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Method for rapidly measuring content of effective crumb rubber in crumb rubber modified asphalt

A modified asphalt, rapid measurement technology, applied in the direction of removing certain components and weighing, etc., can solve the problem of inability to effectively determine the effective rubber powder content of rubber powder modified asphalt, shorten the dissolution time, improve the filtration speed, The effect of improving accuracy

Active Publication Date: 2017-11-24
HEBEI PROVINCIAL COMM PLANNING & DESIGN INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In view of the above analysis, this application aims to provide a method for quickly determining the effective rubber powder content of rubber powder modified asphalt, in order to solve the problem that the existing technology cannot effectively measure the effective rubber powder content in rubber powder modified asphalt

Method used

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  • Method for rapidly measuring content of effective crumb rubber in crumb rubber modified asphalt
  • Method for rapidly measuring content of effective crumb rubber in crumb rubber modified asphalt
  • Method for rapidly measuring content of effective crumb rubber in crumb rubber modified asphalt

Examples

Experimental program
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Effect test

Embodiment 1

[0091] Select 20% rubber powder-modified asphalt, of which the viscosity at 180°C is 2.4Pa·S, the penetration is 48 (0.1mm), the softening point is 71.5°C, and the ductility at 5°C is 13cm; among them, 20% rubber powder is mixed in The raw materials in the modified asphalt are 100 parts by mass of asphalt, 25 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 2 parts of reinforcing agent phenolic resin, and 0.5 parts of crosslinking agent sulfur.

[0092] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0093] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm-diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, then transfer to a desiccator to cool for 30 minutes, and weigh the mass m1 of the round-bottom flask to be 95.474 g, taking the glass rod quality m2 is 14.271g, and taking the Buchner funnel quality m3 is 273.285g;

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Embodiment 2

[0115] Select 25% rubber powder-modified asphalt, which has a viscosity of 3.1Pa·S at 180°C, a penetration of 64 (0.1mm), a softening point of 73.0°C, and a ductility of 14cm at 5°C; 25% rubber powder is mixed in it The raw materials in the modified asphalt are 100 parts by mass of asphalt, 34 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 0.1 part of activator 980, 2 parts of reinforcing resin, and 0.5 parts of crosslinking agent sulfur share.

[0116] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0117] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, then transfer it to a desiccator to cool for 30 minutes, and weigh the mass m1 of the round-bottom flask to be 95.480 g, taking the glass rod quality m2 is 14.273g, and taking the Buchner funnel quality m3 is 273.28...

Embodiment 3

[0140] Select 30% rubber powder-modified asphalt, of which the viscosity at 180°C is 3.2Pa·S, the penetration is 56 (0.1mm), the softening point is 71.5°C, and the ductility at 5°C is 17cm; among them, 30% rubber powder is mixed in The raw materials in the modified asphalt are 100 parts by mass ratio of asphalt, 43 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 0.14 parts of activator 980, 3 parts of reinforcing phenolic resin, and 0.5 parts of crosslinking agent sulfur .

[0141] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0142] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm-diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, and then transfer it to a desiccator to cool for 30 minutes. Weigh the mass m1 of the round-bottom flask to be 95.467 g, taking the glass rod quality m2 is 14.276g, and taking the Buchner...

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Abstract

The application relates to a method for rapidly measuring the content of effective crumb rubber in crumb rubber modified asphalt. The method mainly comprises the following steps: firstly, processing an instrument for testing; secondly, heating the crumb rubber modified asphalt to a melting state; preparing a crumb rubber modified asphalt solution; thirdly, inserting a Buchner funnel into a suction filtration flask; fourthly, putting filter paper into the Buchner funnel; fifthly, pouring the crumb rubber modified asphalt solution into the Buchner funnel, and carrying out suction filtration; sixthly, putting the Buchner funnel and filter paper together at a ventilation part; seventhly, putting the instrument into a baking oven, drying and cooling; weighing the mass of the Buchner funnel, the filter paper, a round bottomed flask and a glass rod together; eighthly, calculating the content of the effective crumb rubber, and determining overall performance of the crumb rubber modified asphalt according to the content of the effective crumb rubber. The application has the beneficial effects that the dissolution time of the crumb rubber modified asphalt is substantially shortened, the experiment cycle is compressed, and a large amount of solvent is saved; the performance and the thermal stability of modified asphalt internally doped with 20 percent or above of the crumb rubber can be comprehensive evaluated.

Description

technical field [0001] The present application relates to the technical field of determination of effective rubber powder content in rubber powder modified asphalt, in particular to a method for rapidly measuring the effective rubber powder content of rubber powder modified asphalt. Background technique [0002] With the blowout growth of the number of cars in modern society, as of June 2016, the number of motor vehicles in the country reached 285 million. At the same time, the number of heavy-duty trucks is also increasing, which makes my country's Road traffic is faced with many challenges such as large flow and axle load. Ordinary road petroleum asphalt refined by oil refineries can no longer meet the various requirements of high-grade highways, especially expressways, on the performance of asphalt binders. SBS has been widely used because it can greatly improve the road performance of road asphalt, but SBS is a high value-added material, and its application in the field ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N5/04
CPCG01N5/04
Inventor 蔡斌王国清秦禄生张忠民朱冀军王联芳王庆凯薛善光高海涛刘家辉李磊王洪涛高辉张文哲
Owner HEBEI PROVINCIAL COMM PLANNING & DESIGN INST