Preparation method of ferrite material

A technology of ferrite material and ferrite pre-fired material, which is applied in the field of ferrite material preparation, can solve the problems of reduced degree of alignment, poor magnetic properties, and reduced orientation of ferrite, so as to increase density and improve Dispersion and the effect of improving the degree of orientation

Inactive Publication Date: 2018-07-06
浙江朗基新材料科技有限公司
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  • Summary
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  • Application Information

AI Technical Summary

Problems solved by technology

Compared with wet molding, since there is no dispersion medium, the friction between ferrite particles increases sharply, and the inevitable adhesion of ferrite particles occurs during the drying process, resulting in the arrangement of ferrite particles along the direction of easy magnetization The degree of the ferrite is significantly reduced, which will reduce the orientation degree of the formed ferrite, so the magnetic properties obtained by the dry formed ferrite in the prior art are poor

Method used

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Embodiment Construction

[0013] The present invention will be further described below in conjunction with specific embodiment:

[0014] A method for preparing a ferrite material, comprising the following steps,

[0015] Step 1, preparing ferrite calcined material, and performing wet crushing on the ferrite calcined material until the average particle size of the ferrite calcined material reaches 0.2-0.5 microns, washing with 3mol / L HCl solution and Filtration to remove impurity ions dissolved in the HCl solution in the calcined material;

[0016] Step 2, adding ferrite pre-sintered material into alkaline water, filtering after standing for 5 minutes, washing with deionized water, and then drying until the ferrite pre-sintered material dry powder with a water content lower than 0.4wt% is obtained, Using a vibration mill to vibrate and grind the dry ferrite pre-sintered powder, and after vibrating for 30 minutes, obtain the ferrite pre-sintered powder after vibration grinding;

[0017] Step 3, perform...

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Abstract

The invention discloses a preparation method of a ferrite material. The preparation method comprises the following steps: 1, preparing a ferrite pre-sintered material, and performing a wet crushing treatment on the ferrite pre-sintered material until the average particle size of the ferrite pre-sintered material reaches 0.2 to 0.5 micrometers; washing with 3mol/L HCl solution, and filtering to remove impurity ions, dissolved in the HCl solution, in the pre-sintered material; 2, adding the ferrite pre-sintered material into alkaline water, standing for 5 minutes and then filtering, washing withdeionized water, and then carrying out drying treatment until ferrite pre-sintered dry powder having a water content of less than 0.4wt% is obtained; carrying out vibration milling treatment on the ferrite pre-sintered dry powder for 30 minutes by using a vibrating mill so as to obtain ferrite pre-sintered powder subjected to vibration milling. The invention provides the preparation method of theferrite material.

Description

Technical field: [0001] The invention relates to a method for preparing a ferrite material. Background technique: [0002] At present, the forming methods of anisotropic sintered permanent magnet ferrite can be mainly divided into wet forming and dry forming. [0003] In wet forming, due to the presence of dispersion media such as water or ethanol, the ferrite particles are easy to rotate, and the ferrite particles are easy to arrange along the direction of easy magnetization in the magnetic field, which will make the formed ferrite obtain higher The degree of orientation, so wet-formed ferrite can obtain higher magnetic properties. However, wet molding needs to discharge the dispersion medium out of the mold cavity during press molding, so the productivity is low; in addition, wet molding has higher requirements for production equipment and higher production costs. [0004] In the existing dry molding, dry ferrite powder is directly filled into the mold cavity, and then p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/26C04B35/622
CPCC04B35/26C04B35/622C04B2235/6567
Inventor 王涛杨震亚
Owner 浙江朗基新材料科技有限公司
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