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Preparation method of liquid dust suppressant capable of rapidly forming film

A dust suppressant and film-forming technology, which is applied in chemical instruments and methods, and other chemical processes, can solve the problems of ineffective dust prevention, poor dust suppression effect of solid dust suppressant, and short film-forming time of liquid dust suppression. To achieve the effect of suppressing dust flying

Inactive Publication Date: 2016-11-16
河南省九金科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem that the present invention mainly solves: for the traditional road surface dust prevention method is to use sprinkler to sprinkle water high temperature summer moisture evaporates and infiltrates quickly and cannot effectively prevent dust, solid dust suppressant dust suppression effect is poor, dust suppression period is short, liquid suppresses To solve the problem of short film-forming time of dust, a preparation method of fast film-forming liquid dust suppressant is provided. The present invention extracts sodium alginate and kelp cellulose from kelp respectively, and first grafts kelp cellulose with acrylic acid and dimethyl Diallyl ammonium chloride, the reactant of sodium alginate and polyvinyl alcohol compounded after grafting, and the dust suppressant can be obtained by adding surfactant after compounding. The dust suppressant prepared by the present invention has the properties of water absorption, penetration , bonding effect, mixed with water and sprayed on the road surface, not only can absorb water molecules in the air, quickly form a moist, non-volatile water-retaining film on the road surface, to achieve the purpose of suppressing dust, and the rapid formation of continuous complete film can be It can resist wind and rain, and can protect the road surface. The raw materials of the dust suppressant are green and easy to degrade, and there is no secondary pollution

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0019] Weigh 200g of fresh kelp, clean the surface, dry it, put it into a pulverizer, pulverize it, and sieve it to obtain 120 mesh kelp powder. Mix the kelp powder with deionized water at a solid-to-liquid ratio of 1:3, stir and mix with a mass of Fraction 20% hydrochloric acid to adjust the pH value of the mixed solution to 4.5, after adjustment, add 5% protease of kelp mass, and enzymolyze at 45°C for 1 hour, squeeze and filter with gauze after enzymolysis, separate the enzymatic solution and filter residue, and set aside; The enzymolysis solution obtained above was adjusted to pH 7.0 with a mass fraction of 5% sodium hydroxide solution, and the volume of the enzymolysis solution added after adjustment was 8% with a concentration of 8mol / L calcium chloride solution for 50 minutes of calcium precipitation, and filtered after the calcium precipitation was completed. , get the filtrate and put it in an oven and dry it at 50°C to get sodium alginate for later use; put the spare ...

example 2

[0022] Weigh 250g of fresh kelp, clean the surface, dry it, put it into a pulverizer, pulverize, and sieve to obtain 135 mesh kelp powder, mix the kelp powder with deionized water according to the solid-to-liquid ratio of 1:3, stir and mix with mass The fraction of 20% hydrochloric acid was used to adjust the pH value of the mixed solution to 5.0. After the adjustment, 6% protease of the mass of kelp was added, and it was enzymatically hydrolyzed at a temperature of 47°C for 1.5 hours. The enzymolysis solution obtained above was adjusted to a pH of 7.0 with a mass fraction of 5% sodium hydroxide solution, and the enzymolysis solution added after adjustment had a volume of 10% and a concentration of 9mol / L calcium chloride solution for 60 minutes of calcium precipitation. Filter to obtain the filtrate and put it in an oven to dry at 55°C to obtain sodium alginate for later use; put the spare filter residue at a solid-to-liquid ratio of 1:5 and a mass fraction of 5% sodium hydrox...

example 3

[0025] Weigh 300g of fresh kelp, clean the surface, dry it, put it into a pulverizer, pulverize, and sieve to obtain 150 mesh kelp powder, mix the kelp powder with deionized water according to the solid-to-liquid ratio of 1:3, stir and mix with mass The fraction of 20% hydrochloric acid was used to adjust the pH value of the mixed solution to 5.5. After adjustment, 7% protease of kelp mass was added, and enzymolysis was carried out at a temperature of 50°C for 2 hours. The enzymolysis solution obtained above was adjusted to a pH of 7.0 with a mass fraction of 5% sodium hydroxide solution, and the volume of the enzymolysis solution added after adjustment was 12% with a concentration of 10mol / L calcium chloride solution for 70 minutes of calcium precipitation, and filtered after the calcium precipitation was completed. , get the filtrate and put it in an oven and dry it at 60°C to get sodium alginate for later use; put the spare filter residue at a solid-to-liquid ratio of 1:5 an...

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Abstract

The invention discloses a preparation method of a liquid dust suppressant capable of rapidly forming a film and belongs to the field of dust suppressants. Sodium alginate and kelp cellulose are extracted from kelp respectively, kelp cellulose is grafted with acrylic acid and dimethyl diallylammonium chloride, reactants of sodium alginate and polyvinyl alcohol are compounded after grafting, a surfactant is added after compounding, and the dust suppressant can be obtained. The prepared dust suppressant has the effects of water absorption, permeation and bonding and is mixed with water and then sprayed to a pavement, water molecules in air can be absorbed, a wet and nonvolatile water retention film is formed on the pavement rapidly, the film forming time is 20-50 s, the purpose of dust flying inhibition is achieved, the rapidly formed continuous and complete film can resist wind and rainwater and can have a protection function on the pavement, raw materials of the dust suppressant are environment-friendly and easy to degrade, and no secondary pollution is caused.

Description

technical field [0001] The invention discloses a preparation method of a fast film-forming liquid dust suppressant, belonging to the field of dust suppressants. Background technique [0002] The air quality of most cities in my country is affected by three major factors: coal-burning smoke exhaust, motor vehicle exhaust, and ground dust. Coal smoke and dust pollution dominate during the heating period, and the proportion of motor vehicle exhaust and dust pollution gradually increases during the non-heating period. Dust is a pollution source that leads to poor air quality throughout the year and is difficult to control. my country has a long history of research on stationary industrial pollution sources, especially particulate matter emitted from energy combustion and production processes, and has a relatively complete set of testing, treatment, and management methods. However, there is no systematic research on the dust pollution and control of open dust sources, such as co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F251/02C08F285/00C08F220/06C08F222/38C08F226/04C08B37/04C08B1/00C08L51/00C08L29/04C08L5/04C09K3/22
CPCC08B1/00C08B37/0003C08B37/0084C08F251/02C08F285/00C08L51/00C08L2205/03C09K3/22C08F220/06C08F222/385C08F226/04C08L29/04C08L5/04
Inventor 丁玉琴王统军
Owner 河南省九金科技有限公司
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