A production device and production method for graphene-based composite negative electrode materials
A negative electrode material, graphene-based technology, applied in the field of production and preparation of new battery materials, can solve the problems of short battery cycle life, achieve the effect of improving cycle life, reducing internal resistance, and improving key performance
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Embodiment 1
[0029] A production device for graphene-based composite negative electrode material, comprising a feeding device, a vacuum planetary mixer arranged downstream of the feeding device, and a reaction kettle arranged downstream of the vacuum planetary mixer, and the reaction kettle also includes a discharging device.
[0030] In this embodiment, the feeding device includes an automatic device for aqueous solution of graphene oxide, an automatic feeding device for negative electrode materials, and an automatic pure water production device. After the three are connected in parallel, the raw materials of the composite negative electrode material are simultaneously sent to a vacuum planetary mixer for mixing to obtain reaction raw materials with uniform texture.
[0031] In this embodiment, a control center is also included, and the control center is connected to the feeding device, the vacuum planetary mixer, the reaction kettle and the discharging device. Parameters and production p...
Embodiment 2
[0034] This embodiment is a production method for producing a graphene-based composite negative electrode material with a core-shell structure by applying the production device for graphene-based composite negative electrode material described in Embodiment 1.
[0035] The reaction raw material is generated by the vacuum planetary mixer and the feeding device, and the reaction raw material is formed into a core-shell structure in the reaction kettle at a reaction temperature of 600-700 degrees and a dynamic pressure for 10-12 hours. The graphene base is in line with the negative electrode material, and after the reaction is completed, the temperature is sent out through the discharging device, and the parameters and the production process are adjusted by the control center during production.
[0036] The specific production process is as follows:
[0037] 1. Get 1000ML of dispersed graphene oxide aqueous solution, the negative electrode material is nano-graphite and get qualit...
Embodiment 3
[0048] The production method described in the third embodiment is similar to that of the second embodiment, except that the negative electrode material is nanometer lithium titanate. In the first step of the heating and pressurizing stage, the heating temperature is 700 degrees within 25-30 minutes.
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