Infrared nonlinear optical crystal, its preparation method and application
A nonlinear optics, crystal technology, applied in nonlinear optics, chemical instruments and methods, optics, etc., can solve the problems of low laser damage threshold, two-photon absorption, nonlinear optical coefficient, high, medium and far infrared transmittance, etc. Excellent second-order nonlinear optical properties, strong frequency doubling response, the effect of realizing large frequency doubling coefficient and high laser damage threshold
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[0042] The molar ratio of strontium sulfide, zinc sulfide and gallium sulfide is SrS:ZnS:Ga 2 S 3 =5:1:3 Fully grind and mix evenly and press into tablets, and place the pressed raw materials in a graphite crucible. Place the graphite crucible with raw materials in the quartz reaction tube, and vacuum to 10 -3 Pa, and use a hydrogen-oxygen flame to melt and seal the quartz reaction tube. Put the sealed quartz reaction tube into a tube furnace with a temperature controller, heat it to 950°C, keep it warm for 120 hours, then cool it down to 300°C at a rate of no more than 5°C / hour, stop heating, and naturally After cooling to room temperature, the pure phase of microcrystalline powder of nonlinear optical crystal material is obtained.
[0043] Put the quartz tube containing the pure phase of the above-mentioned microcrystalline powder into a tube furnace with a temperature controller to raise the temperature to 1000°C, keep it for at least 100 hours, and then cool it down to ...
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