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105 results about "Lauroyl peroxide" patented technology

LAUROYL PEROXIDE is a white solid with a faint soapy odor. Less dense than water and insoluble in water.Hence floats on water.Melting point 49°C. Toxic by ingestion and inhalation.

Macroporous strong alkaline carbon nanotube composite ion exchange resin and preparation method thereof

The invention relates to a macroporous strong alkaline carbon nanotube composite ion exchange resin and a preparation method thereof, and aims to solve problems of weak heat resistance and weak swelling resistance of an ion exchange resin in a prior art. The macroporous strong alkaline carbon nanotube composite ion exchange resin comprises the following components: (1) 40-65% of monomer; (2) 3-10% of copolymerization monomer; (3) 0.1-10% of nano material; and (4) 0.1-2% of initiator. The monomer is at least one selected from p-chloromethyl styrene, 4-(3-chloropropyl) styrene, 4-(3-bromopropyl) styrene, 4-(4-chlorobutyl) styrene, 4-(4-brombutyl) styrene, 4-(5-chloroamyl) styrene and 4-(5-bromoamyl) styrene; the copolymerization monomer is at least one selected from EGDMA, dipropenyl benzene, divinyl phenyl methane and divinyl benzene; the nano material is at least one selected from multi-wall carbon nanotube, single arm carbon nanotube and fullerene of C60 or C70; the initiator is at least one selected from benzoyl peroxide, azodiisobutyronitrile, lauroyl peroxide and cumyl hydroperoxide. The invention also provides a preparation method of the macroporous strong alkaline carbon nanotube composite ion exchange resin. The above technical scheme well solves the problems and can be applied to industrial production of ethylene oxide catalytic hydration.
Owner:CHINA PETROLEUM & CHEM CORP +1

Temperature-sensitive swelling microcapsule anti-gas-channeling agent and anti-gas-channeling cement slurry system

ActiveCN106947447AGas volume controllableStable performance on the groundDrilling compositionMicroballoon preparationCross-linkWater baths
The present invention discloses a temperature-sensitive swelling microcapsule anti-gas-channeling agent and an anti-gas-channeling cement slurry system. The temperature-sensitive expansion microcapsule anti-gas-channeling agent preparation method comprises: adding 3-4 parts of acrylonitrile, 0.4-0.5 part of methyl acrylate and 2-3 parts of methyl methacrylate to a beaker, adding 1-2 parts of lauroyl peroxide as an initiator, 10-30 parts of a low boiling point solvent as a foaming agent, and 0.1-0.2 part of 1, 4-butanediol dimethacrylate as a cross-linking agent, carrying out stirring dissolving, transferring into a glass reaction kettle, adding 20-25 parts of nano-silica as a dispersant and 300-350 parts of deionized water, carrying out a constant temperature water bath reaction for 20-24 h at a temperature of 60-70 DEG C under nitrogen protection, cooling, washing, and drying. The anti-gas-channeling cement slurry system comprises 100 parts of oil well cement, 1.5-2 parts of a fluid loss additive, 2-3 parts of a dispersant, 0.1-1 part of an anti-gas-channeling agent, 0-3 parts of a retarder, 0.2 part of a defoamer, 0-50 parts of a density adjuster, and 44 parts of water. According to the present invention, with the temperature-sensitive expansion microcapsule anti-gas-channeling agent and the anti-gas-channeling cement slurry system, the cement stone volume shrinkage can be effectively made up, the stratum fluid can be sealed, the channeling can be prevented, the occurrence of the annulus pressure phenomenon can be prevented, and the service life of the oil well can be prolonged.
Owner:SOUTHWEST PETROLEUM UNIV

Anti-tear cable material used for high-speed railway motor train unit and preparation method of anti-tear cable material

The invention discloses an anti-tear cable material used for a high-speed railway motor train unit and a preparation method of the anti-tear cable material. The anti-tear cable material used for the high-speed railway motor train unit comprises the following raw materials in parts by weight: 67 to 89 parts of polyurethane rubber, 22 to 36 parts of styrene-butadiene rubber, 15 to 25 parts of thermoplastic polyester elastic bodies, 4 to 8 parts of vinyl silicone oil, 17 to 26 parts of fumed silica, 3 to 6 parts of cadmium carbonate, 2 to 3 parts of lauroyl peroxide, 1.5 to 2.5 parts of triallyl isocyanurate, 1 to 2 parts of ammonium benzoate, 3 to 5 parts of poly-alpha-olefin, 5 to 10 parts of tert-butyl phenolic tackifying resin, 2 to 4 parts of triethylhexanoin, 10 to 15 parts of methylpentachlorostearate, 14 to 18 parts of carbon nano tubes, 10 to 15 parts of a diopside powder, 1 to 2 parts of 4,4'-dithiodimorpholine, 0.5 to 1 part of P-tert-butylphenol, and 20 to 25 parts of a composite flame retardant. The cable material provided by the invention combines the advantages of the raw materials such as the polyurethane rubber, the styrene-butadiene rubber, and the thermoplastic polyester elastic bodies, the tearing strength of a conventional cable material is improved, and the cable material is enabled to have excellent tear resistance, has the effect of bearing relatively great mechanical external force, and has the advantages of excellent chemical stability, heat resistance and age resistance, and long service life.
Owner:ANHUI KANGLIYA CO LTD

