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Single-phase supersaturated solid solution magnesium-aluminum alloy and preparation method thereof

A magnesium-aluminum alloy and solid solution technology, applied in the field of metallurgy, can solve problems such as difficulty in obtaining single-phase supersaturated solid solution, decline in mechanical properties and processing properties of materials, and coarse grains, etc., to achieve reasonable and novel method design, low manufacturing cost, Effect of high elongation at room temperature

Inactive Publication Date: 2018-05-04
YANGZHOU POLYTECHNIC INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the currently used heat treatment process is difficult to completely dissolve aluminum for high-alumina-magnesium alloys to obtain single-phase supersaturated solid solution high-alumina-magnesium alloys. Generally speaking, this method has two shortcomings. One is that long-term heating causes coarse grains, The mechanical properties and processing properties of the material are reduced. Second, it is difficult to completely dissolve the second phase in the matrix even if it is homogenized for a long time, and it is difficult to obtain the structure of a single-phase supersaturated solid solution.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The invention is a method for preparing a single-phase supersaturated solid solution magnesium-aluminum alloy, comprising the following steps:

[0025] (1) Melting magnesium, aluminum and other alloying elements after heating, wherein the other alloying elements are alloying elements such as manganese, zinc, and rare earth;

[0026] (2) stirring and refining the melted metal in step (1);

[0027] (3) casting the molten metal after refining in step (2) into an alloy ingot, the quality of the aluminum element in the alloy ingot is 5% of the quality of the alloy ingot, and the mass content of other alloy elements in the alloy ingot is 0.9 %, the balance is magnesium; homogenization heat treatment is carried out after the alloy ingot casting is completed;

[0028] (4) carrying out the equal-channel extrusion deformation operation to the alloy ingot completed in step (3), the number of extrusion deformation operations of the equal-channel extrusion deformation operation is ...

Embodiment 2

[0036] The difference between this embodiment and embodiment 1 is that the present invention is a method for preparing a single-phase supersaturated solid solution magnesium-aluminum alloy, comprising the following steps:

[0037] (1) Melting magnesium, aluminum and a small amount of other alloying elements after heating, wherein the alloying elements are alloying elements such as manganese, zinc, and rare earth;

[0038] (2) stirring and refining the melted metal in step (1);

[0039] (3) casting the molten metal after refining in step (2) into an alloy ingot, the quality of the aluminum element in the alloy ingot is 13% of the quality of the alloy ingot, and the mass content of other alloy elements in the alloy ingot is 0.6 %, the balance is magnesium; homogenization heat treatment is carried out after the alloy ingot casting is completed;

[0040] (4) carrying out the equal-channel extrusion deformation operation to the alloy ingot completed in step (3), the number of extr...

Embodiment 3

[0046] The difference between this embodiment and embodiment 1 and embodiment 2 is: a method for preparing a single-phase supersaturated solid solution magnesium-aluminum alloy, comprising the following steps:

[0047] (1) Melting magnesium, aluminum and a small amount of other alloying elements after heating, wherein the alloying elements are alloying elements such as manganese, zinc, and rare earth;

[0048] (2) stirring and refining the melted metal in step (1);

[0049] (3) casting the molten metal after refining in step (2) into an alloy ingot, the quality of the aluminum element in the alloy ingot is 8% of the quality of the alloy ingot, and the mass content of other alloy elements in the alloy ingot is less than 0.7%, and the balance is magnesium; after the alloy ingot is cast, homogenization heat treatment is carried out;

[0050] (4) carrying out the equal-channel extrusion deformation operation to the alloy ingot completed in step (3), the number of extrusion deform...

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Abstract

The invention discloses a preparation method of a single-phase supersaturated solid solution magnesium-aluminum alloy. The method is characterized by comprising steps as follows: (1) magnesium, aluminum and a few alloy elements are heated and then smelted; (2) metal melt smelted in the step (1) is subjected to stirring and refining treatment; (3) the metal melt refined in the step (2) is cast to form an alloy ingot; (4) the alloy ingot completed in the step (3) is subjected to equal channel angular pressing operation; (5) a magnesium-aluminum alloy completed in the step (4) is subjected to solid solution treatment, and heating and heat insulation operations are performed during solid solution treatment; (6) the magnesium-aluminum alloy completed in the step (5) is subjected to cooling quenching, and then the micro-structure of the single-phase supersaturated solid solution magnesium-aluminum alloy can be obtained. The method has the advantages that defects in the prior art can be overcome, and the method is reasonable and novel in design.

Description

technical field [0001] The invention relates to a single-phase supersaturated solid solution magnesium-aluminum alloy and a preparation method thereof, belonging to the field of metallurgy. Background technique [0002] Magnesium-aluminum alloys have excellent mechanical properties and processing properties, and are widely used in the fields of aviation, aerospace, automobiles and electronics. Common magnesium-aluminum alloys are AZ31 (Mg-3Al-1Zn), AM60 (Mg-6Al-0.5Mn), AZ91 (Mg-9Al-1Zn) and domestic AZ61M, AZ62M, AZ80M, etc., which are characterized by good It can carry out large plastic deformation, so it is often used as a deformed magnesium alloy. The strength and plasticity of magnesium-aluminum alloys mainly depend on the form of aluminum in the alloy, because the solubility of aluminum in magnesium has a high rate of change with temperature, and the saturation solubility at high temperatures is extremely high (437 ° C, aluminum in magnesium The saturated solubility c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C23/02C22C1/02C22F1/06
CPCC22C1/02C22C23/02C22F1/002C22F1/06
Inventor 封娜徐军
Owner YANGZHOU POLYTECHNIC INST
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