A kind of piezoelectric ceramic and its preparation method and 3D printing piezoelectric ceramic device
A technology of piezoelectric ceramics and 3D printing, which is applied in ceramic forming machines, manufacturing tools, additive processing, etc., can solve the problems of low piezoelectric performance and low density of piezoelectric ceramics, achieve excellent density, improve electrical properties, Effect of improving density and electrical properties
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Embodiment 1
[0057] Step 1: Preparation of the first piezoelectric ceramic template grain
[0058] (1) Pure trioxide will be analyzed (Bi 2 O 3 ) And titanium dioxide (TiO 2 The molar ratio is 1: 1 mixed with butanone as a medium, ball milling 8h, and then mixed with mixed base at 120 ° C.
[0059] (2) The NaCl molten salt and the KCl molten salt were mixed with a molar ratio of 1: 1 to obtain a mixed molten salt, and then (1) obtained mixed base was added to the mixed molten salt, heated to 1000 ~ 1150 ° C, and after 1 hour after heat BI 4 Ti 3 O 12 . Bring the resulting BI 4 Ti 3 O 12 Batio 3 TiO 2 Mass moon is 1: 1: 1: 1 ~ 1: 1.1: 1.1 mix, Join Bacl 2 And mixed molten salt of KCl (bacl 2 The molar ratio of KCl is 1: 1), and the magnetic stirring is mixed and mixed, and the reaction is heated to 1000 ~ 1100 ° C, the temperature is about 1 hour, the reaction is obtained by Babi 4 Ti 4 O 15 Precursor.
[0060] (3) Put Babi 4 Ti 4 O 15 Precarrier and Baco 3 Mix, KCl was added as a melt salt, an...
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