Composite nanofiber filter material with photocatalytic function and preparation method thereof

A technology of composite nanofibers and filter materials, which is applied in the field of photocatalytic materials, can solve problems such as easy blockage of the liquid outlet of the needle/nozzle, and achieve the effects of high efficiency, low resistance, increased spinning speed, and fine diameter

Active Publication Date: 2018-01-19
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology uses an integrated combination of two different types of nozzles or needles: one used for electric field force (EFL) pulling fibers towards another object called target, such as paper, plastic sheet, etc., and the second type that helps create tiny holes on it through evaporation process. These techniques help prevent blockages from happening during production processes without causing damage to equipment. Additionally, this new method allows for more efficient use of resources than traditional methods like water jet cleaning.

Problems solved by technology

This patented technical problem addressed in this patent relates to finding ways to efficiently remove small amounts of gaseous substances like formalin that are released during construction projects without causing damage to surrounding areas due to their negative effects on human health. Current methods involve filters made up mostly of glass fibers which may become clogged over time leading to increased cleaning costs for maintenance workers. Therefore there needs a new type of catalyst called TiOn/nanosiloxane that works well even at low concentrations while still maintains good physical properties.

Method used

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  • Composite nanofiber filter material with photocatalytic function and preparation method thereof

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Effect test

Embodiment 1

[0045] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:

[0046] 1) Spinning liquid preparation: uniformly disperse titanium dioxide (0.5wt% added, particle size 10nm) in formic acid to form a dispersion liquid, and use an ultrasonic disperser (ultrasonic frequency 40kHz, ultrasonic temperature 80°C) to ultrasonically stir for 20min, and then Nylon 6 (with a weight average molecular weight of 50,000) was added to the dispersion, and after sealing, it was continuously stirred for 15 hours with a magnetic stirring device, and finally a stable and uniform polymer spinning solution with a mass concentration of 10% was prepared;

[0047] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to be stretched at the ...

Embodiment 2

[0052] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:

[0053] 1) Preparation of spinning solution: uniformly disperse titanium dioxide (addition amount 1wt%, particle size 15nm) in N,N-dimethylacetamide to form a dispersion solution, and use an ultrasonic disperser (ultrasonic frequency 40kHz, ultrasonic temperature 70°C ) after ultrasonic stirring for 30 min, polyurethane (weight-average molecular weight is 80,000) was added to the dispersion, and after sealing, it was continuously stirred for 8 hours with a magnetic stirring device, and finally a stable and uniform mass concentration of 15% polymer spinning was prepared. liquid;

[0054] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to be stretc...

Embodiment 3

[0059] A composite nanofiber filter material with photocatalytic function and a preparation method thereof, the preparation method comprising the following steps:

[0060] 1) Preparation of spinning solution: uniformly disperse titanium dioxide (addition amount 1.5wt%, particle size 18nm) in N,N-dimethylformamide to form a dispersion, and use an ultrasonic disperser (ultrasonic frequency 35kHz, ultrasonic temperature 50 ℃) after ultrasonic stirring for 40 minutes, polyvinylidene fluoride (weight-average molecular weight: 320,000) was added to the dispersion, and after sealing, it was continuously stirred for 9 hours with a magnetic stirring device, and finally a stable and uniform mass concentration of 18% was prepared. polymer spinning solution;

[0061] 2) Electrospinning: the prepared polymer spinning solution is sucked into the spinning module through the liquid supply device, and the combined needle for electrospinning is used to realize the spinning polymer solution to b...

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Abstract

The invention relates to a composite nanofiber filter material with photocatalytic function and a preparation method thereof. The filter material consists of a support layer and a nanofiber filter layer attached to the surface of the support layer, and the nanofiber layer is uniformly filled with a photocatalyst. The preparation method comprises the steps of: 1) preparation of a spinning solution:dispersing a certain amount of photocatalyst evenly in a solvent to form a dispersion, conducting ultrasonic treatment, then adding a high polymer to form a stable and homogeneous electrostatic spinning solution; 2) electrospinning: setting electrospinning parameters, using a combined needle for electrospinning to achieve silk stretching of a spinning polymer solution at a solid metal wire tip; and 3) use of recovered solvent vapor for slight dissolving treatment on the composite nanofiber filter material surface at certain release rate, thus obtaining the composite nanofiber filter materialwith photocatalytic function finally. The composite nanofiber filter material with photocatalytic function provided by the invention effectively solves the easy blocking problem of existing electrospinning needle/nozzle liquid discharge ends, has good photocatalytic efficiency on formaldehyde, amine, toluene and the like, and also has excellent filtration performance, thus having broad applicationprospects.

Description

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Claims

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Application Information

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Owner DONGHUA UNIV
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