Preparation method of organic silicon material for LED encapsulation
An LED packaging and organic silicon technology, which is applied in the field of preparation of organic silicon materials for LED packaging, can solve the problems of low light extraction efficiency of chips, achieve excellent resistance to ultraviolet aging and thermal aging, high refractive index, and improve light transmittance. and the effect of hardness
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[0011] Component A is synthesized by the following method: Vinyl silicon high polymer and polyphenylene phenylene ether oxide silicone oil containing olefin group are put into the reactor and stirred for 15 minutes, then a certain amount of distilled water is added dropwise, refluxed for 4 hours, and alcohol water is removed. Wash with deionized water until neutral, add KOH, wash with water to remove alkali, decolorize activated carbon, and finally remove low boilers in vacuum, add solid catalyst, mix well to obtain component A. The vinyl silicon polymer used includes vinyl silicone resin and vinyl-containing polysiloxane; the ratio of the number of Si-C to Si-O in the main chain structure of polyphenylene phenylene ether silicone oil containing olefin group 1:1;
[0012] Component B is synthesized by the following method: Put olefin-based hydrogen-based polyphenylene phenylene ether and vinyl hydrogen-based silicone resin into the reactor for stirring, slowly add a certain am...
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