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Treatment method for contact end of surface of oriented carbon nano tube-modified carbon fiber on the basis of gas-phase carbon nano tube dispersion mist

A carbon nanotube modification, carbon nanotube technology, applied in fiber processing, carbon fiber, textiles and papermaking, etc., to achieve the effect of simple operation, enhanced bonding force, and obvious effect

Active Publication Date: 2018-01-19
QINGDAO UNIV OF SCI & TECH
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Problems solved by technology

[0005] Aiming at the deficiencies of the existing multi-component nanomaterial dispersion technology, the present invention provides a method for treating the contact end of the carbon fiber surface modified by oriented carbon nanotubes based on gas-phase carbon nanotube dispersion mist. This method can not introduce additional sizing agents into the carbon fiber body Solve the problem of firm adhesion between oriented carbon nanotubes and carbon fiber contact ends on the basis of

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  • Treatment method for contact end of surface of oriented carbon nano tube-modified carbon fiber on the basis of gas-phase carbon nano tube dispersion mist

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Embodiment Construction

[0022] The present invention is described in detail below. However, these implementations do not limit the present invention, and method or functional changes made by those skilled in the art according to these implementations are included in the protection scope of the present invention.

[0023] Specific steps are as follows:

[0024] (1) Evenly mix carbon nanotubes, sizing agent, and deionized water in a mass ratio of 1:1:4;

[0025] (2) Press the mixture described in step (1) into a block and connect it to the cathode of the pulsed high-voltage DC power supply, use a tungsten columnar electrode to connect to the anode of the pulsed high-voltage DC power supply, and keep the distance between the adjacent ends of the cathode and the anode at 1 mm, and turn on Power supply to complete the gas phase dispersion of carbon nanotubes;

[0026] Specifically, the high-voltage DC power supply adopts a voltage of 20000V and a maximum power of 100W; the pulse parameters are: frequenc...

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Abstract

The invention discloses a treatment method for a contact end of a surface of an oriented carbon nano tube-modified carbon fiber on the basis of gas-phase carbon nano tube dispersion mist. The method includes the steps of: 1) uniformly mixing carbon nano tubes, a sizing agent and a diluting agent to form a semi-fluid; 2) dispersing the mixture to form gas-phase carbon nano tube mist with pulsed arc; 3) moving a carbon fiber close to a discharge point of the arc; 4) forming relative constant-speed movement between the discharge point of the pulsed arc and the carbon fiber; 5) baking the carbon fiber in a baking oven; and 6) after the carbon fiber is baked, cooling the carbon fiber to room temperature to finish the treatment for the contact end of the surface of the oriented carbon nano tube-modified carbon fiber.

Description

technical field [0001] The invention relates to the field of new materials, in particular to a method for treating the contact end of carbon nanotube modified carbon fiber surface. Background technique [0002] Carbon fiber, as a typical application representative of new carbon materials, is widely used in the manufacture of high-end composite materials due to its excellent mechanical, electrical and chemical stability, and has become a popular choice in many fields, especially including aerospace, lightweight equipment, military industry, etc. The key research object is an indispensable key material for today's advanced manufacturing and advanced equipment. [0003] The surface of carbon fiber is smooth and its chemical activity is low. Affected by this, it is easy to debond from the composite material matrix. For this reason, many technologies represented by improving the surface roughness of carbon fiber have been disclosed one after another. It mainly includes electroch...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M23/06D06M11/74D06M101/40
Inventor 何燕李少龙张传琪宫秀斌
Owner QINGDAO UNIV OF SCI & TECH
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