A kind of insulating gasket and its preparation method and lithium battery
A technology of insulating gaskets and macroporous materials, applied in the field of energy storage, can solve problems such as uneven infiltration, achieve good cycle consistency, long service life, and increase the effect of liquid storage space
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Embodiment 1
[0060] The present embodiment adopts the following method to prepare insulating pads:
[0061] (1) Mix ethyl orthosilicate, poly-N-vinylpyridine, polystyrene-b-polyacrylic acid and ammonia water in water, heat and react at 60°C for 2h, centrifuge after reaction, and heat the obtained solid at 580°C The sintering is carried out at a temperature of 6 hours to obtain porous silica.
[0062] (2) Polyethylene terephthalate (PET) with a mass ratio of 3.7:6.3 and the porous silica described in step (1) are melt-mixed at 200° C., the time of melt-mixing is 110 min, and the melt-mixing It is accompanied by stirring, and after the mixing is completed, it is extruded under a pressure of 20MPa, and the extruded product is cut, and the pole hole and / or the lower liquid hole are made by die-cutting to obtain the insulation gasket.
[0063] The insulating gasket obtained in this embodiment is composed of a polyethylene terephthalate base material and porous silica dispersed in the base mat...
Embodiment 2
[0068] The present embodiment adopts the following method to prepare insulating pads:
[0069] (1) Mix ethyl orthosilicate, poly-N-vinylpyridine, polystyrene-b-polyacrylic acid and ammonia water in water, heat and react at 50°C for 3 hours, and separate solid and liquid after the reaction. The sintering is carried out at ℃, and the sintering time is 7 hours to obtain porous silica.
[0070] (2) The polyethylene terephthalate with a mass ratio of 3:6.3 and the porous silica described in step (1) were melt-mixed at 160° C., and the time of melt-mixing was 40 minutes. There is stirring, and after the mixing is completed, it is extruded under a pressure of 10 MPa, and the extruded product is cut, and the ear hole and / or the lower liquid hole are made by die cutting to obtain the insulating gasket.
[0071] The insulating gasket obtained in this embodiment is composed of a polyethylene terephthalate base material and porous silica dispersed in the base material, and the polyethyle...
Embodiment 3
[0074] The present embodiment adopts the following method to prepare insulating pads:
[0075] (1) Mix ethyl orthosilicate, poly-N-vinylpyridine, polystyrene-b-polyacrylic acid and ammonia water in water, heat and react at 70°C for 1.5h, and separate the solid and liquid after the reaction. Carry out sintering at 600° C. for 5 hours to obtain porous silicon dioxide.
[0076] (2) Melt and mix polypropylene (PP) with a mass ratio of 5:6.3 and the porous silica described in step (1) at 265°C, the time for melt mixing is 180min, while stirring and mixing After completion, it is extruded under a pressure of 35 MPa, and the extruded product is cut, and the tab hole and / or the lower liquid hole are manufactured by a die cutting method to obtain the insulating gasket.
[0077] The insulating gasket obtained in this embodiment is composed of polypropylene base material and porous silica dispersed in the base material, the mass ratio of polypropylene base material to porous silica is 5...
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Abstract
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