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Control method for sigma-phase precipitation of ER316L austenitic stainless steel wire rods

An austenitic stainless steel, ER316L technology, applied in heat treatment process control, manufacturing tools, heat treatment equipment, etc., can solve the problems of billet corner cracking, low rolling speed, pitting corrosion resistance and crevice corrosion resistance. The effect of good drawing performance and optimized rolling process

Inactive Publication Date: 2018-11-06
CHANGSHU INSTITUTE OF TECHNOLOGY
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Problems solved by technology

But this will cause damage to the material properties. The reduction of the content of chromium equivalent elements will reduce the effect of pitting corrosion resistance and crevice corrosion resistance, while the increase of nickel equivalent elements will reduce the solubility of carbon in austenitic stainless steel, resulting in the precipitation of carbides. Tendency to increase, which is detrimental to the subsequent cold working properties of wire rod products
[0004] At present, there have been reports of special steel production lines successfully rolling austenitic stainless steel wire rods, but there are still problems such as low rolling speed, billet corner cracks, and poor surface quality. The reason is that the rolling parameters (including rolling temperature, rolling Form a deep understanding of the influence of σ phase precipitation and wire rod performance

Method used

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  • Control method for sigma-phase precipitation of ER316L austenitic stainless steel wire rods
  • Control method for sigma-phase precipitation of ER316L austenitic stainless steel wire rods
  • Control method for sigma-phase precipitation of ER316L austenitic stainless steel wire rods

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Embodiment

[0036] 1) Preparation of austenitic stainless steel ER316L forging billet

[0037] The austenitic stainless steel ER316L ingot was smelted in a 4.5t German ALD vacuum induction furnace, and its chemical composition is shown in Table 1. The steel ingot was forged into a billet after electroslag remelting, and the size after surface grinding was 140×140×1600mm.

[0038] Table 1

[0039]

[0040] 2) Solution heat treatment and high temperature compression treatment of test materials

[0041] The sampled material from the flying shear station in the rough rolling stage was processed into a solution heat treatment test sample with a size of 20×20×20mm, which was heated to a temperature of 850, 950, 1000, and 1100°C in a Nabertherm N31 / H box-type resistance furnace, respectively. Water quenching after 30 min of heat preservation. The material sampled at the flying shear station in the rough rolling stage was processed into a high-temperature compression test sample with a size...

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Abstract

The invention belongs to the field of metal material production and manufacture, and specifically discloses a control method for sigma-phase precipitation of ER316L austenitic stainless steel wire rods. According to the method, sigma-phase precipitation proportions of ER316L austenitic stainless steel wire rods are controlled through the cooperation of rolling temperature and strain rate in the process of producing and rolling wire rods, the rolling temperature is higher than 1000 DEG C, and the strain rate is lower than 40 s-1. A solid solution heat treatment method and a high-temperature compression experiment in the field of metal heat processing are adopted, so that the laws of influences, on second-phase precipitation behaviors, of ER316L austenitic stainless steel, of solid solutiontemperature and strain rate are discovered and grasped, optimum rolling temperature and spinning temperature are determined, and reasonable rough / intermediate rolling speed and pass deformation are determined at the same time, thereby optimizing the rolling process and carrying out high-speed rolling. According to the method, the surfaces and internal parts of the produced wire rods do not defects, the tissues focus on austenite grains, the sigma-phase content is smaller than 3% and is distributed in a dispersion manner, the tensile strength mean value is 640.2 MPa, the elongation mean value is 48.7%, and relatively good drawing performance is embodied.

Description

technical field [0001] The invention belongs to the field of production and manufacture of metal materials, and in particular relates to a control method for σ-phase precipitation of ER316L austenitic stainless steel wire rods. Background technique [0002] ER316L austenitic stainless steel wire rod is a high-quality ultra-low carbon welding material. The deposited metal has good low-temperature performance, pitting corrosion resistance, intergranular corrosion and stress corrosion resistance, so the welding wire made of this material is widely used in Petrochemical, nuclear power, cryogenic vessels and other fields. However, the rolling of this kind of wire rod is very different from that of ordinary carbon steel. It has the characteristics of high deformation resistance, thermal inhomogeneity, and large expansion coefficient under thermoplastic deformation. It often appears in high-wire rolling. Cracks on the surface or inside seriously affect the quality of the product. ...

Claims

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Application Information

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IPC IPC(8): C21D8/06C21D11/00C22C38/02C22C38/04C22C38/58C22C38/44C22C38/42
CPCC21D8/065C21D11/00C21D2211/001C21D2211/004C22C38/02C22C38/04C22C38/42C22C38/44C22C38/58
Inventor 董利明于照鹏姜巍左克生胡顺安焦红宇胡天润
Owner CHANGSHU INSTITUTE OF TECHNOLOGY
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