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Lubricating grease and preparation method thereof

A grease, gallium-based technology, applied in the field of grease and its preparation, can solve the problems of poor anti-wear performance, strong corrosion, strong irritation, etc.

Active Publication Date: 2018-04-20
TSINGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the extreme pressure agents of lubricating grease are usually sulfur-containing compounds (such as sulfurized olefins, sulfurized lard, sulfurized oleic acid, polysulfides), phosphorus-containing compounds (such as phosphates, phosphites, phosphates) and nanomaterials. , and sulfur-containing compounds and phosphorus-containing compounds have the disadvantages of strong irritation and strong corrosion when they are used as extreme pressure agents for grease; in addition, when liquid metal is directly used as a lubricant, the cost is high, and under low load conditions Poor wear resistance

Method used

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  • Lubricating grease and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Take 98g of grease base, add 0.5g of antioxidant 2,6-di-tert-butyl-p-cresol, 1g of anti-wear agent diethyl phosphate amine salt, 0.5g of pure gallium, heat to 90°C and stir for 30min until uniform, cool to room temperature, transferred to a three-roll mill and ground for 3-5 hours to obtain sample 1.

Embodiment 2

[0044] Take 98g of grease matrix, add 0.5g of antioxidant 2,6-di-tert-butyl-p-cresol, 1g of anti-wear agent diethyl phosphate amine salt, 0.5g of a mixture containing 75 parts by weight of gallium and 25 parts by weight of indium, Heat to 90°C and stir for 30min until uniform, transfer to a three-roll mill and grind for 3-5h uniformly, cool to room temperature to obtain sample 2.

Embodiment 3

[0046] Take 98g of grease base, add 0.5g of antioxidant 2,6-di-tert-butyl-p-cresol, 1g of anti-wear agent diethyl phosphate amine salt, containing 64 parts by weight of gallium, 24 parts by weight of indium and 12 parts by weight of tin 0.5 g of the mixture was heated to 90°C and stirred for 30 min until uniform, cooled to room temperature, transferred to a three-roll mill and ground for 3-5 h to obtain sample 3.

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Abstract

The invention provides a lubricating grease and a preparation method thereof. The lubricating grease comprises a lubricating grease matrix and a gallium-based liquid metal. The lubricating grease hasthe advantages of non-toxicity, no irritation and no corrosion, achieves same excellent extreme pressure performances with the gallium-based liquid metal under a high load condition with only 1 / 10 orless of the cost of the gallium-based liquid metal, has significantly better wear resistance than the gallium-based liquid metal under a low load condition, and is suitable for various working environments from low load to high load.

Description

technical field [0001] The invention relates to the technical field of lubrication, in particular to lubricating grease and a preparation method thereof. Background technique [0002] At present, the extreme pressure agents of lubricating grease are usually sulfur-containing compounds (such as sulfurized olefins, sulfurized lard, sulfurized oleic acid, polysulfides), phosphorus-containing compounds (such as phosphate esters, phosphite esters, phosphates) and nanomaterials. , and sulfur-containing compounds and phosphorus-containing compounds have the disadvantages of strong irritation and strong corrosion when they are used as extreme pressure agents for grease; in addition, when liquid metal is directly used as a lubricant, the cost is high, and under low load conditions Poor wear resistance. [0003] Therefore, the relevant technology of existing lubricating grease still needs to be improved. Contents of the invention [0004] The present invention aims to solve one of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M125/04C10M169/00C10M169/06C10N30/06C10N50/10
CPCC10M125/04C10M169/00C10M169/06C10M2201/05C10M2203/1006C10M2207/1236C10M2207/1285C10N2030/06C10N2050/10C10N2010/02
Inventor 田煜白鹏鹏李少伟陶大帅贾文鹏孟永钢
Owner TSINGHUA UNIV
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