Preparation method of heat-resistant and anti-static water-based polyurethane/titanium diboride composite material
A water-based polyurethane and titanium diboride technology, which is applied in the field of special materials, can solve the problems of complex synthesis, high cost, and single function, and achieve the effects of low synthesis cost, improved heat resistance, and improved heat resistance
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[0018] In order to deepen the understanding of the present invention, the present invention will be further described below in conjunction with the examples, which are only used to explain the present invention, and do not constitute a limitation to the protection scope of the present invention.
[0019] Such as figure 1 As shown, the present embodiment provides a kind of preparation of heat-resistant and antistatic waterborne polyurethane / titanium diboride composite material, comprising the following steps:
[0020] Step 1: Synthesize water-based polyurethane (hereinafter collectively referred to as WPU). First, water-based polyurethane is synthesized in a 250ml four-necked flask, and 0.0015mol / 3g of polytetrahydrofuran and 0.0021mol / 0.275g of 2,2-dihydrofuran are added to the reactor. Methylolpropionic acid and 2ml of 1-methyl-2-pyrrolidone, then when the temperature is raised to 80°C, after the system becomes a uniform and stable solution, add 0.0062mol / 1.38g of isophorone ...
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