Silicon-dioxide aerogel thermal-insulation material and preparation method thereof
A technology of silica and thermal insulation materials, applied in chemical instruments and methods, inorganic chemistry, ceramic products, etc., can solve the problems of cumbersome and complicated preparation process, lack of popularization, low strength of airgel and thermal insulation materials, etc., and achieve Improve the thermal insulation performance, enhance the overall thermal insulation performance and toughness, and enhance the effect of thermal insulation
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Embodiment 1
[0025] Embodiment 1: A kind of silica insulation material of this embodiment comprises the following components by weight: 20 parts of silica airgel sol, 15 parts of water, 10 parts of glass fiber, 5 parts of silicon nanotube and oxidation 0.6 parts of aluminum powder.
[0026] The silica airgel sol is made of the following raw materials in parts by weight: 35 parts of ethyl orthosilicate, 40 parts of absolute ethanol, 1.2 parts of ammonia water, 3 parts of trimethylchlorosilane, 6 parts of n-hexane, six parts 2 parts of methyldisilazane, 3 parts of deionized water and 0.6 parts of oxalic acid.
[0027] The preparation process of silica airgel is as follows: prepare the solution with tetraethyl orthosilicate, absolute ethanol and deionized water according to the molar ratio of 1:14:6.23, stir evenly, add 0.75mol / L oxalic acid solution, adjust the pH to 4; hydrolyze the obtained solution for 15 hours, add 0.5mol / L ammonia solution, adjust the pH value of the hydrolyzed solutio...
Embodiment 2
[0034] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the heat treatment temperature of the glass fiber is 450°C;
Embodiment 3
[0035] Embodiment 3: The difference between this embodiment and Embodiment 1 is that the heat treatment temperature of the glass fiber is 500°C;
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