Reinforced product comprising a composition with a low sulphur content and tyre comprising said reinforced product
A composition, sulfur content technology, applied in the direction of the reinforcement layer of pneumatic tires, special tires, tire parts, etc., can solve the problems of preparation of semi-finished products, prolonged preparation time, cracking of the mixture, etc.
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Embodiment 1
[0144] 3.3 - Example 1 - Rubber Test
[0145] For the requirements of these tests, rubber compositions were prepared according to the invention, the formulations of which are given in Table 1; the contents of the different products are expressed in phr (parts by weight per one hundred parts by weight of elastomer).
[0146] These compositions were prepared using the following procedure: Reinforcing fillers (carbon black and / or silica), diene elastomer and various other ingredients, in addition to the vulcanization system, were introduced continuously into an internal mixer which The initial vessel temperature was about 50°C; the mixer was thus filled to about 70% (volume %). Thermomechanical processing (non-production stage) is then carried out in one step for about 3 to 5 minutes until a maximum "dropping" temperature of 160°C is reached. The mixture thus obtained is recovered and cooled before introducing sulfur and accelerators of sulfenamide type in an external mixer (h...
Embodiment 2
[0170] 3.4 - Example 2 - Test of adhesion of coating composition and filamentary reinforcement
[0171] In order to test the adhesion of the coating composition on the filamentary reinforcement, the measurement is carried out according to the standard ASTM D2229.
[0172] Compositions C(a), C(b) (control) and C(c) presented in Table 3 below (according to the invention and identical to C4 above) are combined with brass metal reinforcement, which Reinforcement consists of 2+7 0.7% carbon steel wires 28 / 100mm diameter with an assembled lay length of 7.5mm / 15mm, brass contains 68% copper, clad or unclad, as shown in table 4 below , and the adhesion of the coating composition to the reinforcement was tested for these combinations. In the case of reinforcement cladding, the cladding is made of polyamide 6-6, the average thickness of the cladding is about 0.14 mm for a clad cord diameter of ca. 1.35 mm, and is bonded by RFL agent coverage.
[0173] table 3
[0174]
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