A pressure swing adsorption method for pressure change linkage control in cycle operation

A pressure swing adsorption and cyclic operation technology, applied in chemical instruments and methods, separation methods, dispersed particle separation, etc., can solve problems such as high failure rate of program control valves, poor adaptability to raw gas fluctuations, and shortened service life of adsorbents. Achieve the effect of not easy to wear, prolong the service life and prolong the service life

Active Publication Date: 2019-12-17
SICHUAN TECHAIRS
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The present invention provides a pressure swing adsorption method of pressure change linkage control in cycle operation to solve the gap between the boundary condition setting of the inlet and outlet of the adsorption tower and the connection between the adsorption tower and the deviation between the traditional PSA process design and the actual operation. The program control valves on the inlet and outlet pipelines that only function to open and close are not linked, resulting in poor adaptability to raw gas fluctuations, high investment costs and poor stability caused by excessive pressure equalization times used to increase yields, and some industrial processes. However, there are technical problems such as double drop of "yield and purity", shortened service life of adsorbent and high failure rate of program control valve

Method used

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  • A pressure swing adsorption method for pressure change linkage control in cycle operation
  • A pressure swing adsorption method for pressure change linkage control in cycle operation
  • A pressure swing adsorption method for pressure change linkage control in cycle operation

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Embodiment 1

[0044] Such as figure 1 Shown, a kind of pressure swing adsorption method of pressure change linkage control in cyclic operation, described one group (section) pressure swing adsorption (PSA) adsorption and desorption cycle operating system adsorption tower that is formed by 5 adsorption towers is formed The linkage control of the determination mode of the boundary conditions of the inlet and outlet of the adsorption tower (mechanical designation, or independent judgment, or a combination of the two modes) and the program control valve-regulating valve combination in the simulation of the pressure swing adsorption (PSA) adsorption and desorption cycle operation process, According to the real-time pressure in the two target adsorption towers as a reference, by adjusting the opening and closing of the valve combination and the opening degree, the gas flow rate and the pressure change trend in the target adsorption tower and the inlet and outlet are controlled in real time, thus i...

Embodiment 2

[0057] Such as figure 2 As shown, further optimization on the basis of the pressure swing adsorption method of pressure change linkage control in a cycle operation described in Example 1, the pressure is 2.4MPa, and the temperature is a hydrogen-containing (50-60% H2 ) The feed gas fluctuates, that is, under the same temperature and other conditions, the feed gas pressure fluctuates by more than 5% and rises to 2.6MPa. The pressure swing adsorption (PSA) adsorption and desorption cycle composed of five adsorption towers 2 In the operating system, the operating pressure change of each step is determined by the boundary conditions independently determined by the inlet and outlet of each adsorption tower (indicated by double dashed lines) and the program control valve on the pipeline connected to the inlet and outlet of each adsorption tower- The combination mode of the regulating valve is realized by linkage control, in which the intermediate pressure values ​​of the first-stag...

Embodiment 3

[0059] Such as image 3 As shown, further optimize on the basis of the pressure swing adsorption method of pressure change linkage control in a kind of cyclic operation described in embodiment 1, described pressure swing adsorption (PSA) adsorption that is made up of 5 adsorption towers 2 and In the desorption cycle operating system, the program control valve-regulating valve combination on the pipeline connected to the inlet and outlet of each adsorption tower 2 is a program control valve followed by a regulating valve connected in series to form a one-to-one correspondence combination mode. The purpose of this embodiment is to greatly increase the stability of the system (device), and to be more adaptable to the relatively large fluctuations in pressure during feed gas and cycle operation, so that the operation of the device can at least even exceed the level of Embodiment 1.

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Abstract

The invention discloses a pressure-swing adsorption method for coupling control of pressure change in cyclic operation and relates to the technical field of pressure-swing adsorption gas-separation technologies. The pressure-swing adsorption method comprises the following steps: carrying out simulation on the cyclic operation process of adsorption and desorption of a pressure-swing adsorption system to determine a mechanical designation mode, an autonomous judgment mode and a mechanical-autonomous combining mode by boundary conditions of an inlet and an outlet of an adsorbing tower in simulation, wherein the pressure-swing adsorption system consists of one or more groups of adsorbing tower sections consisting of at least two adsorbing towers; and carrying out coupling control on the determined control mode and combination of a program control valve and an adjusting valve, by adopting instantaneous pressure in two or more target adsorption towers as basis, adjusting opening and closing as well as opening degree of valve combination, carrying out instantaneous coupling control on gas flowing speed and pressure change trend in the target adsorption tower and the inlet and outlet so as to increase the composition and pressure of raw gas of a pressure-swing adsorption device and the fault tolerance of pressure change of each step in the cyclic operation process of adsorption and desorption of pressure-swing adsorption.

Description

technical field [0001] The invention relates to the technical field of pressure swing adsorption gas separation technology, in particular to a pressure swing adsorption method for pressure change linkage control in cycle operation. Background technique [0002] Pressure Swing Adsorption (PSA for short) refers to, at a certain temperature, through the cyclic process of pressure adsorption and decompression (vacuumization) or normal pressure desorption or flushing replacement regeneration, the mixture gas is separated, purified and separated. purify. It can be seen that PSA achieves the purpose of adsorption and desorption by changing the pressure or pressure change. Adsorption is often carried out in a pressure environment. Pressure swing adsorption proposes a method of combining pressure and decompression. At a certain temperature, it is usually an adsorption-desorption (regeneration) process consisting of pressure adsorption and decompression regeneration. Loop operating ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D53/047
CPCB01D53/0454B01D53/047
Inventor 钟雨明陈运刘开莉唐金财陈勇蔡跃明
Owner SICHUAN TECHAIRS
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