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Novel portable electrostatic spinning device

An electrospinning, portable technology, used in textiles and papermaking, filament/thread forming, fiber processing, etc., can solve the problems of accurate deposition of nanofiber materials, unsolved problems, inability to carry around, etc., to achieve fiber directional deposition, The effect of expanding the scope of use and being convenient to use

Inactive Publication Date: 2017-04-05
青岛中科凯尔科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, in 2012, Long Yunze et al. reported for the first time "a portable handheld electrospinning device" (201210229010.3). This device uses a square battery to provide power for the high-voltage DC inverter, which overcomes the defect that the existing equipment cannot be carried around, making Portability is really possible, but the structure of the device is relatively simple, and there are still many deficiencies in the directional deposition of nanofibers; the Chinese patent "An Electric Field Spray Gun for Rapidly Obtaining Nanomaterials" (201320598875.7) also uses a miniature high-voltage pack for power supply, which is free from However, the problem of accurate deposition of nanofibrous materials is still unsolved.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] 1. If Figures 1 to 4 As shown, a novel portable electrospinning device includes a host 1 and a hand-held spray gun 6. The host 1 includes a host shell 11, and a power supply, a gas generating mechanism and a high-voltage power supply mechanism are arranged in the host shell 11. The hand-held spray gun 6 Comprising a gun body shell 14, a spinneret 19 and a liquid supply mechanism that provides spinning precursor liquid for the spinneret 19, the gun body shell 14 is provided with an air inlet 21 and an air outlet 22, and the air inlet 21 The air guide pipe connected to the gas generating mechanism inflates the gun body shell 14, and the gas charged into the gun body shell 14 is discharged from the air outlet 22 to form an air flow. The spinneret 19 stretches from the air outlet 22 to the gun body shell 14, and the spray The injection port of the wire head 19 coincides with the central axis of the air outlet 22; the power supply is connected to the high-voltage power supp...

Embodiment 2

[0032] Weigh 1.3 grams of polyvinylpyrrolidone powder (PVP, molecular weight 1.3 million), dissolve it in 8.7 grams of absolute ethanol, stir magnetically at room temperature for 2 hours until completely dissolved, and obtain a uniform PVP spinning precursor solution with a solute mass fraction of 13% .

Embodiment 3

[0035] Weigh 2 grams of polycaprolactone (PCL, molecular weight 45,000), dissolve them all in 8 grams of acetone, and magnetically stir at room temperature for 2 hours until completely dissolved, and obtain a uniform PCL spinning precursor solution with a solute mass fraction of 20%.

[0036] Apply the device of Example 1 to prepare PVP micro-nano fibers, first add the prepared PCL spinning precursor solution into the syringe barrel, open the liquid replacement cover 7, and fix the syringe barrel in the slot inside the hand-held gun body 6 Inside, the front end of the syringe barrel is connected to the spinneret 19, connected to the mains power supply through the socket, and the propulsion speed adjustment knob 4 is adjusted to set the spinning liquid propulsion rate to 100 μL / min, and the air volume control knob 3 is adjusted to set the air volume to 6th gear, and the rotation voltage Adjust the knob 5 to set the spinning voltage to 8 kV, and the spinning height is set to 10 c...

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Abstract

The invention discloses a novel portable electrostatic spinning device which comprises a host and a handheld spray gun. The host comprises a host shell, a power supply, and an air generation mechanism and a high-voltage power supply mechanism are arranged in the host shell; the handheld spray gun comprises a gun body shell, a spinning nozzle and a liquid supplying mechanism used for supplying spinning precursor liquid to the spinning nozzle, the gun body shell is provided with an air inlet and an air outlet, the air inlet is connected with an air guide pipe of the air generation mechanism, the spinning nozzle stretches out of the gun body shell from the air outlet, and the spraying end opening of the spinning nozzle coincides with the central axis of the air outlet; the power supply is electrically connected with the high-voltage power supply mechanism, the air generation mechanism and the liquid supplying mechanism, and the positive electrode of the voltage output end of the high-voltage power supply mechanism is connected with the spinning nozzle through a wire. According to the device, the spinning part and the device host are separated, use is more convenient, spinning parameters are precisely controlled and adjusted by adopting micro equipment, the application range is wide, and orientated deposition of fibers can be achieved.

Description

technical field [0001] The invention relates to an electrospinning device, in particular to a novel hand-held electrospinning device which is portable, directional deposition, and in-situ spinning. Background technique [0002] Electrospinning is one of the simplest and most efficient methods for preparing one-dimensional micro-nano fibers. Compared with traditional nanomaterials preparation technology, it has the advantages of simple processing equipment, wide source of raw materials, low spinning cost, and large-scale preparation. In recent years, To receive extensive research reports at home and abroad. Micro-nano fibers processed by electrospinning technology have excellent characteristics such as high specific surface area, large length / diameter ratio, and unique physical and chemical properties. It shows great application potential in other fields. The principle of the electrospinning method is very simple. It is briefly described as follows: under the action of a hi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D5/00
CPCD01D5/0069D01D5/0092
Inventor 于淼龙云泽
Owner 青岛中科凯尔科技有限公司
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