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Triglycidyl isocyanurate having undergone physical coating and preparation method thereof

A technology of tris, glycidyl isocyanurate, applied in polyester coatings, coatings, etc., can solve the problems of undiscovered patent publications, achieve elimination of toxicity and irritation to the human body, improve anti-pollution, improve Easy to absorb moisture and not easy to store

Inactive Publication Date: 2017-09-05
阜阳市诗雅涤新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Through the search, no patent publications related to the patent application of the present invention have been found

Method used

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  • Triglycidyl isocyanurate having undergone physical coating and preparation method thereof
  • Triglycidyl isocyanurate having undergone physical coating and preparation method thereof
  • Triglycidyl isocyanurate having undergone physical coating and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A kind of triglycidyl isocyanurate (TGIC) through physical coating, its raw material composition component and its weight are as follows:

[0024] 10 parts of glycidyl acrylic resin;

[0025] TGIC 90 copies;

[0026] The triglycidyl isocyanurate is uncoated triglycidyl isocyanurate, and the epoxy value is greater than or equal to 0.92eq / 100g.

[0027] The above-mentioned preparation method of triglycidyl isocyanurate through physical coating, the steps are as follows:

[0028] Add the two materials with a certain mass ratio to the high-speed mixer, crush and mix at high speed for 3-20min, and then extrude through the twin-screw extruder. The temperature in the first zone is 80-90℃, and the temperature in the second zone is 100-120℃ ℃, melting, kneading, extruding, cooling, and tableting to become a flaky milky white solid, that is, physically coated triglycidyl isocyanurate;

[0029] The residence time of the two materials in the molten state in the screw of the twin...

Embodiment 2

[0032] A kind of triglycidyl isocyanurate (TGIC) through physical coating, its raw material composition component and its weight are as follows:

[0033] 20 parts of carboxyl acrylic resin;

[0034] TGIC 80 copies.

[0035] The above-mentioned preparation method of triglycidyl isocyanurate through physical coating, the steps are as follows:

[0036] Add the two materials with a certain mass ratio to the high-speed mixer, crush and mix at high speed for 3-20min, and then extrude through the twin-screw extruder. The temperature in the first zone is 80-90℃, and the temperature in the second zone is 100-120℃ ℃, melting, kneading, extruding, cooling, and tableting to become a flaky milky white solid, that is, physically coated triglycidyl isocyanurate;

[0037] The residence time of the two materials in the molten state in the screw of the twin-screw extruder is 5-30 seconds, and the longest is no more than 40 seconds.

[0038] Method of use: The obtained coated TGICB and 97:3 t...

Embodiment 3

[0040] A kind of triglycidyl isocyanurate (TGIC) through physical coating, its raw material composition component and its weight are as follows:

[0041] 10 parts of hydroxyacrylic resin;

[0042] TGIC 90 copies;

[0043] The triglycidyl isocyanurate is uncoated triglycidyl isocyanurate, and the epoxy value is greater than or equal to 0.92eq / 100g.

[0044] The above-mentioned preparation method of triglycidyl isocyanurate through physical coating, the steps are as follows:

[0045] Add the two materials with a certain mass ratio to the high-speed mixer, crush and mix at high speed for 3-20min, and then extrude through the twin-screw extruder. The temperature in the first zone is 80-90℃, and the temperature in the second zone is 100-120℃ ℃, melting, kneading, extruding, cooling, and tableting to become a flaky milky white solid, that is, physically coated triglycidyl isocyanurate;

[0046] The residence time of the two materials in the molten state in the screw of the twin-s...

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Abstract

The invention relates to triglycidyl isocyanurate having undergone physical coating. The triglycidyl isocyanurate having undergone physical coating comprises the following raw materials by weight: 10 to 30 parts of acrylic resin and 70 to 90 parts of triglycidyl isocyanurate. The coated triglycidyl isocyanurate overcomes the problems of toxicity and irritation to the human body of uncoated triglycidyl isocyanurate and problems in storage caused by moisture absorption performance of uncoated triglycidyl isocyanurate; and the physically coated triglycidyl isocyanurate reduces or eliminates toxicity and irritation of triglycidyl isocyanurate to the human body and improves storage performance under the condition of no deterioration of the performance of triglycidyl isocyanurate, or even under the condition of improvement of decorative performance, weatherability and mechanical properties of a film formed by the physically coated triglycidyl isocyanurate.

Description

technical field [0001] The invention belongs to the technical field of curing crosslinking agents, and relates to a curing agent, in particular to a physically coated triglycidyl isocyanurate (TGIC) and a preparation method thereof. Background technique [0002] Powder coating and coating technology is a new technology and new process developed in the middle of the 20th century. Due to its characteristics of no need to discharge organic matter into the air, reduce environmental pollution, simple process, easy industrial automation, and excellent coating performance, it has attracted worldwide attention. The attention of the coating industry in various countries. The powder coating itself is a new type of solvent-free, 100% solid powder coating, but its saturated polyester resin / TGIC type outdoor system powder coating has certain toxicity to human skin and respiratory tract because of its TGIC. Its use has been restricted in foreign countries, but domestically, it is still th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D7/12C09D167/00C08K9/10C08K5/3477
CPCC08K5/3477C08K9/10C09D167/00
Inventor 陈超王焱王浩吕朝忍冯士海闻欣王鹏飞
Owner 阜阳市诗雅涤新材料科技有限公司