A production device and production method for graphene-based composite negative electrode materials

A negative electrode material, graphene-based technology, applied in the field of production and preparation of new battery materials, can solve the problems of short battery cycle life, achieve the effect of improving cycle life, reducing internal resistance, and improving key performance

Active Publication Date: 2020-07-10
福州鼎烯飞扬科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The object of the present invention is to provide a production device and production method for graphene-based composite negative electrode materials, through which the production equipment and production method solve the problem of short battery cycle life of lithium batteries, and improve the critical performance of the battery at the same time Specifically, it is to reduce the internal resistance of the battery, and at the same time, improve the heat dissipation of the battery cell during high-rate charge and discharge.

Method used

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Embodiment 1

[0029] A production device for graphene-based composite negative electrode material, comprising a feeding device, a vacuum planetary mixer arranged downstream of the feeding device, and a reaction kettle arranged downstream of the vacuum planetary mixer, and the reaction kettle also includes a discharging device.

[0030] In this embodiment, the feeding device includes an automatic device for aqueous solution of graphene oxide, an automatic feeding device for negative electrode materials, and an automatic pure water production device. After the three are connected in parallel, the raw materials of the composite negative electrode material are simultaneously sent to a vacuum planetary mixer for mixing to obtain reaction raw materials with uniform texture.

[0031] In this embodiment, a control center is also included, and the control center is connected to the feeding device, the vacuum planetary mixer, the reaction kettle and the discharging device. Parameters and production p...

Embodiment 2

[0034] This embodiment is a production method for producing a graphene-based composite negative electrode material with a core-shell structure by applying the production device for graphene-based composite negative electrode material described in Embodiment 1.

[0035] The reaction raw material is generated by the vacuum planetary mixer and the feeding device, and the reaction raw material is formed into a core-shell structure in the reaction kettle at a reaction temperature of 600-700 degrees and a dynamic pressure for 10-12 hours. The graphene base is in line with the negative electrode material, and after the reaction is completed, the temperature is sent out through the discharging device, and the parameters and the production process are adjusted by the control center during production.

[0036] The specific production process is as follows:

[0037] 1. Get 1000ML of dispersed graphene oxide aqueous solution, the negative electrode material is nano-graphite and get qualit...

Embodiment 3

[0048] The production method described in the third embodiment is similar to that of the second embodiment, except that the negative electrode material is nanometer lithium titanate. In the first step of the heating and pressurizing stage, the heating temperature is 700 degrees within 25-30 minutes.

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Abstract

The invention relates to a production apparatus for a graphene-based composite negative electrode material. The production apparatus comprises a loading apparatus, a vacuum planetary stirrer arrangedon the downstream of the loading apparatus and a reaction kettle arranged on the downstream of the vacuum planetary stirrer, wherein the reaction kettle also comprises a discharging apparatus. The invention also provides a production method of a graphene-based composite negative electrode material for a lithium ion battery. The production method comprises the following steps: producing a graphene-based composite negative electrode material of a core-shell structure by utilizing the production for the graphene-based composite negative electrode material, producing a reaction raw material by virtue of the vacuum planetary stirrer, and forming the graphene-based composite negative electrode material of the core-shell structure from the reaction raw materials at the reaction temperature of 600to 700 DEG C and a dynamic pressure condition of 10 to 12 hours in the reaction kettle. By virtue of the production device and the production method, the problem of the lithium battery that the cyclelife of the battery is low can be solved, the key performance of the battery is improved, the internal resistance of the battery is reduced, and the heat dissipation problem of a battery cell when inhigh-magnification charging and discharging can be solved.

Description

technical field [0001] The invention relates to the technical field of production and preparation of novel battery materials, in particular to a production device and production method for a graphene-based composite negative electrode material. Background technique [0002] Lithium-ion batteries have brought revolutionary changes to the field of energy storage since their birth, due to their advantages of large specific energy, high operating voltage, low self-discharge rate, small size and light weight, and are widely used in various In portable electronic devices and electric vehicles, however, with the improvement of people's living standards, higher user experience has put forward higher requirements for lithium-ion batteries. Lighter weight, longer cycle life, larger capacity, longer use time, etc. [0003] In order to solve the above problems, it is necessary to find new electrode materials with better performance. The current commercial lithium-ion battery anode mate...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01M4/36H01M4/38H01M4/485H01M4/587H01M4/62H01M10/0525
CPCH01M4/366H01M4/386H01M4/485H01M4/587H01M4/62H01M4/625H01M10/0525Y02E60/10
Inventor 徐睿
Owner 福州鼎烯飞扬科技有限公司
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