Cultural relic fumigation method
A technology of cultural relics and fumigants, applied in the field of cultural relics fumigation, can solve the problems of cumbersome operation, danger, fluoride human bone poisoning, etc., and achieve the effect of simple operation, low cost and low pollution
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Embodiment 1
[0022] Embodiment 1: the preparation of fumigant
[0023] 1. The compound of methyl methyl thiosulfinate and ethyl ethyl thiosulfinate:
[0024] Stir and mix methyl methyl thiosulfinate and ethyl ethyl thiosulfinate at room temperature according to the volume ratio of 1:3; abbreviated as fumigant A; determine the oral LD of mice 50 >500mg / Kg, belongs to low toxicity.
[0025] 2. Compound of ethyl ethyl thiosulfinate and methyl methyl thiosulfinate:
[0026] Stir and mix ethyl ethyl thiosulfinate and methyl methyl thiosulfinate evenly at room temperature according to the volume ratio of 1:2; abbreviated as fumigant B; determine the oral LD of mice 50 >500mg / Kg, belongs to low toxicity.
[0027] 3. Compound of ethyl ethyl thiosulfinate and ethyl ethyl thiosulfinate:
[0028] Stir and mix ethyl ethyl thiosulfinate and ethyl ethyl thiosulfinate at room temperature according to the volume ratio of 1:1; abbreviated as fumigant C; determine the oral LD of mice 50 >500mg / Kg...
Embodiment 2
[0041] Embodiment 2: cultural relics fumigation experiment
[0042] Cultural relic material: paper
[0043] Diseases: Aspergillus and Penicillium, etc.
[0044] Fumigant: Fumigant A
[0045] Fumigation method:
[0046] Put the fumigant and cultural relic samples into the fumigation box, close the fumigation box, control the temperature in the fumigation box to 25°C, and after 36 hours of fumigation, depressurize and pump for 2 hours, open the fumigation box, and remove the cultural relic samples;
[0047] It is known from the microscope inspection that no mold has grown on the cultural relic samples after the above-mentioned fumigation treatment;
[0048] And it is known from the detection and analysis of gas chromatography and mass spectrometry (GC-Ms): there is no fumigant residue on the cultural relic samples after the above-mentioned fumigation treatment.
[0049] Place the samples of cultural relics after the fumigation treatment in this embodiment in the collection r...
Embodiment 3-1
[0052] Example 3-1: Cultural relics fumigation experiment
[0053] Cultural relic material: silk material
[0054] Diseases: Aspergillus and Penicillium, etc.
[0055] Fumigant: Fumigant C
[0056] Put the fumigant and cultural relic samples into the fumigation box, close the fumigation box, control the temperature in the fumigation box to 25°C, and after 24 hours of fumigation, depressurize and pump for 2 hours, open the fumigation box, and remove the cultural relic samples;
[0057] It is known from the microscope inspection that no mold has grown on the cultural relic samples after the above-mentioned fumigation treatment;
[0058] And by the detection and analysis of gas chromatography and mass spectrometry (GC-Ms), it is known that there is no fumigant residue on the cultural relic samples after the above-mentioned fumigation treatment;
[0059] Place the samples of cultural relics after the fumigation treatment in this embodiment in the collection room of the cultural...
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