Preparation method and application of visible light and Fenton composite catalyst
A composite catalyst, visible light technology, applied in catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of poor photocatalytic performance and insufficient reactivity, and achieve large specific surface area and visible light response frequency. Wide range and high light conversion efficiency
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Embodiment 1
[0027] A preparation method of visible light Fenton composite catalyst, comprising the following steps:
[0028] (1) Take ferrous nitrate and lithium nitrate and add them to deionized water, so that the molar ratio of ferrous ions and lithium ions is 1: 1, stir and dissolve to obtain solution A;
[0029] (2) Weigh Li 2 WO 4 2H 2 O was added to deionized water, stirred and dissolved to obtain Li 2 WO 4 solution, to Li 2 WO 4 Add isobutanol in the solution, the addition of isobutanol is every 1mmolM 2 WO 4 2H 2 O was added to 8mL, and stirred evenly to obtain solution B;
[0030] (3) Slowly add solution A to solution B and stir evenly so that the molar ratio of ferrous ions, lithium ions and tungsten ions is 2:2:1, then add sodium hydroxide solution to adjust the pH value of solution B to 8.5, The mixture C was obtained, and the mixture C was transferred to a hydrothermal reactor and sealed, and reacted at 190° C. for 18 hours;
[0031] (4) After the reaction kettle i...
Embodiment 2
[0035] A preparation method of visible light Fenton composite catalyst, comprising the following steps:
[0036] (1) Take ferrous chloride and lithium nitrate and add them to deionized water, so that the molar ratio of ferrous ions and lithium ions is 1: 1, stir and dissolve to obtain solution A;
[0037] (2) Weigh tungstate Na 2 WO 4 2H 2 O was added to deionized water, stirred and dissolved to obtain Na 2 WO 4 solution, to Na 2 WO 4 Add isobutanol in the solution, and the addition amount of isobutanol is every 1mmolNa 2 WO 4 2H 2 Add 10mL of O and stir evenly to obtain solution B;
[0038] (3) Slowly add solution A to solution B and stir evenly so that the molar ratio of ferrous ions, lithium ions and tungsten ions is 2:2:1, then add sodium hydroxide solution to adjust the pH value of solution B to 8.8, The mixture C was obtained, and the mixture C was transferred to a hydrothermal reactor and sealed, and reacted at 195° C. for 16 hours;
[0039] (4) After the rea...
Embodiment 3
[0042] A preparation method of visible light Fenton composite catalyst, comprising the following steps:
[0043] (1) Take ferrous sulfate and lithium nitrate and add them to deionized water, so that the molar ratio of ferrous ions and lithium ions is 1: 1, stir and dissolve to obtain solution A;
[0044] (2) Weigh tungstate K 2 WO 4 2H 2 O was added to deionized water, stirred and dissolved to obtain K 2 WO 4 solution, to K 2 WO 4 Add isobutanol in the solution, the addition of isobutanol is every 1mmolK 2 WO 4 2H 2 O was added to 12mL and stirred evenly to obtain solution B;
[0045] (3) Slowly add solution A to solution B and stir evenly so that the molar ratio of ferrous ions, lithium ions and tungsten ions is 2:2:1, then add sodium hydroxide solution to adjust the pH value of solution B to 9.0, The mixture C was obtained, and the mixture C was transferred to a hydrothermal reactor and sealed, and reacted at 200° C. for 12 hours;
[0046] (4) After the reaction k...
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