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Manufacturing method of corrosion-resistant high-flame-retardant silicon core pipe

A production method and high flame retardant technology are applied in the field of production of corrosion-resistant and high-flame-retardant silicon core tubes, which can solve the problems of inappropriate production methods, layer-by-layer separation, and high product production costs.

Pending Publication Date: 2019-01-04
RONGCHENG PIPE IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Silicon core tube is a new type of composite tube with silica gel solid lubricant on the inner wall. It has good sealing performance, chemical corrosion resistance and low engineering cost. It is widely used in optical cable communication network systems such as highways and railways. However, the existing The formula of the silicon core tube is unreasonable, so that the mixing degree of the raw materials is not high, the corrosion resistance of the final product is very poor, and the flame retardancy has been difficult to be greatly improved. In addition, the production method is not appropriate, which makes the reliability of the silicon core tube made Low, it is easy to have the problem of layer-by-layer detachment, and the production cost of the product is also high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] The manufacturing method of the corrosion-resistant and highly flame-retardant silicon core tube of the present embodiment comprises the following steps:

[0019] A. Mix 230 parts of n-decane and 35 parts of dodecene at room temperature and stir evenly, heat up to 145°C and react for 1 hour, then cool down to 100°C, and then add 135 parts of methyl hydrogen Silicone oil, heat up to 130°C, and continue to react for 3 hours to obtain olefin-modified silicone oil;

[0020] B, 6 parts of graphene, 3 parts of nano-bentonite and 2 parts of nano borides are put into a grinder for grinding, the grinding time is 1 hour, then 3 parts of triethyl phosphate, 2 parts of The chlorinated paraffin is added into the mixer for stirring, the stirring speed is 700 rpm, the stirring time is 1 hour, the stirring temperature is 100°C, and finally the ground and stirred product is mixed and stirred, and the mixing and stirring time is 2 hours;

[0021] C. Add 25 parts of hydroxystearic acid a...

Embodiment 2

[0025] The manufacturing method of the corrosion-resistant and highly flame-retardant silicon core tube of the present embodiment comprises the following steps:

[0026] A. Mix 275 parts of n-decane and 40 parts of dodecene at room temperature and stir evenly, heat up to 150°C and react for 2 hours, then cool down to 105°C, and then add 140 parts of methyl hydrogen Silicone oil, heat up to 135°C, and continue to react for 4 hours to obtain olefin-modified silicone oil;

[0027] B, 7 parts of graphene, 4 parts of nano-bentonite and 3 parts of nano-borides are put into a grinder for grinding, and the grinding time is 1 hour, then 4 parts of triethyl phosphate, 2 parts of The chlorinated paraffin is added into the mixer for stirring, the stirring speed is 800 rpm, the stirring time is 2 hours, the stirring temperature is 110°C, and finally the ground and stirred product is mixed and stirred, and the mixing and stirring time is 3 hours;

[0028] C. Add 28 parts of hydroxystearic ...

Embodiment 3

[0033] The manufacturing method of the corrosion-resistant and highly flame-retardant silicon core tube of the present embodiment comprises the following steps:

[0034] A. Mix 320 parts of n-decane and 45 parts of dodecene at room temperature and stir evenly, heat up to 165°C and react for 2 hours, then cool down to 110°C, and then add 145 parts of methyl hydrogen Silicone oil, heat up to 140°C, and continue to react for 5 hours to obtain olefin-modified silicone oil;

[0035] B, 8 parts of graphene, 5 parts of nano-bentonite and 4 parts of nano-borides are put into a grinder for grinding, and the grinding time is 2 hours, then 5 parts of triethyl phosphate, 3 parts of The chlorinated paraffin is added into the mixer for stirring, the stirring speed is 900 rpm, the stirring time is 2 hours, the stirring temperature is 120°C, and finally the ground and stirred product is mixed and stirred, and the mixing and stirring time is 3 hours;

[0036] C. Add 30 parts of hydroxystearic...

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PUM

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Abstract

The invention discloses a corrosion-resistant high-flame-retardant silicon core pipe which is prepared from, by weight, 230-320 parts of n-paraffin hydrocarbon, 195-225 parts of high-density polyethylene, 35-45 parts of dodecene, 135-145 parts of methyl hydrogen silicone oil, 25-30 parts of hydroxy stearic acid, 75-85 parts of polyolefin resin, 10-12 parts of color master batches, 6-8 parts of graphene, 3-5 parts of sodium-based bentonite, 2-4 parts of polyvinyl alcohol, 1-2 parts of zinc naphthenate, 2-4 parts of nano-boride, 3-4 parts of polyurethane, 1-2 parts of polyacrylic acid, 3-5 partsof triethyl phosphate, 2-3 parts of chlorinated paraffin, 1-2 parts of antioxidants, 5-7 parts of glycerol and 7-9 parts of deionized water. By the aid of the formula, the corrosion-resistant high-flame-retardant silicon core pipe has high wear resistance, high flame resistance and high reliability, overall consistency is improved, and the problem of delaminating is avoided. In addition, variousreactants with different functions are added, so that reaction is sufficient, various composition effects of the pipe are maximally achieved, and finally, the pipe is quite high in overall performance.

Description

technical field [0001] The invention relates to a production technology of a silicon core tube, in particular to a production method of a corrosion-resistant and highly flame-retardant silicon core tube. Background technique [0002] Silicon core tube is a new type of composite tube with silica gel solid lubricant on the inner wall. It has good sealing performance, chemical corrosion resistance and low engineering cost. It is widely used in optical cable communication network systems such as highways and railways. However, the existing The formula of the silicon core tube is unreasonable, so that the mixing degree of the raw materials is not high, the corrosion resistance of the final product is very poor, and the flame retardancy has been difficult to be greatly improved. In addition, the production method is not appropriate, which makes the reliability of the silicon core tube made Low, it is easy to have the problem of layer-by-layer separation, and the production cost of...

Claims

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Application Information

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IPC IPC(8): C08L23/00C08L83/07C08L33/00C08L91/06C08L29/04C08K3/04C08K3/34C08K3/38C08K5/521C08K5/098C08K5/053
CPCC08L23/00C08L2205/035C08L2203/18C08L2201/02C08L83/04C08L33/00C08L91/06C08L29/04C08K3/042C08K3/346C08K3/38C08K5/521C08K5/098C08K5/053
Inventor 朱加荣虞敏
Owner RONGCHENG PIPE IND
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