A waste flow type rainwater deep circulation purification device and its purification process
A recycling purification and rainwater technology, applied in runoff/rainwater treatment, combined device, filtration treatment, etc., can solve problems affecting the normal operation of sewage treatment plants, difficult renovation work, high treatment costs, etc., to achieve novel and reasonable structure, gas-liquid High isolation ability and high removal efficiency
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Embodiment 1
[0053] Manufacture the gas-liquid separation separator 2-9 of the present invention according to the following steps, and by weight fraction:
[0054] Step 1: Add 569 parts of ultrapure water with a conductivity of 0.69μS / cm into the reaction kettle, start the stirrer in the reaction kettle at a speed of 109rpm, start the heating pump, and raise the temperature in the reaction kettle to 79°C; add in sequence 79 parts of N-diisopropyl-2-chloroethylamine hydrochloride, bis[3-hydroxy-4-[(2-hydroxy-1-naphthyl)azo]-1-naphthalenesulfonate]chromic acid 99 parts of diethanolamine sodium salt, 169 parts of N,N'-diphenyl-N,N'-di(1-naphthyl)-1,5-naphthalenediamine, stirred until completely dissolved, and adjusted the pH value to 6.9, Adjust the speed of the agitator to 169rpm, the temperature is 109°C, and the esterification reaction takes 29 hours;
[0055] Step 2: Take 99 parts of 3,7-bis(1,1-dimethylethyl)-1-naphthalenesulfonate sodium and 89 parts of bis(β-chloroethyl)amine hydrochlor...
Embodiment 2
[0060] Manufacture the gas-liquid separation separator 2-9 of the present invention according to the following steps, and by weight fraction:
[0061] Step 1: Add 1519 parts of ultrapure water with a conductivity of 0.89μS / cm into the reactor, start the stirrer in the reactor at a speed of 269rpm, start the heating pump, and raise the temperature in the reactor to 99°C; add in order 169 parts of N-diisopropyl-2-chloroethylamine hydrochloride, bis[3-hydroxy-4-[(2-hydroxy-1-naphthyl)azo]-1-naphthalenesulfonato]chromic acid 169 parts of diethanolamine sodium salt, 359 parts of N,N'-diphenyl-N,N'-bis(1-naphthyl)-1,5-naphthalenediamine, stirred until completely dissolved, and adjusted the pH value to 8.9, Adjust the speed of the agitator to 269rpm, the temperature is 179°C, and the esterification reaction is 39 hours;
[0062] Step 2: Take 209 parts of 3,7-bis(1,1-dimethylethyl)-1-naphthalenesulfonate sodium and 169 parts of bis(β-chloroethyl)amine hydrochloride and grind them int...
Embodiment 3
[0067] Manufacture the gas-liquid separation separator 2-9 of the present invention according to the following steps, and by weight fraction:
[0068] Step 1: Add 919 parts of ultrapure water with a conductivity of 0.79μS / cm into the reactor, start the stirrer in the reactor at a speed of 169rpm, start the heat pump, and raise the temperature in the reactor to 89°C; add in sequence 119 parts of N-diisopropyl-2-chloroethylamine hydrochloride, bis[3-hydroxy-4-[(2-hydroxy-1-naphthyl)azo]-1-naphthalenesulfonate]chromic acid 149 parts of diethanolamine sodium salt, 259 parts of N,N'-diphenyl-N,N'-di(1-naphthyl)-1,5-naphthalenediamine, stirred until completely dissolved, and adjusted the pH value to 7.9, Adjust the speed of the agitator to 189rpm, the temperature is 129°C, and the esterification reaction is 32 hours;
[0069] Step 2: Take 159 parts of 3,7-bis(1,1-dimethylethyl)-1-naphthalenesulfonate sodium and 129 parts of bis(β-chloroethyl)amine hydrochloride and grind them into ...
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