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Manufacture method for nanocrystallization of natural phytoncide molecule without agglomeration

A production method and natural fen technology, which is applied in the field of plant phytondine, can solve the problems of phytondine's nano-molecular distance becoming smaller, phytoncine essential oil with many impurities, and uneven distribution, so as to enhance the bactericidal ability and purify the air Effect

Inactive Publication Date: 2017-09-26
野艳玲
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most of the phytondo products on the market are based on the unilateral phytondo essential oil distilled under high temperature and high pressure as the main raw material, and then a certain proportion of base oil is added to make the compound phytondo essential oil (the unilateral phytondo essential oil has harmful effects on human skin. It is highly irritating and cannot be directly used on the surface of the human body), the unilateral phytondo essential oil produced by this high-temperature and high-pressure distillation method will make phytondo essential oil have too many impurities, and the high-temperature and high-pressure distillation method will make phytondo essential oil The distance between fine nano-molecules becomes smaller, which will cause molecular aggregation and uneven distribution. This will lead to the molecular aggregation of phytoncine, which will greatly reduce the specific surface area of ​​the reaction and reduce the bactericidal effect

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] 1). Filter the impurities of phytondo essential oil: Pour 1000ml of phytondo essential oil into a supramolecular membrane filter to filter impurities. After filtering, pure phytondo essential oil can be obtained.

[0020] 2). Make phytondo essential oil from unilateral formula into compound phytondo essential oil: take 800ml phytondo essential oil unilaterally + 200ml tea tree essential oil, mix and pour into a blender, stir at 500 rpm, and continue heating to 65 degrees Celsius. Stir The time is 5 minutes, and you can get 1000ml compound phytondo essential oil.

[0021] 3). To enhance the volatility of compound phytondo and prevent freezing: Take 1000ml of compound phytondo essential oil and pour it into a blender, then pour 3000ml of ethanol, 6000ml of deionized water, and stir at 500 rpm for 8 minutes.

[0022] Pour 10,000ml of compound phytoncine aqueous solution into the blender, then add 0.5% silicate, stir for 3 minutes, pour it into an ultrasonic oscillator and ...

Embodiment 2

[0024] 1). Filter the impurities of phytondo essential oil: Pour 1000ml of phytondo essential oil into a supramolecular membrane filter to filter impurities. After filtering, pure phytondo essential oil can be obtained.

[0025] 2). Make phytondo essential oil from unilateral formula into compound phytondo essential oil: take 800ml phytondo essential oil unilaterally + 200ml tea tree essential oil, mix and pour it into a blender, stir at 500 rpm, and continue heating to 68 degrees Celsius. Stir The time is 7 minutes, and you can get 1000ml compound phytondo essential oil.

[0026] 3). To improve the volatility of compound phytondo and prevent freezing: Take 1000ml of compound phytondo essential oil and pour it into a blender, then pour 3000ml of ethanol, 6000ml of deionized water, and stir at 500 rpm for 9 minutes.

[0027] Pour 10,000ml of compound phytoncine aqueous solution into the blender, then add 0.7% silicate, stir for 4 minutes, pour it into an ultrasonic oscillator a...

Embodiment 3

[0029] 1). Filter the impurities of phytondo essential oil: Pour 1000ml of phytondo essential oil into a supramolecular membrane filter to filter impurities. After filtering, pure phytondo essential oil can be obtained.

[0030] 2). Make phytondo essential oil from unilateral formula into compound phytondo essential oil: take 800ml phytondo essential oil unilaterally + 200ml tea tree essential oil, mix and pour it into a blender, stir at 500 rpm, and continue heating to 68 degrees Celsius. Stir The time is 8 minutes, and you can get 1000ml compound phytondo essential oil.

[0031] 3). To improve the volatility of compound phytondo and prevent freezing: Take 1000ml of compound phytondo essential oil and pour it into a blender, then pour 3000ml of ethanol, 6000ml of deionized water, and stir at 500 rpm for 9 minutes.

[0032] Pour 10,000ml of compound phytoncine aqueous solution into the blender, then add 1% silicate, stir for 5 minutes, then pour it into an ultrasonic oscillato...

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PUM

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Abstract

The invention discloses a manufacture method for nanocrystallization of natural phytoncide molecule without agglomeration, and relates to a manufacture method of plant essential oil. Compound phytoncide essential oil is conducted according to the following step sequence: firstly, pouring 1000ml of pure phytoncide essential oil into a supermolecular film filter, so as to filter impurities; secondly, mixing and pouring 800ml of pure phytoncide essential oil and 200ml of tea tree essential oil into a blender, stirring at 500 revolutions per minute, continuously heating the pure phytoncide essential oil and the tea tree essential oil to 65 to 70 DEG C, and ensuring that the stirring time is 5 to 8 minutes, so as to obtain 1000ml of compound phytoncide essential oil; thirdly, pouring the 1000ml of compound phytoncide essential oil into the blender, then pouring 3000ml of alcohol and 6000ml of deionized water into the blending, and stirring for 8 to 10 minutes at 500 revolutions per minute. A manufacture method for preventing agglomeration of phytoncide molecule comprises the following steps: pouring 1000ml of compound phytoncide aqueous solution into the blender, then adding 0.5 to 1 percent of an inorganic dispersant, stirring for 3 to 5 minutes, and then pouring the compound phytoncide aqueous solution and the inorganic dispersant into a supersonic oscillator to perform oscillation for 2 to 4 minutes at the frequency of 20KHz.

Description

technical field [0001] The invention relates to a method for preparing plant essential oils, and belongs to the technical field of plant phytoncide. In particular, it refers to a method for making natural phytoncine molecules into nanometers without agglomeration. Background technique [0002] When higher plants are injured, they will emit "phytoncine" to kill other organisms in their surroundings. However, all plants contain "phytoncine". If protozoa such as amoeba or pathogenic bacteria such as typhoid, cholera, and diphtheria are placed next to fresh crushed leaves, these pathogenic bacteria will be killed after a few minutes Exhausted, so it can be proved that the plant has a defense system against mold or bacteria. Phytondine is an aromatic carbohydrate, and different tree species have different phytondines. [0003] At present, the production of phytondo essential oil is a unilateral phytondoline made from the roots, stems, and leaves of higher plants (such as pine,...

Claims

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Application Information

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IPC IPC(8): C11B3/00A61L9/013A01N65/28A01P1/00A61L101/56
CPCA01N65/00A01N65/28A61L9/013A61L2209/21C11B3/008A01N2300/00
Inventor 野艳玲
Owner 野艳玲
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