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Method for preparing sodium ion battery electrode carbon material through peanut shell

A sodium-ion battery and peanut shell technology, applied in battery electrodes, secondary batteries, carbon preparation/purification, etc., can solve problems such as resource waste, environmental pollution, etc., achieve low cost, increase battery capacity, and enhance battery cycle performance Effect

Active Publication Date: 2017-05-31
LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For now, except that less than 20% of peanut shells are used as feed additives, more than 80% of peanut shells are thrown away or burned, which will undoubtedly cause serious waste of resources and environmental pollution.

Method used

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  • Method for preparing sodium ion battery electrode carbon material through peanut shell
  • Method for preparing sodium ion battery electrode carbon material through peanut shell
  • Method for preparing sodium ion battery electrode carbon material through peanut shell

Examples

Experimental program
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Effect test

Embodiment 1

[0033] A kind of method utilizing peanut shell to prepare sodium ion battery electrode carbon material, comprises the following steps:

[0034] Step 1. After washing the peanut shells with ethanol and deionized water respectively, place them in a blast drying oven for 24 hours at 60°C;

[0035] Step 2. Place the dried peanut shells in a porcelain boat, use a high-temperature tube furnace to heat up to 800°C at a rate of 30°C / min under the protection of an inert atmosphere, and then heat-preserve and carbonize for 4 hours;

[0036] Step 3, after grinding the carbonized peanut shells into powder, sieve them through a 100-mesh sieve to obtain a peanut shell-derived carbon powder with uniform particles, which is the electrode carbon material for sodium ion batteries; image 3 It is the peanut shell derived carbon XRD pattern prepared in Example 1. Where the abscissa is the angle and the ordinate is the relative intensity. Depend on image 3It can be seen that there are obvious ...

Embodiment 2

[0038] A kind of method utilizing peanut shell to prepare sodium ion battery electrode carbon material, comprises the following steps:

[0039] Step 1. After washing the peanut shells with ethanol and deionized water respectively, place them in a blast drying oven for 24 hours at 60°C;

[0040] Step 2. Place the dried peanut shells in a porcelain boat, use a high-temperature tube furnace to heat up to 750°C at a rate of 15°C / min under the protection of an inert atmosphere, and then heat-preserve and carbonize for 12 hours;

[0041] Step 3: Grind the carbonized peanut shells into powder, and then sieve through a 100-mesh sieve to obtain a peanut shell-derived carbon powder with uniform particles, which is the electrode carbon material for sodium ion batteries.

Embodiment 3

[0043] A kind of method utilizing peanut shell to prepare sodium ion battery electrode carbon material, comprises the following steps:

[0044] Step 1. After washing the peanut shells with ethanol and deionized water respectively, place them in a blast drying oven for 24 hours at 60°C;

[0045] Step 2. Place the dried peanut shells in a porcelain boat, use a high-temperature tube furnace to heat up to 850°C at a rate of 20°C / min under the protection of an inert atmosphere, and then heat-preserve and carbonize for 3 hours;

[0046] Step 3: Grind the carbonized peanut shells into powder, and then sieve through a 100-mesh sieve to obtain a peanut shell-derived carbon powder with uniform particles, which is the electrode carbon material for sodium ion batteries.

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PUM

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Abstract

The invention discloses a method for preparing sodium ion battery electrode carbon material through peanut shell. The method comprises the following steps: the first step of cleaning the peanut shell through ethyl alcohol and deionized water respectively and drying; the second step of putting the dried peanut shell into a high-temperature furnace to be carbonized to obtain peanut shell derivative carbon; the third step of grinding the peanut shell derivative carbon into powder and sieving through a 10 to 100 meshes screen to obtain the peanut shell derivative carbon powder with even particles, namely the sodium ion battery electrode carbon material. The preparation method disclosed by the invention has the characteristics of being simple and easy to operate, strong in repeatability, low in cost and free of environmental pollution. When the peanut shell derivative carbon material prepared through the method is utilized as a negative electrode material of a room-temperature sodium ion battery, self specific surface area of the material is effectively enlarged, battery capacity is improved, and battery circulation performance is enhanced.

Description

technical field [0001] The invention belongs to the field of battery electrode materials, and relates to a sodium ion battery electrode carbon material, in particular to a method for preparing the sodium ion battery electrode carbon material by using peanut shells. Background technique [0002] Although the lithium-ion battery technology is relatively mature, as its scope becomes wider and wider, especially in the large-scale application in the field of electric vehicles, we have to start to consider the sustainable development of lithium-ion batteries. According to the current development speed of electric vehicles, global lithium resources will not be able to effectively meet the huge demand for power lithium-ion batteries, which will further increase the price of lithium-related materials that were originally scarce, and will continue to increase battery costs, hindering the development of electric vehicles. Represented by the development of new energy industries. Theref...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/05H01M4/587H01M10/0525
CPCC01P2002/72C01P2004/03C01P2006/40H01M4/587H01M10/0525Y02E60/10Y02P20/54
Inventor 米睿付志兵王朝阳袁磊刘淼钟铭龙杨曦赵海波杨帆
Owner LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS