System and method for recovering alcohol ketone by using thermal energy of wastewater

A heat recovery and waste water technology, which is applied in the field of cyclohexanone refining, can solve the problems of waste of resources such as alcohol and ketone, waste of energy, increase of waste water treatment cost, etc., and achieve the effect of saving the use of external energy and increasing the feed temperature

Inactive Publication Date: 2017-05-31
聊城鲁西甲酸化工有限公司
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Problems solved by technology

[0004] However, the existing alcohol and ketone recovery unit is difficult to recover the alcohol and ketone and other organic substances in the process condensate more thoroughly, and the wastewater discharged from the waste water stripping tower still contains organic substances such as alcohol and ketone, which increases the cost of wastewater treatment. And caused a waste of resources such as alcohol and ketone
At the same time, the temperature of the wastewater discharged from the waste water stripping tower is relatively high, and it needs to be cooled to 50-55°C before it can be discharged into the sewage treatment system. The cooling heat of the wastewater requires a large amount of cooling circulating water, which also causes a waste of energy.

Method used

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  • System and method for recovering alcohol ketone by using thermal energy of wastewater

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Embodiment Construction

[0037] The solution of the present invention will be further described below in combination with specific embodiments and accompanying drawings.

[0038] Such as figure 1 Shown, a kind of system that utilizes waste water heat energy to reclaim ketone alcohol, the tower top inlet of extraction tower 3 is communicated with the water inlet pipeline of the process condensed water that contains ketone alcohol, the tower top outlet of waste water stripping tower 6 is fed with alkane distillation tower The heat medium passage inlet of preheater 14 is connected, and the heat medium passage outlet of alkane distillation column feed preheater 14 is communicated with the heat medium passage entrance of waste water condenser 8; The cold medium inlet of alkane distillation tower feed preheater 14 It is communicated with the tower top outlet of extraction tower 3, and the cold medium outlet of alkane distillation tower feed preheater 14 is communicated with the inlet of alkane distillation ...

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Abstract

The invention discloses a system and a method for recovering alcohol ketone by using thermal energy of waste water. The column top inlet of an extraction column communicates with a water inlet pipeline of process condensed water containing ketone alcohol; the column top outlet of the extraction column communicates with the middle inlet of an alkyl distillation column; the material outlet of the alkyl distillation column communicates with the column reactor inlet of the extraction column; the column top outlet of a wastewater stripping column communicates with the thermal medium inlet of a wastewater condenser; the thermal medium outlet of the wastewater condenser communicates with an alcohol ketone collection device; the column reactor outlet of the wastewater stripping column communicates with the thermal medium inlet of a wastewater heat exchanger; the thermal medium outlet of the wastewater heat exchanger communicates with the thermal medium inlet of a wastewater cooler; the cold medium inlet of the wastewater heat exchanger communicates with the column kettle outlet of the extraction column; the cold medium outlet of the wastewater heat exchanger communicates with the column top inlet of the wastewater stripping column; the thermal medium outlet of the wastewater cooler communicates with a wastewater conveying pipeline.

Description

technical field [0001] The invention belongs to the technical field of cyclohexanone refining, and in particular relates to a system and method for recovering alcohol and ketone by using waste water heat energy. [0002] technical background [0003] The process condensate produced in the refining process of cyclohexanone contains organic substances such as alcohol and ketone. The alcohol and ketone recovery unit uses the extractant cyclohexane to extract and recover the organic substances such as alcohol and ketone in the water seal tank of the refining unit. The cyclohexane is recycled, and the After extraction, the process condensate containing a small amount of alcohol and ketone organic matter is stripped by the waste water stripping tower, and the organic matter is recovered to the system, and the qualified high-temperature waste water is cooled to a qualified temperature and sent out to the device for harmless treatment. [0004] However, the existing alcohol and keton...

Claims

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Application Information

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IPC IPC(8): C02F9/10C02F103/36
CPCC02F1/26C02F1/10C02F2103/36
Inventor 张庆喜刘福青朱士超魏传奇李怀增孙立平张鑫王士波谢培建郭平袁东立李海滨王彤
Owner 聊城鲁西甲酸化工有限公司
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