Composite nanofiber filter material with photocatalytic function and preparation method thereof
A technology of composite nanofibers and filter materials, which is applied in the field of photocatalytic materials, can solve problems such as easy blockage of the liquid outlet of the needle/nozzle, and achieve the effects of high efficiency, low resistance, increased spinning speed, and fine diameter
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Embodiment 1
[0045] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:
[0046] 1) Spinning liquid preparation: uniformly disperse titanium dioxide (0.5wt% added, particle size 10nm) in formic acid to form a dispersion liquid, and use an ultrasonic disperser (ultrasonic frequency 40kHz, ultrasonic temperature 80°C) to ultrasonically stir for 20min, and then Nylon 6 (with a weight average molecular weight of 50,000) was added to the dispersion, and after sealing, it was continuously stirred for 15 hours with a magnetic stirring device, and finally a stable and uniform polymer spinning solution with a mass concentration of 10% was prepared;
[0047] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to be stretched at the ...
Embodiment 2
[0052] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:
[0053] 1) Preparation of spinning solution: uniformly disperse titanium dioxide (addition amount 1wt%, particle size 15nm) in N,N-dimethylacetamide to form a dispersion solution, and use an ultrasonic disperser (ultrasonic frequency 40kHz, ultrasonic temperature 70°C ) after ultrasonic stirring for 30 min, polyurethane (weight-average molecular weight is 80,000) was added to the dispersion, and after sealing, it was continuously stirred for 8 hours with a magnetic stirring device, and finally a stable and uniform mass concentration of 15% polymer spinning was prepared. liquid;
[0054] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to be stretc...
Embodiment 3
[0059] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:
[0060] 1) Preparation of spinning solution: uniformly disperse titanium dioxide (addition amount 1.5wt%, particle size 18nm) in N,N-dimethylformamide to form a dispersion, and use an ultrasonic disperser (ultrasonic frequency 35kHz, ultrasonic temperature 50 ℃) after ultrasonic stirring for 40 minutes, polyvinylidene fluoride (weight-average molecular weight: 320,000) was added to the dispersion, and after sealing, it was continuously stirred for 9 hours with a magnetic stirring device, and finally a stable and uniform mass concentration of 18% was prepared. polymer spinning solution;
[0061] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to b...
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