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Silicon-dioxide aerogel thermal-insulation material and preparation method thereof

A technology of silica and thermal insulation materials, applied in chemical instruments and methods, inorganic chemistry, ceramic products, etc., can solve the problems of cumbersome and complicated preparation process, lack of popularization, low strength of airgel and thermal insulation materials, etc., and achieve Improve the thermal insulation performance, enhance the overall thermal insulation performance and toughness, and enhance the effect of thermal insulation

Inactive Publication Date: 2017-06-13
XINHUASHENG ENERGY SAVING TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The application of aerogels to thermal insulation materials has gradually attracted people's attention, but the strength of airgel and thermal insulation materials in the prior art is not high, and the preparation process is cumbersome and complicated, so it has not been well promoted

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Embodiment 1: A kind of silica insulation material of this embodiment comprises the following components by weight: 20 parts of silica airgel sol, 15 parts of water, 10 parts of glass fiber, 5 parts of silicon nanotube and oxidation 0.6 parts of aluminum powder.

[0026] The silica airgel sol is made of the following raw materials in parts by weight: 35 parts of ethyl orthosilicate, 40 parts of absolute ethanol, 1.2 parts of ammonia water, 3 parts of trimethylchlorosilane, 6 parts of n-hexane, six parts 2 parts of methyldisilazane, 3 parts of deionized water and 0.6 parts of oxalic acid.

[0027] The preparation process of silica airgel is as follows: prepare the solution with tetraethyl orthosilicate, absolute ethanol and deionized water according to the molar ratio of 1:14:6.23, stir evenly, add 0.75mol / L oxalic acid solution, adjust the pH to 4; hydrolyze the obtained solution for 15 hours, add 0.5mol / L ammonia solution, adjust the pH value of the hydrolyzed solutio...

Embodiment 2

[0034] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the heat treatment temperature of the glass fiber is 450°C;

Embodiment 3

[0035] Embodiment 3: The difference between this embodiment and Embodiment 1 is that the heat treatment temperature of the glass fiber is 500°C;

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Abstract

The invention provides a silicon-dioxide aerogel thermal-insulation material and a preparation method thereof, belongs to the technical field of thermal-insulation materials, and particularly relates to the silicon-dioxide aerogel thermal-insulation material and the preparation method thereof. The invention aims at solving the problems that in the prior art, aerogel and thermal-insulation materials are low in intensity, tedious and complicated in preparation process, and not well popularized. The silicon-dioxide aerogel thermal-insulation material comprises, by weight, 20-40 parts of silicon-dioxide aerogel sol, 15-35 parts of water, 10-20 parts of glass fiber, 5-8 parts of silicon nanotube and 0.5-2 parts of active agent. The prepared silicon-dioxide aerogel thermal-insulation material has better stability, and long fibers are fused with the nanotubes and aerogel materials. The heat conductivity coefficient reaches 0.011W / (m<2>*K), the thermal-insulation performance of the thermal-insulation material is greatly improved, and the thermal-insulation effect is improved.

Description

technical field [0001] A thermal insulation material and a preparation method thereof belong to the technical field of thermal insulation material preparation, and mainly relate to a silica airgel thermal insulation material and a preparation method thereof. Background technique [0002] Airgel is a solid form of matter, one of the smallest solids in the world. The density is 3 kilograms per cubic meter. Because of the extremely low density, the lightest aerogel at present is only 0.16 mg per cubic centimeter, which is slightly lower than air density, so it is also called "frozen smoke" or "blue smoke". Because the particles inside are very small (nanoscale), visible light is less scattered when it passes through it (Rayleigh scattering), just like sunlight passing through air. Therefore, it also looks blue like the sky (if nothing else is in it), and looks a little reddish when held up to the light. (The sky is blue, while the evening sky is red). Because generally more...

Claims

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Application Information

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IPC IPC(8): C04B28/24C01B33/141C04B38/00
CPCC04B28/24C01B33/141C04B38/0045C04B2201/32C04B14/42C04B14/02C04B22/06
Inventor 朱晓辉
Owner XINHUASHENG ENERGY SAVING TECH CO LTD
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