Medical anti-microbial dressing and preparation method thereof

The invention discloses medical anti-microbial dressing and a preparation method thereof. The medical anti-microbial dressing comprises a bacterial cellulose membrane, nano-silver, water soluble chitosan, sodium alginate, polyvinylpyrrolidone and a composite cross-linking agent, wherein the composite cross-linking agent is prepared by compounding lauroyl peroxide, methacrylic acid-2-hydroxyethyl ester and 2-ethyl-4-methylimidazole. The preparation method comprises the steps that the sodium alginate is added into deionized water and is heated and mixed evenly to obtain a mixed liquid I; the polyvinylpyrrolidone is dissolved in ethylene glycol, the nano-silver is added, temperature rise is kept for a certain time, filtration is performed, solid matter is cleaned with deionized water and then is dried and smashed to obtain a material I; the water soluble chitosan and the material I are added into the mixed liquid I to be mixed evenly, the bacterial cellulose membrane is added, the composite cross-linking agent is added after the temperature rise is kept for a certain time, and temperature rise reaction is performed to obtain the anti-microbial dressing. The anti-microbial dressing has good anti-microbial dressing, bleeding-stop and wound surface healing effects and can be better applied to the medical field.
Owner:JIANGSU LANWAN BIOTECH

Low-temperature and crack resistant chlorinated polyethylene cable material and preparation method thereof

The invention discloses a low-temperature and crack resistant chlorinated polyethylene cable material and a preparation method thereof. The cable material is prepared from, by weight, 60-80 parts of chlorinated polyethylene, 26-30 parts of low-phenyl silicone rubber, 30-40 parts of a tetrafluoroethene-perfluoromethyl vinyl ether copolymer, 8-12 parts of stearic acid, 7-9 parts of magnesium oxide, 5-8 parts of di-n-hexyl azelate, 25-35 parts of di(butylcarbitol) adipate, 5-7 parts of bis-(gamma-triethoxysilylpropyl)tetrasulfide, 6-8 parts of 2-imidazolidinethione, 1-2 parts of lauroyl peroxide, 6-8 parts of stannous chloride and 25-35 parts of silicon oxynitride. The low-phenyl silicone rubber and the tetrafluoroethene-perfluoromethyl vinyl ether copolymer added in the invention have excellent low-temperature resistance, and can be combined with the chlorinated polyethylene to form one body in order to effectively improve the low-temperature resistance of the chlorinated polyethylene cable material; and the di-n-hexyl azelate and di(butylcarbitol) adipate added in the invention enhance the cold resistance of the material, and can cooperate with the silicon oxynitride and calcium titanate nano-fibers to enhance the crack resistance of the material.
Owner:WENZHOU RENHE CULTURAL ORIGINALITY CO LTD

High-tensile-strength power transmission cable

The invention discloses a high-tensile-strength power transmission cable comprising four circular conductive units and one hollow micro-tube used for embedding of an optical fiber. Each conductor unit comprises a conductive wire core and an insulating layer which wraps the external surface of the conductive wire core, wherein the conductive wire core and the insulating layer are arranged from inside to outside in turn. The four circular conductive units are arranged along the circumferential direction of the hollow micro-tube. A wrapping tape wraps the external surface of the four circular conductive units. The external surface of the wrapping tape is wrapped by an internal sheath layer. An armored layer wraps the external surface of the internal sheath layer. The external surface of the armored layer is wrapped by an external sheath layer. Maleic anhydride grafted amorphous polyolefin is prepared in a way that amorphous polyolefin, maleic anhydride, lauroyl peroxide and ethylene bisstearamide are put into a double-screw extruder according to the proportion of 100:0.4-3:0.03-1:0.1-0.3 through graft polymerization The situation that common air blowing laying is only suitable for parallel laying can be overcome, air pressure of the air compressor can be increased and finally the bending air blowing laying function can be realized.
Owner:JIANGSU HENGTONG POWER CABLE

