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Preparation method of large materials

A technology of large size and molding method, applied in metal processing equipment, transportation and packaging, etc., can solve the problems of inability to meet application requirements, high preparation cost, high price, etc., and achieve the effect of not easy to deform, meet application requirements, and save costs.

Inactive Publication Date: 2018-07-27
SOUTHWEST INST OF APPLIED MAGNETICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The preparation methods of the materials are all through the powder metallurgy process. The powder metallurgy process is a preparation method well known to those skilled in the art, including powder making, molding, isostatic pressing, sintering, and post-processing steps. The molding pressure of the molding process varies with the material. The force area and height become larger and larger. To prepare materials with larger dimensions, the higher the forming pressure of the press is required, and the press with greater forming pressure is more expensive and the preparation cost is higher. The preparation height is Take the 200mm rare earth cobalt permanent magnet material as an example. The traditional method needs to be pressed by a press of more than 300T, and the formed material has a density gradient. Large and small deformations in the middle cannot meet the application requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] This embodiment is to prepare a quadrilateral block samarium cobalt permanent magnet material with a length of 100mm, a width of 100mm and a height of 200mm;

[0025] Using the traditional method, the preparation of this material requires a press of more than 300T to press, and because the height is too high, the density difference between the two ends and the middle density is about 5%, forming a density gradient, which is easy to deform during sintering and cannot meet the needs;

[0026] This example figure 1 Shown, the procedure of its preparation is:

[0027] First use a 100T press to press ten ( figure 1 Only four) small blank blocks 1 with a length of 100mm, a width of 100mm and a height of 20mm are shown;

[0028] Then ten blank pieces 1 are stacked together to form blank 2;

[0029] Then the blank 2 is sealed with a plastic bag, and isostatically pressed under a pressure of 200 MPa, so that a plurality of blank pieces 1 are tightly combined and difficult to ...

Embodiment 2

[0034] This embodiment prepares a cylindrical manganese zinc ferrite core with a diameter of 100 mm and a height of 200 mm;

[0035] Using the traditional method, the preparation of the material requires a press of more than 300T to press, and because the height is too high, the density at the two ends is much higher than the density in the middle, forming a density gradient, which is easy to deform during sintering and cannot meet the needs;

[0036] This example figure 2 Shown, the procedure of its preparation is:

[0037] First use a 100T press to press ten ( figure 1 Only four) small blank blocks 1 with a diameter of 100 mm and a height of 20 mm are shown;

[0038] Then ten blank pieces 1 are stacked together to form blank 2;

[0039] Then the blank 2 is sealed with a plastic bag, and isostatically pressed under a pressure of 400 MPa, so that a plurality of blank pieces 1 are tightly combined and difficult to disperse, and by isostatic pressing, the blank 2 has a unifo...

Embodiment 3

[0044] In this embodiment, a ring-shaped nickel-zinc ferrite core with a diameter of φ200mm×180mm and a height of 200mm is prepared;

[0045] Using the traditional method, the preparation of the material requires a press of more than 300T to press, and because the height is too high, the density at the two ends is much higher than the density in the middle, forming a density gradient, which is easy to deform during sintering and cannot meet the needs;

[0046] This example image 3 Shown, the procedure of its preparation is:

[0047] First use a 100T press to press ten ( figure 1 Only four) φ200mm×180mm high 20mm blank small block 1 is shown;

[0048] Then ten blank pieces 1 are stacked together to form blank 2;

[0049] Then the blank 2 is sealed with a plastic bag, and isostatically pressed under a pressure of 600 MPa, so that a plurality of blank pieces 1 are tightly combined and difficult to disperse, and by isostatic pressing, the blank 2 has a uniform density and is n...

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Abstract

The invention discloses a preparation method of large materials. According to the preparation method, on the basis of a traditional powder metallurgy process, a forming process is improved, small workblanks (1) with low height are pressed first, then a plurality of small workblanks are overlaid so as to form workblanks (2), isostatic pressing is performed on the workblanks (2), the workblanks (2)are vertically loaded during sintering in an overlaying direction, the small workblanks (1) are completely in solution through high-temperature sintering, and then traces of edges between the small workblanks (1) on the surface are ground and removed through processing, so that the required size and shape are processed. According to the preparation method, the materials of which the axial size reaches 1000 mm can be prepared, the pressure requirement on a pressing machine is not high, the cost is reduced, and the density gradient caused by once forming is reduced, so that the materials are difficult to deform after sintering, and the application requirement is satisfied.

Description

technical field [0001] The invention relates to the technical field of powder metallurgy process preparation, in particular to a method for preparing large-sized materials. Background technique [0002] At present, with the development of motors, wireless charging technology and the urgent need for magnetic shielding technology, it is necessary to prepare large-sized materials of more than 100mm. The preparation methods of the materials are all through the powder metallurgy process. The powder metallurgy process is a preparation method well known to those skilled in the art, including powder making, molding, isostatic pressing, sintering, and post-processing steps. The molding pressure of the molding process varies with the material. The force area and height become larger and larger. To prepare materials with larger dimensions, the higher the forming pressure of the press is required, and the press with greater forming pressure is more expensive and the preparation cost is ...

Claims

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Application Information

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IPC IPC(8): B22F1/00B22F3/00
CPCB22F3/005B22F1/14
Inventor 袁涛罗治涛王敬东沈安国张明邹杨王林梅王磊叶健曾德群向海蓉
Owner SOUTHWEST INST OF APPLIED MAGNETICS