Radiation-proof glass and preparation method of radiation-proof glass
A radiation protection and glass technology, applied in the field of glass, can solve the problems of limited radiation shielding range of radiation protection glass, hidden dangers of radiation protection glass, damage to health, etc., to improve radiation protection effect, ideal compressive strength, and avoid pollution. Effect
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[0080] The present invention also proposes a method for preparing radiation-proof glass, which includes the following steps: providing raw material components, the raw material components are based on oxides, and contain the following components in terms of weight percentage:
[0081] SiO 2 , 3 to 5 copies;
[0082] B 2 o 3 , 40-45 copies;
[0083] La 2 o 3 , 25-30 copies;
[0084] ZrO 2 , 3 to 5 copies;
[0085] ZnO, 4-6 parts;
[0086] BaO, 35-40 parts;
[0087] WO 3 , 12 to 15 copies;
[0088] 0.1-0.3 parts of clarifying agent;
[0089] The raw material components are sequentially mixed, melted, clarified, homogenized, shaped, and annealed to obtain the radiation-proof glass.
[0090] In this embodiment, the raw materials used to make radiation-proof glass are in parts by weight, namely silicon dioxide, diboron trioxide, lanthanum trioxide, zirconium dioxide, zinc oxide, barium oxide, tungsten trioxide and clarified Agents are measured in parts by weight.
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Embodiment 1
[0108] Based on oxides, the radiation-proof glass contains the following components by weight:
[0109] SiO 2 , 3.11g;
[0110] B 2 o 3 , 41.68g;
[0111] La 2 o3 , 26.37g;
[0112] ZrO 2 , 4.44g;
[0113] ZnO, 5.07g;
[0114] BaO, 38.28g;
[0115] WO 3 , 14.44g;
[0116] Clarifying agent, 0.26g.
[0117] The preparation method of the radiation-proof glass includes the following steps: mixing the above-mentioned raw material components, grinding and dispersing the evenly mixed raw materials, dispersing by ultrasonic high-speed dispersion for 1 hour, and setting the ultrasonic frequency to 3.0k-5.5kHz. Melt the ground batch material, and when the melting temperature reaches 1290°C, keep it warm for 40 minutes, so that the radiation-proof glass batch material can be better melted, clarified and homogenized. After 40 minutes of heat preservation, the crucible was quickly taken out, and the sample was poured on the preheated iron mold. After 10 minutes, the heating re...
Embodiment 2
[0119] Based on oxides, the radiation-proof glass contains the following components by weight:
[0120] SiO 2 , 4.11g;
[0121] B 2 o 3 , 40g;
[0122] La 2 o 3 , 26.37g;
[0123] ZrO 2 , 3.84g;
[0124] ZnO, 5.57g;
[0125] BaO, 38.28g;
[0126] WO 3 , 14.44g;
[0127] Clarifying agent, 0.26g.
[0128] The preparation method of the radiation-proof glass includes the following steps: mixing the above-mentioned raw material components, grinding and dispersing the evenly mixed raw materials, dispersing by ultrasonic high-speed dispersion for 1 hour, and setting the ultrasonic frequency to 3.0k-5.5kHz. Melt the ground batch material, and when the melting temperature reaches 1290°C, keep it warm for 40 minutes, so that the radiation-proof glass batch material can be better melted, clarified and homogenized. After 40 minutes of heat preservation, the crucible was quickly taken out, and the sample was poured on the preheated iron mold. After 10 minutes, the heating res...
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