A kind of aging oil demulsifier and preparation method thereof

The invention relates to an ageing oil demulsifier and a preparation method thereof, and belongs to the technical field of petroleum processing. The ageing oil demulsifier comprises mixed acid, a demulsifier monomer and an initiator, wherein the mixed acid consists of acrylic acid and maleic anhydride based on the molar ratio of (1-3): (0.5-1.5); the molar ratio of the mixed acid to the demulsifier monomer, namely, alkyl phenolic resin-polyoxyethylene polyoxypropylene ether, is (0.5-1.7): (0.5-1.5); the initiator, namely, lauroyl peroxide, accounts for 8 to 12% of the mass of the mixed acid. The preparation method comprises the following processes: adding the initiator, namely lauroyl peroxide to mixed acid and demulsifier monomer, namely alkyl phenolic resin-polyoxyethylene polyoxypropylene ether; polymerizing for 1 to 4 hours under a temperature of 70 to 100 DEG C; heating to reach 100 to 150 DEG C; esterifying for 3 to 7 hours to obtain the ageing oil demulsifier. The ageing oil demulsifier has the characteristics of being simple in components, simple in process, convenient, fast and efficient to prepare, low in cost, small in dosage, small in toxic and side effects, wide in application scope, good in demulsifying effect, etc.
Owner:河南鼎源化工科技有限公司

Preparation method of 2-phosphonothioflavone compound

The invention discloses a preparation method of a 2-phosphonothioflavone compound, which is a method for synthesizing the 2-phosphonothioflavone compound by utilizing water phase visible light catalysis. According to the invention, tetrazole m-dibenzonitrile (4-CzIPN) is used as a photosensitizer, lauroyl peroxide is used as an oxidizing agent, 2-methylthiophenyl propynone and diarylphosphine oxide are used as initial raw materials, water is used as a solvent, and under the protection of nitrogen, an illumination reaction is carried out at room temperature for 24 hours to obtain a target product. The invention provides a method for preparing the 2-phosphonothioflavone compound through water-phase photocatalysis of radical series cyclization reaction for the first time. Compared with a traditional method, according to the method, traditional precious metal (such as ruthenium and iridium) organic photosensitizers do not need to be used, the 2-phosphonothioflavone compound is rapidly andefficiently synthesized under the extremely mild and environment-friendly reaction condition, and the method has huge potential application value in the fields of environment-friendly synthetic chemistry, heterocyclic compound construction through photocatalytic reaction and pharmaceutical and chemical engineering.
Owner:XINYANG AGRI & FORESTRY UNIV

Cardanol grafted high-density polyethylene synthesized by reactive extrusion and application thereof in bamboo-plastic composite material

The invention discloses cardanol grafted high-density polyethylene synthesized by reactive extrusion and application thereof in a bamboo-plastic composite material. A method comprises the following steps: a) a step of preparing the cardanol grafted high-density polyethylene, namely a step of dissolving a compound initiator which includes lauroyl peroxide (LPO) and dibenzoyl peroxide (BPO) into cardanol, adding the mixture into high-density polyethylene (HDPE) resin, uniformly stirring and mixing the mixture at a high speed, then performing extrusion by using an extruder, and carrying out watercooling and granulation to obtain the cardanol grafted high-density polyethylene synthesized by reactive extrusion; and b) a step of application of the cardanol grafted high-density polyethylene, namely a step of uniformly stirring and mixing the cardanol grafted high-density polyethylene prepared in the step a) with bamboo powder and plastic at a high speed, and performing extrusion, injection molding or hot press molding to obtain the bamboo-plastic composite material. The cardanol grafted high-density polyethylene prepared by reactive extrusion utilizing the composite initiator has the advantages of stable free radical concentration, low processing temperature, no need of purification of the product and high grafting rate, and can prevent thermal degradation of the bamboo powder when used as a plastic matrix or a coupling agent of the bamboo-plastic composite material.
Owner:QUANGANG PETROCHEM RES INST OF FUJIAN NORMAL UNIV

A kind of preparation method and application of amphiphilic polymer

The invention relates to a preparation method and application of an amphiphilic polymer. The problems that an insoluble drug is poor in absorption and treatment effect and low in bioavailability and has more adverse effects can be effectively solved. According to the technical scheme, the amphiphilic polymer is formed by connecting a N-vinyl pyrrolidone monomer with maleic acid Guerbet eicosanol monoester, the maleic acid Guerbet eicosanol monoester is generated through esterification of maleic anhydride and 2-octyl-dodecane Guerbet alcohol, a free radical polymerization reaction is conducted in n-heptane by taking lauroyl peroxide as an initiating agent and taking N-vinyl pyrrolidone and the maleic acid Guerbet eicosanol monoester as monomers, and then the amphiphilic polymer is obtained. According to the preparation method and application of the amphiphilic polymer, the insoluble drug is embedded into polymeric micelles by taking the amphiphilic polymer as a carrier material to prepare an insoluble drug-loaded micelle injection, a very good tumor inhibiting effect is achieved, the toxicity is low, the water solubility of the insoluble drug can be enhanced, the bioavailability of the drug can be improved, and the toxic and side effects of the drug can be reduced.
Owner:ZHENGZHOU UNIV

