium-aluminum alloy melt. Among them, the atomic percentage of the composition of titanium aluminum alloy is: Al: 48%, Cr: 2.2%, Nb: 2.2%, the balance is Ti and unavoidable impurities; the purity of ...

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Abstract

A method for preparing large-size titanium-aluminum alloy plates, belonging to the field of intermetallic compound material plate manufacturing. Method: The titanium-aluminum alloy melt is obtained by smelting; then the melt is cast into a tundish and chute with continuous argon protection, and flows through the chute into a cavity composed of two counter-rotating crystallization rollers and side sealing plates to form In the molten pool, by controlling the superheat of the melt, the height of the liquid level in the molten pool, and the contact time between the melt and the surface of the crystallization roller, the melt is directly solidified and exported through the crystallization roller to form a large-size TiAl alloy plate. The alloy plate prepared by the method of the present invention has a thickness of 1 to 6 mm, a width of 100 to 1000 mm, and a length of 400 to 3000 mm; and the alloy plate has a fine and uniform equiaxed lamellar structure. The method of the invention is low in cost and can solve the problem of difficult deformation of intermetallic compound materials.

Description

technical field [0001] The invention belongs to the field of manufacturing intermetallic compound material plates, in particular to a preparation method of large-size titanium-aluminum alloy plates. Background technique [0002] Due to its low density, good high-temperature strength, oxidation resistance and high-temperature creep resistance, titanium-aluminum alloy is considered to be an important high-temperature structural material in the future aviation field. Its plates can be used for nozzles of high-performance engines, ultra-high-speed Aircraft thermal protection system, wings, shell and other parts. However, titanium-aluminum alloy is inherently brittle, has low room temperature plasticity and is difficult to form, and it is difficult to prepare large-size plates by conventional production processes. The processing and forming technology of titanium-aluminum alloy has become the forefront and the focus of competition in the international research on new high-temper...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C14/00C22C1/03B21B1/46B21B3/00
CPCB21B1/46B21B3/00C22C1/03C22C14/00
Inventor 刘国怀王昭东李天瑞徐莽付天亮李勇刘海涛王国栋
Owner NORTHEASTERN UNIV