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Method of preparing carbon black by wet granulation

A wet granulation and granular carbon black technology, applied in the direction of fibrous fillers, can solve the problems of temperature fluctuation of carbon black at the outlet of the dryer, and achieve the effect of improving stability and preventing calculation errors.

Active Publication Date: 2019-02-01
SUZHOU BAOHUA CARBON BLACK
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This mode of relying on manual adjustment must not be adjusted in a timely and accurate manner, which will inevitably cause large fluctuations in the temperature of carbon black at the outlet of the dryer.

Method used

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  • Method of preparing carbon black by wet granulation
  • Method of preparing carbon black by wet granulation
  • Method of preparing carbon black by wet granulation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0078] The carbon black varieties prepared in Examples 1-3 are different, and the carbon black varieties prepared in Example 1 are carbon black varieties N326, carbon black varieties N330, and carbon black varieties N660

[0079] The hot air preheated to 550-650 ℃ by the air preheater is provided by the main supply fan, and sent to the combustion chamber of the reaction furnace through the hot air pipeline, mixed with the preheated and fully atomized fuel, and burned. The temperature range is 1500~1800℃. After the raw oil is preheated to 130-170 ℃ by the raw oil preheater, it is injected from the rear of the combustion chamber of the reaction furnace, and after atomization and shearing (the force of the high-temperature airflow on the oil droplets breaks the oil droplets, thereby further Atomization), the cracking reaction is carried out in the reaction section of the reactor to generate carbon black flue gas containing powdered carbon black and tail gas.

[0080] The carbon ...

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Abstract

The application provides a method of preparing carbon black by wet granulation, comprising: (1) collecting data, to be specific, acquiring dryer outlet carbon black temperature, primary lift outlet carbon black temperature and secondary lift outlet carbon black temperature as basic data; (2) estimating tail gas flow, to be specific, acquiring a coefficient of ratio of the tail gas flow to granulation water flow as well as a primary lift outlet carbon black temperature adjustment variable, and determining new tail gas flow for use in operation; (3) executing, to be specific , granulating and drying the carbon black according to the determined new tail gas flow. The method has the advantages that the quantity of tail gas fed to a dryer tail gas combustor is controlled in the carbon black preparation process so as to control carbon black drying temperature, the temperature of the carbon black at a dryer outlet can be stably controlled, it is effectively ensured that the obtained carbon black has qualified and stable water content, and the qualified carbon black is attained.

Description

technical field [0001] The application relates to the technical field of chemical industry, in particular to a method for preparing carbon black by wet granulation, in particular to automatically control the preparation process of wet granulation through the automatic calculation of the carbon black tail gas flow rate and the ratio coefficient of the granulation water flow rate A method of drying carbon black. Background technique [0002] At present, most domestic carbon black enterprises use the wet granulation process to produce carbon black. The wet granulation of carbon black is to put powdered carbon black and an aqueous solution containing a certain amount of binder (referred to as granulation water) in a granulator. , a method of forming granular carbon black by the rotation of the stirring teeth. After the granular carbon black leaves the pelletizer, the wet pellets must be dried by a rotary kiln dryer supplemented by external heating and passage of hot flue gas. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09C1/58
CPCC09C1/58
Inventor 王伟兴斛小晋王军晓
Owner SUZHOU BAOHUA CARBON BLACK