Preparation method of chitosan modified amphiprotic crosslinked starch sludge dehydrating agent

The invention discloses a preparation method of a chitosan modified amphiprotic crosslinked starch sludge dehydrating agent and belongs to the technical field of dehydrating agent preparation. The preparation method comprises the following steps of adding methacryloyloxyethyl trimethyl ammonium chloride, hydrochloric acid, ammonium sulfate and azobisisobutryamide chloride into prepared crosslinked starch; performing a stirring reaction to obtain cation crosslinked starch; then preparing amphiprotic crosslinked starch; then adding chitosan, lauroyl peroxide and the azobisisobutryamide chloride into the amphiprotic crosslinked starch; obtaining chitosan modified amphiprotic crosslinked starch after a reaction; carrying out reduced pressure distillation and drying to obtain the chitosan modified amphiprotic crosslinked starch sludge dehydrating agent. Examples prove that according to the preparation method, the problem of resource exhaustion is solved when the cost is reduced; in addition, in the preparation process, the environment is not polluted, the prepared sludge dehydrating agent can self-degrade under the nature conditions, the water content of sludge can be lowered from original 60 percent to below 10 percent after the chitosan modified amphiprotic crosslinked starch sludge dehydrating agent is used, and the dehydrating efficiency is very dramatic.
Owner:郭舒洋

High-temperature-resistant anti-aging resin anchoring agent

The invention discloses a high-temperature-resistant anti-aging resin anchoring agent, belonging to the technical field of roadway support materials. According to the invention, montmorillonite is crushed, then impregnated with hydrochloric acid and finally undergoes filtering and separation so as to obtain filter residues; the filter residues are mixed with moss pulp prepared from Polytrichum alpinum for culture, then the cultured filter residues undergo oscillation together with a sodium silicate solution, and the obtained mixture is subjected to filtering and separating so as to obtain a filter cake; the obtained filter cake and hydrochloric acid are subjected to oscillation, dipping and heating reaction, and then filtering and separating are carried out so as to obtain a pre-modified filter cake; the pre-modified filter cake is carbonized and then undergo mixing and grinding together with natural resin so as to obtain a modified self-made high-temperature-resistant anti-aging filling material; the filling material, bisphenol A type unsaturated polyester resin, dimethylaniline and tetrachlorobenzoquinone are uniformly mixed to obtain a component A; lauroyl peroxide, dibenzoyl peroxide and water are uniformly mixed to obtain a component B; and in use, the component A and the component B are mixed so as to obtain the high-temperature-resistant anti-aging resin anchoring agent. The high-temperature-resistant anti-aging resin anchoring agent has excellent ageing resistance, can maintain high compressive strength and anchoring force under a high temperature condition and exerts good supporting effect in a severe underground environment.
Owner:常州瑞坦商贸有限公司

Wear-resisting and shock-resisting polypropylene material for inner barrel of washing machine and preparation method thereof

The invention discloses a wear-resisting and shock-resisting polypropylene material for an inner barrel of a washing machine and a preparation method thereof. The wear-resisting and shock-resisting polypropylene material is prepared from, by weight, 90-110 parts of polypropylene, 20-30 parts of acrylic acid, 3-5 parts of lauroyl peroxide, 8-10 parts of xylene, 40-50 parts of acetone, 20-25 parts of ethylene-trifluorochlor oethylene copolymer, 5-7 parts of tetra-(2-ethylhexyl)pyromellitate, 7-9 parts of cotton stalk bark fiber, 4-6 parts of aerosol, 5-7 parts of zinc stearate, 2-4 parts of dibasic lead stearate, 6-8 parts of polyethylene wax, 8-10 parts of epoxy linseed oil, 15-20 parts of sub-white corundum fine powder, 10-12 parts of hollow glass bead, 7-9 parts of graphene oxide, and 5-7 parts of nepheline powder, and so on. Through blending and modifying polypropylene resin by ethylene- trifluorochlor oethylene copolymer, the mechanical strength and wear resistance of the composite polypropylene material are improved, and the corrosive resistance and creep resistance are also improved; acrylic acid is grafted with modified polypropylene, so as to improve the compatibility between the mixed filler consisting of sub-white corundum fine powder, graphene oxide and others, and organic resin, promote the wear resistance, shockproof and anti-impact performances of the composite materials.
Owner:杨烨
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