Corrosion-resistant glass flake resin
A technology of glass flake resin and glass flakes, which is applied in the direction of anti-corrosion coatings, coatings, etc., can solve the problems of poor corrosion resistance of fluorine, enhancement, poor compatibility of organic polymers, etc.
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[0052] A second aspect of the present invention provides a method for preparing a corrosion-resistant glass flake resin, comprising the steps of:
[0053] (1) Preparation of component A: Stir glass flakes, calcium carbonate, titanium dioxide, and methyl isobutyl ketone in the reactor for 10 minutes, then add mercaptosilane and aminosilane, and stir for 1 hour; then add allyl Glycidyl ether, vinyl thiophene, vinyl benzimidazole, then add cyclohexanone peroxide, heat to 158°C, react for 12 hours, cool to room temperature, add simethicone, stir well, and age for 24 hours to obtain the compound score A;
[0054] (2) Preparation of component B: stir pentaerythritol glycidyl ether, 2-aminomethyl-15-crown ether-5, and tetrahydrofurfuryl alcohol at room temperature to obtain component B;
[0055] (3) Mix component A and component B, stir evenly, and after aging for 30 minutes, brushing can be carried out.
Embodiment 1
[0058] Corrosion-resistant glass flake resin, including component A and component B, component A is measured in parts by weight, and the preparation raw materials include: 50 parts of allyl glycidyl ether, 25 parts of 2-vinylthiophene, 2-mercaptoethyltris 5 parts of ethoxysilane, 4 parts of N-methyl-3-aminopropyltrimethoxysilane, 15 parts of (5-vinyl-1H-benzimidazol-2-yl) methyl mercaptan, 380 mesh of glass flakes 25 parts, 1 part of titanium dioxide, 12 parts of methyl isobutyl ketone, 1 part of light calcium carbonate, 0.05 part of simethicone;
[0059] Component B is in parts by weight, and the raw materials for preparation include: 2 parts of pentaerythritol glycidyl ether, 8 parts of 2-aminomethyl-15-crown ether-5, and 3 parts of tetrahydrofurfuryl alcohol;
[0060] The weight ratio of component A and component B is 1:0.3;
[0061] The preparation method comprises the following steps:
[0062] (1) Preparation of component A: Stir glass flakes of 380 mesh, light calcium ...
Embodiment 2
[0066] Corrosion-resistant glass flake resin, including component A and component B, component A is in parts by weight, and the raw materials for preparation include: 50 parts of allyl glycidyl ether, 25 parts of 3-vinylthiophene, 2-mercaptoethyltris 5 parts of ethoxysilane, 4 parts of N-methyl-3-aminopropyltrimethoxysilane, 15 parts of (5-vinyl-1H-benzimidazol-2-yl) methyl mercaptan, 380 mesh of glass flakes 25 parts, 1 part of titanium dioxide, 12 parts of methyl isobutyl ketone, 1 part of light calcium carbonate, 0.05 part of simethicone;
[0067] Component B is in parts by weight, and the raw materials for preparation include: 2 parts of pentaerythritol glycidyl ether, 8 parts of 2-aminomethyl-15-crown ether-5, and 3 parts of tetrahydrofurfuryl alcohol;
[0068] The weight ratio of component A and component B is 1:0.3;
[0069] The preparation method comprises the following steps:
[0070] (1) Preparation of component A: Stir glass flakes of 380 mesh, light calcium carbo...
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