Tobacco moisturizer and preparation method and application thereof
A moisturizing agent, tobacco technology, applied in the direction of tobacco, tobacco preparation, tobacco treatment, etc., to achieve the effects of improving moisturizing quality and stability, reducing irritation, and improving aftertaste
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Embodiment 1
[0035] Preparation of tobacco humectant Uio-66 by solvothermal method:
[0036] 15mmol anhydrous ZrCl 4 Put it into a beaker, add 30ml of N,N'-dimethylamide, and then perform ultrasonic treatment for 30 minutes until it is completely dissolved. Add 15mmol terephthalic acid and 60ml N,N'-dimethylamide into the above solution, and continue to sonicate for 30 minutes until completely dissolved. The above mixed solution was transferred into a polytetrafluoroethylene reactor and reacted at 120°C for 24h. Filter out the solid product, wash it with 20ml of 60°C ethanol, dry it, transfer it to a conical flask, add 30ml N,N'-dimethylamide and stir to remove unreacted ligand. The above-mentioned product was filtered out, washed with 20ml of ethanol, dried and transferred to a reaction kettle, and then dried in an oven at 90°C for 12 hours. The solid product was obtained by centrifugation, and was centrifugally washed twice with 20 ml of ethanol and twice with 20 ml of acetone, and th...
Embodiment 2
[0037] Embodiment 2: Preparation of tobacco humectant Uio-66-NH by solvothermal method 2
[0038] 18mmol anhydrous ZrCl 4Put it into a beaker, add 30ml of N,N'-dimethylamide, and then perform ultrasonic treatment for 30 minutes until it is completely dissolved. Add 14mmol of 2-amino-terephthalic acid and 50ml of N,N'-dimethylamide into the above solution, and continue ultrasonic treatment for 30 minutes. The above mixed solution was transferred into a polytetrafluoroethylene reactor and reacted at 120°C for 24h. Filter out the solid product, wash it with 20ml of 60°C ethanol, dry it, transfer it to a conical flask, add 30ml N,N'-dimethylamide and stir to remove unreacted ligand. The above-mentioned product was filtered out, washed with 20ml of ethanol, dried and transferred to a reaction kettle, and then dried in an oven at 90°C for 12 hours. The solid product was obtained by centrifugation, and was centrifugally washed twice with 20 ml of ethanol and twice with acetone, a...
Embodiment 3
[0040] Embodiment 3: the mensuration of the dynamic content of moisture added in tobacco by tobacco humectant Uio-66
[0041] Dissolve the tobacco humectant Uio-66 prepared in Example 1 in a mixed solvent of 1,2-propanediol and glycerin, and add it to shredded tobacco according to the amount of humectant at 0.2%, so as to add an equal amount of alcohol mixed solvent but not Cut tobacco samples containing humectant Uio-66 were used as blank control. Then the shredded tobacco sample was placed in a DVS dynamic moisture adsorption instrument with a temperature of 22° C. and a relative humidity of RH46%, to measure the dynamic moisture content. The results are shown in Table 1 and Figure 4 shown. From Figure 4 It can be seen that the adsorption-desorption curve of Uio-66 has a large adsorption hysteresis. Under a certain pressure, it has a certain degree of adsorption and retention of water, and the maximum adsorption capacity can reach 14%, which has a good water adsorption ...
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