Preparation method of low-carbon mixed gas hydrate explosion inhibitor
A technology of mixed gases and hydrates, applied in chemical instruments and methods, and other chemical processes, can solve the problems of strong greenhouse effect of pure carbon dioxide anti-explosion agents, poor anti-explosion effect, and no public reports of anti-explosion materials. To achieve the effect of abundant raw materials, good explosion suppression effect and low cost
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Embodiment 1
[0019] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0020] (1) Preparation of hydration agent:
[0021] adding the inorganic salt silicon dioxide into the water so that the mass content of the silicon dioxide is 0.05mol / L;
[0022] (2) Preparation of inert mixed gas:
[0023] The inert mixed gas is composed of a mixture of 10% carbon dioxide, 90% nitrogen and argon, and the volume ratio of nitrogen and argon is 1:1;
[0024] (3), mixed reaction:
[0025] Fill the inert mixed gas into the hydration agent, make the pressure reach 7MPa, and react at 3°C for 150 minutes to form mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction below -10°C into particles with a particle size of less than 1.0mm Hydrate powder and serve.
Embodiment 2
[0027] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0028] (1) Preparation of hydration agent:
[0029] Add the inorganic salt NaCl to the dry water so that the mass content of NaCl is 0.01mol / L;
[0030] (2) Preparation of inert mixed gas:
[0031] The inert mixed gas is composed of a mixture of 7% carbon dioxide, 93% nitrogen and argon by volume, and the volume ratio of nitrogen to argon is 1:3;
[0032] (3), mixed reaction:
[0033] Fill the inert mixed gas into the hydration agent, make the pressure reach 6MPa, and react at 1°C for 160 minutes to generate mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction into particles with a particle size of less than 1.0mm at a temperature below -10°C Hydrate powder and serve.
Embodiment 3
[0035] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0036] (1) Preparation of hydration agent:
[0037] adding the inorganic salt MgF into the dry solvent water, so that the mass content of the inorganic salt is 0.03mol / L;
[0038] (2) Preparation of inert mixed gas:
[0039] The inert mixed gas is composed of a volume ratio: 14% of carbon dioxide, 86% of a mixture of nitrogen and argon, and the nitrogen and argon are in any volume ratio;
[0040] (3), mixed reaction:
[0041] Fill the inert mixed gas into the hydration agent, make the pressure reach 8MPa, react at -10-5°C for 100-240min to form mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction below -10°C into granules Hydrate powder with a diameter less than 1.0mm is ready.
[0042] As can be seen from the above, the present invention is a preparation method of a low-carb...
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