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Method for measuring contents of carbon and sulfur in chromium ores

A determination method and technology for sulfur content, which are used in measuring devices, material analysis by optical means, instruments, etc., can solve the problems of inability to guarantee the accuracy of detection, narrow detection range of sulfur content, etc., and save reagents and personnel input. , the detection speed is fast, the result is accurate

Inactive Publication Date: 2018-02-16
阿拉山口出入境检验检疫局综合技术服务中心
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Problems solved by technology

[0006] The purpose of the present invention is to overcome the deficiencies in the prior art, provide a kind of assay method of carbon, sulfur content in chrome ore, method is simple, preferably overcome only the sulfur content in chrome ore is measured in existing method, and the limitation of sulfur content The detection range is relatively narrow, and the technical problem that the accuracy of the detection cannot be guaranteed for samples higher than 0.5%, to achieve not only the determination and analysis of single elements, but also solve the technical problems of the determination of different levels of carbon and sulfur elements

Method used

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  • Method for measuring contents of carbon and sulfur in chromium ores
  • Method for measuring contents of carbon and sulfur in chromium ores
  • Method for measuring contents of carbon and sulfur in chromium ores

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Embodiment

[0019] A method for measuring carbon and sulfur content in chrome ore, comprising the following steps:

[0020] S1. Crush the sample to pass through a 100-mesh sieve, then dry it in an oven at 60°C for 4 hours, and then cool it to room temperature in a desiccator;

[0021] S2. Weigh 0.05-0.5 parts by weight of the sample to be tested and place it in a burnt crucible with 0.38-0.42 parts by weight of pure iron flux on the bottom, and cover the surface of the sample to be tested with 1.1-1.3 parts by weight of tungsten particles and 0.24 parts by weight. ~0.26 parts by weight of tin particles are detected by a high-frequency infrared carbon-sulfur analyzer to obtain the content of carbon and sulfur.

[0022] In a preferred embodiment, the sample to be tested is 50-500 mg, the pure iron flux is 0.4 g, the tungsten particle is 1.2 g, and the tin particle is 0.25 g.

[0023] In a preferred embodiment, the absolute value of the sulfur content in the sample to be tested is not more ...

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Abstract

The invention relates to the technical field of ore detection, in particular to a method for measuring the contents of carbon and sulfur in chromium ores. The method comprises the following steps: S1,smashing a sample to be measured till the sample can pass through sieve pores of 100 meshes, and drying the sample; S2, weighing 0.05 to 0.5 weight part of the sample to be measured, putting the sample to be measured into a crucible which is burnt, and is laid with 0.38 to 0.42 weight part of a pure iron fluxing agent at the bottom, covering the surface of the sample to be measured with 1.1 to 1.3 weight parts of tungsten particles and 0.24 to 0.26 weight part of tin particles, and detecting the sample through a high-frequency infrared carbon-sulfur instrument, thereby obtaining the contentsof the carbon and the sulfur. The method for measuring the contents of the carbon and the sulfur in the chromium ores is easy to operate, high in detection speed and low in cost; the detection range is 0.1 to 15 percent; the accuracy and the precision can meet requirements for measurement of the contents of carbon and sulfur in imported and exported chromium ores; the method has the advantages ofshort detection period, accurate result and saving of reagent and personnel investment, can completely meet a requirement of the foreign trade for inspection, quarantine and quick detection, is relatively high in practicability, and can be widely popularized and applied.

Description

technical field [0001] The invention relates to the technical field of ore detection, in particular to a method for measuring the content of carbon and sulfur in chrome ore. Background technique [0002] Chromium ore, also known as chromite, is mainly used in the fields of metallurgical industry, chemical industry and refractory materials. Chromium ore is a resource that is in short supply in China, and the chrome ore used in my country mainly relies on imports. The content of sulfur in chrome ore is an important indicator of the quality of chrome ore. High sulfur content will directly lead to high sulfur content in downstream products, which will adversely affect product performance. At the same time, it will cause processing costs in downstream processing. Increased air and soil sulfur pollution will have long-term impacts on the environment, crops and human health. In September 2013, the General Office of the State Council issued the "Action Plan for Prevention and Contr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/3563
CPCG01N21/3563
Inventor 吕新明
Owner 阿拉山口出入境检验检疫局综合技术服务中心
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