Preparation method for spinning flame retardation polyester filament using flask return
A technology of flame-retardant polyester and bottle flakes, which is applied in the manufacture of fire-resistant and flame-retardant filaments, the melting of filament raw materials, and melt spinning, which can solve the problems of no reports of flame-retardant polyester filaments and achieve good flame-retardant properties , high safety effect
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[0016] A method for preparing flame retardant polyester filaments (POY176dtex / 96f) with bottle flakes returned from the present invention is to dry the recycled polyester bottle flakes, and then send the dried polyester bottle flakes back through the pipeline into the extruder. It is melted and extruded in the machine, spun through a spinneret, and the tow is cooled and oiled by air blowing, and then wound by a winding head to obtain bottle flake recycled flame-retardant polyester filament (POY176dtex / 96f). Specifically include the following steps:
[0017] Step 1. Pre-crystallize the material. The material is polyester bottle flakes; specifically, dry hot air is used for pre-crystallization; Temperature The temperature is 170-178°C, the air dew point is less than or equal to -70°C, the moisture content of the material is 40ppm, and the drying time is 4-8 hours.
[0018] Step 2. Screw feeding of materials: firstly dry the polyester bottle flakes with hot air, and then feed th...
Embodiment 1
[0025] A method for preparing flame-retardant polyester filament (POY176dtex / 96f) spun from bottle flakes, comprising the following steps:
[0026] Step 1. Pre-crystallize the material. The material is polyester bottle flakes; specifically, dry hot air is used for pre-crystallization; when the material is pre-crystallized, the pre-crystallization temperature is 170°C, and the temperature of the dry hot air
[0027] The temperature is 172°C, the air dew point is -70°C, the moisture content of the material is 40ppm, and the drying time is 6 hours.
[0028] Step 2. Screw feeding of materials: firstly dry the polyester bottle flakes with hot air, and then feed the dried polyester bottle flakes back into the screw extruder through the pipeline; when the materials are screw fed, the Materials
[0029] Recycling for PET (polyethylene terephthalate) bottle flakes.
[0030] Step 3: The flame-retardant masterbatch is added quantitatively. After the flame-retardant masterbatch is dried...
Embodiment 2
[0039] A method for preparing flame-retardant polyester filament (POY176dtex / 96f) spun from bottle flakes, comprising the following steps:
[0040] Step 1. Pre-crystallize the material. The material is polyester bottle flakes; specifically, dry hot air is used for pre-crystallization; when the material is pre-crystallized, the pre-crystallization temperature is 172 ° C, and the temperature of the dry hot air is
[0041] The temperature is 174°C, the air dew point is -60°C, the moisture content of the material is 40ppm, and the drying time is 5 hours.
[0042] Step 2. Material feeding by screw: first dry the polyester bottle flakes with hot air, and then dry the dried
[0043] The polyester bottle flakes are fed back into the screw extruder through the pipeline; when the material is fed into the screw, the material is
[0044] PET (polyethylene terephthalate) bottle flakes return.
[0045] Step 3: The flame-retardant masterbatch is added quantitatively. After the flame-retard...
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