Pressure-sensitive adhesive and preparation method thereof, aluminum coated tape and use thereof
A pressure-sensitive adhesive and tape technology, applied in pressure-sensitive films/sheets, adhesives, adhesive types, etc., can solve problems such as easy transfer of pressure-sensitive adhesives, problems of residual adhesive not being perfectly solved, and residual adhesives, etc. Beautiful product, good stickiness, and the effect of solving residual glue
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[0055] According to another aspect of the present invention, the preparation method of the above-mentioned pressure-sensitive adhesive comprises the steps of:
[0056] (a) Mix part of the soft monomer, all the hard monomer and the functional monomer, stir and heat, then add part of the initiator and part of the solvent to react;
[0057] (b) add remaining soft monomer to the mixture obtained in step (a) to react, heat up and react, add remaining initiator and part of solvent, keep warm;
[0058] (c) adding remaining solvent to the mixture obtained in step (b) for dilution to obtain a pressure-sensitive adhesive.
[0059] The preparation method of the pressure-sensitive adhesive in the present invention is simple and highly controllable. The product with a high glass transition temperature and the product with a low glass transition temperature are connected together to form a substance, which achieves molecular-level dispersion and dispersion effect. Well, the pressure-sensit...
Embodiment 1
[0083] A pressure-sensitive adhesive mainly prepared from the following components in parts by mass:
[0084] 25 parts of n-pentyl acrylate, 30 parts of isopropyl methacrylate, 3 parts of methacrylic acid, 0.8 parts of lauroyl peroxide and 40 parts of butyl acetate.
[0085] The preparation method of described pressure-sensitive adhesive comprises the following steps:
[0086] (a) Mix 20 parts of n-pentyl acrylate, 30 parts of isopropyl methacrylate and 3 parts of methacrylic acid, stir and heat to a temperature of 75°C, then add 0.4 parts of lauroyl peroxide and 4.5 parts of solvent, and react 120min;
[0087] (b) Add 5.5 parts of n-pentyl acrylate to the mixture obtained in step (a) to react for 30 minutes, heat up to 98°C and react for 30 minutes, add 0.4 parts of lauroyl peroxide and 4 parts of butyl acetate, and keep warm for 180 minutes;
[0088] (c) adding 30 parts of butyl acetate to the mixture obtained in step (b) for dilution to obtain a pressure-sensitive adhesiv...
Embodiment 2
[0092] A pressure-sensitive adhesive mainly prepared from the following components in parts by mass:
[0093] 75 parts of isooctyl acrylate, 5 parts of vinyl acetate, 10 parts of acrylic acid, 0.05 parts of benzoyl peroxide and 65 parts of ethyl acetate.
[0094] The pressure-sensitive adhesive is mainly prepared by the following method:
[0095] (a) Mix 40 parts of isooctyl acrylate, 5 parts of vinyl acetate and 10 parts of acrylic acid, stir and heat to a temperature of 90°C, then add 0.025 parts of benzoyl peroxide and 6 parts of ethyl acetate, and react for 60 minutes;
[0096] (b) Add 35 parts of isooctyl acrylate to the mixture obtained in step (a), react for 60 minutes, heat up to 90° C. for 30 minutes, add 0.025 parts of benzoyl peroxide and 10 parts of ethyl acetate, and keep warm for 120 minutes;
[0097] (c) adding 49 parts of ethyl acetate to the mixture obtained in step (b) for dilution to obtain a pressure-sensitive adhesive.
[0098] Wherein, the stirring spee...
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