Silicon-based hardmask
A group, hydrocarbon-based technology, applied in the field of semiconductor device manufacturing, can solve problems such as the incompatibility of resist patterns and the like
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example 1
[0051] Example 1. Addition of phenyltrimethoxysilane (PTMS, 12.7g), vinyltrimethoxysilane (VTMS, 4.75g), bis(triethoxysilyl)ethylene (BSE, 83.5g) and isopropanol over 10 minutes (80 g) was added HCl 0.1 N (0.265 g) and isopropanol (80 g) dissolved in water (29.45 g) and stirred for a further 50 minutes. The reaction mixture was heated to 69 °C for 24 hours, cooled to room temperature, diluted with PGEE (300 g), and the volatiles were removed under reduced pressure. The concentration of the mixture was adjusted to 10 wt% solids by adding PGEE to give a clear solution with a molecular weight of 27,100 relative to polystyrene standards.
example 2
[0053] Example 2. Addition of phenyltrimethoxysilane (PTMS, 6.35g), vinyltrimethoxysilane (VTMS, 9.50g), bis(triethoxysilyl)ethylene (BSE, 83.5g) and isopropanol over 10 minutes (80 g) was added HCl 0.1 N (0.265 g) and isopropanol (80 g) dissolved in water (29.5 g) and stirred for a further 50 minutes. The reaction mixture was heated to 69 °C for 18 hours, cooled to room temperature, diluted with PGEE (300 g), and the volatiles were removed under reduced pressure. The concentration of the mixture was adjusted to 10 wt% solids by adding PGEE to give a clear solution with a molecular weight of 19,300 relative to polystyrene standards.
example
[0057] Examples of formulations. The procedure of Formulation Example 1 was repeated using the components and amounts reported in Table 1 to prepare Formulation Example 2 and Comparative Formulation Examples 1 to 3. In Table 1, component 1 refers to the polymer added to each formulation, component 2 is a 0.1 wt% solution of tetrabutylammonium chloride in PGEE, component 3 is PGEE, and component 4 is lactic acid ethyl ester and component 5 is methyl 2-hydroxyisobutyrate.
[0058] Table 1
[0059]
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